Slow crack growth and acoustic emission characteristics in COD test

Brittle material fractures at a critical value of stress intensity factor or crack opening displacement (COD) without any prior crack growth. In the ductile materials, however unstable fracture initiation may be preceded by a period of slow crack growth from the notch tip. Such slow crack growth may be an essential prelude to unstable fast fracture and thus COD at the start of slow crack growth can also be regarded as a critical value of the fracture characteristics. We have tried to apply the acoustic emission techniques to the COD test. Acoustic emission techniques can be used to detect the onset of slow crack growth and to obtain a relation between COD and AE characteristics in the COD test.     

Effect of stress wave shape on the crack propagation velocity in cyclic delayed failure

Crack propagation velocity in delayed failure under superposed repeating load, ($\text{d}\text{a/}\text{d}\text{t)}{}_{\mathrm{R}}$, was compared with that under static load, ($\text{d}\text{a/}\text{d}\text{t)}{}_{\mathrm{S}}$Two peaks appear on the relation between decreasing rate of crack propagation velocity, $\text{1-β = 1 ? (}\text{d}\text{a/}\text{d}\text{t))}{}_{\mathrm{R}}\text{/(}\text{d}\text{a/}\text{d}\text{t)}{}_{\mathrm{S}}$ and frequency, ?, both under sinusoidal and square load. By changing the ratio of holding time at maximum stress intensity factor to that at minimum stress intensity factor in square load, it was deduced that the existence of two peaks on the 1 ? β vs $\text{f}$ curve was caused by an asymmetric interaction between hydrogen atoms and cyclic moving of the position with triaxial tensile stress at crack tip. Moreover, the relation between 1 ? β and $\text{f}$ under the positive or negative saw tooth load could be well explained by the interaction model.     

Fracture properties of X-phase precipitation hardened ferritic stainless steel and ductility improvement of the steel

The mechanical properties of Fe-13 wt% Cr-2 wt% Mo-2.5 wt% Ti alloy were examined by tensile tests with respect to its fracture mechanism. In order to improve the properties, 1 wt% Nb was added and its effects were examined. In the temperature range, room temperature to 500° C, the fracture characteristics of the alloys are mainly governed by the characteristics of the x-phase precipitation. Fracture elongation is a function of (C/r)_1/2 where C is the radius of the x-phase and r is its mean spacing. 1 wt% Nb addition is an effective method for improving the ductility without a decrease in the strength of the alloy.     

Improvement of bitumen-waste product in leachability—Leachability of bitumen product containing BWR's evaporator concentrate

The method has been developed to improve the bitumen product which incorporates an evaporator concentrate from a BWR, with respect to the swelling and leaching. The leachability of the product has been measured by the method recommended by the IAEA. The swelling of the product is successfully prevented by the addition of calcium chloride. The specimen containing the waste up to Wa/B (Weight ratio of Na₂SO₄ + CaCl₂ and bitumen) = 60:40 shows no pronounced swelling, when it is immersed in water. The cumulative fractions of ¹³⁷Cs and ⁶⁰Co leached from a specimen which does not contain CaCl₂ are 0.65 and 0.2 at the leaching time of 30 days. On the hand, the corresponding value at 100 days for the specimen with calcium chloride addition is 5 × 10^?4 for ¹³⁷Cs and 1 × 10^?4 for ⁶⁰Co. The coating of the specimen surface with a fresh bitumen (5 mm thickness) reduces the leachability further. These results indicate that this method is effective to improve the bitumen product incorporating BWR's evaporator concentrate.     

Quantification of cell adhesion force with AFM: distribution of vitronectin receptors on a living MC3T3-E1 cell

Distribution of vitronectin (VN) receptors on a living murine osteoblastic cell was successfully measured by atomic force microscopy (AFM). First, the distribution of the integrin beta(5) subunit which constitutes a part of the VN receptor on the cell was confirmed by conventional immunohistochemistry after fixing the cell. To visualize the distribution of the receptor on a living cell by an independent and potentially a more quantitative method, the AFM was used with a microbead attached to the cantilever tip to increase the area of contact and VN was immobilized on the microbead. Force measurements were then performed over a large area of a living murine osteoblastic cell using the microbead covered with VN.     

Optical topography: practical problems and new applications

We will briefly review the present status of optical topography and then discuss the method of improving practicality, i.e., the signal-to-noise (S/N) ratio and the spatial resolution in observations of higher-order brain functions. The optimum wavelength pair improved the S/N ratio sixfold for deoxyhemoglobin, and new configurations of light irradiation and detection positions doubled the spatial resolution. We also report on developing application fields of optical topography. This modality will bridge the gap between natural sciences, neuroscience, and pedagogy, and show actual real-time brain activity.     

Visualization of phase objects by use of a differentiation filter

For the visualization of phase objects by use of a differentiation filter, the phase variation is changed into the intensity variation by differentiation, and then the differentiated image is integrated. In the method used in practice, the differentiated image has been recorded on a film, and then integrated by use of a filter. In this paper, however, the image differentiated by means of a filter is entered into a computer using a CCD camera and then integrated. As a result, the method provides rapid on-line processing. We have performed computer simulations and a detailed analysis of the differentiation filter and also provide the experimental results of three-dimensional image visualization.     

Active anion manipulation for emergence of active functions in the nanoporous crystal 12CaO·7Al<Subscript>2</Subscript>O<Subscript>3</Subscript>: a case study of abundant element strategy

This article reviews our approach to render 12CaO · 7Al₂O₃ (C12A7) electronically active using a new concept of ‘active anion manipulation’, where nanostructures embedded within the C12A7 crystal lattice are intentionally utilized to generate chemically unstable (‘water-free active’) anions. Anionic active oxygen radicals, O⁻ and O₂⁻, are formed efficiently in C12A7 cages under high oxygen activity conditions. The configuration and dynamics of O₂⁻ in cages are revealed by a combination of continuous-wave and pulsed electron paramagnetic resonance (EPR). It is demonstrated that metal-loaded C12A7 is a promising oxidation catalyst for syngas (CO + H₂) formation from methane. Furthermore, the O⁻ ion, the strongest oxidant among active oxygen species, can be extracted from the cage into an external vacuum by applying an electric field with thermal assistance, generating a high-density O⁻ beam in the order of μA cm⁻². In contrast, heat treatment of C12A7 in a hydrogen atmosphere forms H⁻ ions in the cages. The resultant C12A7:H⁻ exhibits a persistent insulator-conductor conversion upon ultraviolet-light or electron-beam irradiation. The irradiation-induced conversion mechanism is examined by first-principle theoretical calculations. Furthermore, the presence of a severely reducing environment causes the complete substitution of electrons for anions in the cages. The resulting C12A7:e⁻, which exhibits excellent stability and an electrical conductivity greater than 100 S cm⁻¹, is regarded as an ‘electride’, an ionic compound in which electrons serve as anions. The C12A7 electride exhibits a high potential for applications involving cold cathode and thermal field electron emissions due to its small work function. Electride fabrication methods suitable for large-scale production via melt processing are described. It is also demonstrated that proton or inert gas ion implantations into C12A7 thin films at elevated temperatures are effective for both H⁻ and electron doping.     

The Principles of Eliminating Pulsating Torque in Current Source Inverter Induction Motor Systems

The problem of reducing the pulsating torque in current source inverter induction motor systems is investigated. Two typical approaches presented in recent publications are analyzed by making clear 1) the correlation among the current harmonics and the torque harmonics, and 2) the conceptual contradiction existing between these two approaches. By synthesizing the analyzed results, fundamental principles for treating the current harmonics and torque harmonics are established. In addition, the method for evaluating the degree of torque ripple is described, along with a proposed criterion for torque ripple content. By applying this criterion to these two approaches, objective estimates of degree of torque pulsations, which were unfeasible so far, are now made possible.