Preparation of phenolic resin derived 3-D ordered macroporous carbon

Three-dimensionally ordered long-range macroporous carbon structures were prepared using commercially available phenolic resin by utilizing sacrificial colloidal silica crystalline arrays as templates that were subsequently removed by HF etching after pyrolysis in an argon atmosphere. SEM, TEM, and BET were employed to characterize the morphology and the surface area of the porous carbon structures. The pore size (150–1000 nm) and BET surface area, which reflect pore volume (298.6 m²/g (1.32 cm³/g) ∼ 93.7 m²/g (0.12 cm³/g)), of the macroporous carbon structures produced were approximately proportional to the size (150–1000 nm) of the sacrificial silica sphere templates used (annealing temp. 550°C). The achieved 550 nm porous carbon structures were examined to function as potential catalyst carriers and were successfully impregnated with Ag or Pt-Ru on their inner walls after borohydride reduction at room temperature. In addition, porous carbon patterns were fabricated using the ‘micromolding in capillary’ technique, which has potential applications in the microreaction technology.     

基于PXI总线的LVDS数据采集存储模块的设计

鉴于SAR原始数据量大以及数据传输速率限制的问题,设计了基于PXI的雷达回波和图像数据实时记录模块。大容量数据采集记录系统基于通用的商业PC平台设计,选用FPGA作为主控芯片对电路整体逻辑进行控制;利用LVDS作为数据传输接口对数据进行接收,实现了数据采集、缓存以及通过PXI总线上传至上位机硬盘,以便后续处理。文中介绍了系统方案的总体设计,以及采集存储硬件电路的设计,并对电路的关键技术给以详细的分析。     

电解法处理利福霉素SV钠废渣分离液的研究

根据电化学原理，采用电解法，利用铁屑与炭粒作电极，处理利福霉素SV钠药渣分离液，讨论各种因素对分离液污染物作效果的影响，COD去除率可达91．8％左右，脱色率可达95％左右。     

Effects of the reinforcement and toughening of acrylate resin/CaCO3 nanoparticles on rigid poly(vinyl chloride)

Novel composite particles based on nanoscale calcium carbonate (nano‐CaCO₃) as the core and polyacrylates as the shell were first synthesized by in situ encapsulating emulsion polymerization in the presence of the fresh slush pulp of calcium carbonate (CaCO₃) nanoparticles. Subsequently, these modified nanoparticles were compounded with rigid poly(vinyl chloride) (RPVC) to prepare RPVC/CaCO₃ nanocomposites. At the same time, the effects of the reinforcement and toughening of these modified nanoparticles on RPVC were investigated, and the synergistic effect of modified nanoparticles with chlorinated polyethylene (CPE) was also studied. The results showed that in the presence of nano‐CaCO₃ particles, the in situ emulsion polymerization of acrylates was carried out smoothly, and polyacrylates successfully encapsulated on the surface of nano‐CaCO₃ to prepare the modified nanoparticles, breaking down nano‐CaCO₃ particle agglomerates, improving their dispersion in the matrix, and also increasing the particle–matrix interfacial adhesion. Thus, the effects of the reinforcement and toughening of these modified nanoparticles on RPVC were very significant, and the cooperative effect of the nanoparticles with CPE occurred in the united modification system. Scanning electron microscopy analyses indicated that large‐fiber drawing and network morphologies coexisted in the system of joint modification of nanoparticles with CPE. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 103: 3940–3949, 2007     

脂肪酸系列表面活性剂的研究进展

概括和综述了4大类10余个脂肪酸系列表面活性剂的合成、性能和应用现状，重点评述了烷醇酰胺及其衍生物、乙氧基化脂肪酸甲酯、脂肪酸甲酯磺酸盐、N-酰基ED3A、氨基酸、咪唑啉、甜菜碱、双子表面活性剂等脂肪酸系列表面活性剂的研究进展。此系列表面活性剂易生物降解、安全、多功能和高效能。     

跨文化交际中中式英语词汇层面的表现

从跨文化交际角度,分析了中式英语在词汇层面上的三种表现形式:望文生义、词汇冗余和文化词汇误用.认为中式英语的形成与思维方式差异和文化差异直接相关.     

"再听证"条款考疑

介绍了日本、韩国及我国台湾地区的行政程序法关于再次举行听证会的规定.分析了我国行政程序法试拟稿及部分地方立法中有关于再听证规定存在的问题,并提出了具体的修改意见.     

金纳米线拉伸行为的分子动力学模拟

采用分子动力学方法模拟了不同截面尺寸金纳米线的拉伸力学行为。计算结果表明:相同长度的金纳米线弹性模量随着截面尺寸的减小而减小,而其屈服强度随着截面尺寸的减小而增大,并且发生屈服推迟现象。应力—应变曲线与形变过程相对应。在弹性变形阶段,纳米线形变不显著;随着应变量的增加,发现纳米线出现大量堆垛层错。     

声频谱测井仪器的研制和野外实验

研制成功的声频谱测井仪器在井下发射和接收三种频率的声波信号,其中发射和接收20kHz声波信号的声系有一个发射和四个接收探头,源距为2．1～2．568m,间距为0．156m;发射和接收40kHz声波信号的声系由一个发射和两个接收探头组成,源距1．0—1．5m,间距0．5m;发射和接收10kHz声波信号的声系由一个发射和两个接收探头组成,源距为2．168—2．668m,间距0．5m．用三种不同的频率的声波进行测量记录目的是获得井壁径向深度不同处介质的声学信息,而且不同频率的声波信号在岩石中传播过程中频谱变化也是井壁岩层的可用声学信息．在井下的信息采集、数据传输、地面记录和监控全部由计算机控制．该仪器已经在大庆油田的三口井中成功的进行了野外实验．     

Application of open-pit and underground mining technology for residual coal of end slopes

Given the conditions of residual coal from the boundary of a flat dipping open-pit mine,which uses strip areas mining and inner dumping with slope-covering,we propose an open-pit and underground integrated mining technology for residual coal of end slopes.In the proposal a conveyance road and ventilation conveyance near the slope are built,corresponding to the pit mining area and the surface coal mine dump,as well as an interval haulage tunnel and air-inlet tunnel.The outcome shows that such mining method may reduce the effect to slope stability from underground mining,it does not affect the dumping advance and has a high recovery rate of residual coal resources.The working face is timbered by single hydraulic props,transported by a scraper conveyor and supported by coal walls.This method of mining is one of layered top coal caving,with high resource recovery,low production cost where positive economic benefit can be realized.