固化剂对环氧树脂/蒙脱土纳米复合材料中蒙脱土剥离行为的影响

采用阳离子交换的方法对蒙脱土进行了有机改性，使蒙脱土由亲水性变成亲油性，并使其层间距由原来的1．2nm扩大到2．2nm。分别使用甲基四氢苯酐和4，4’-二胺基二苯基甲烷为固化剂，制备两种环氧树脂／蒙脱土纳米复合材料，并用x一射线衍射仪和透射电镜(TEM)分析有机蒙脱土在环氧树脂中的剥离行为。研究表明，固化剂的选择对有机蒙脱土的剥离行为有很大的影响，用固化剂甲基四氢苯酐和促进剂苄基二甲胺后，有机蒙脱土容易被剥离而得到剥离型的纳米复合材料，而用4，4’-二胺基二苯基甲烷固化剂未能使有机蒙脱土剥离后形成插层型纳米复合材料。     

Effect of Na<Subscript>2</Subscript>CO<Subscript>3</Subscript> and CaCO<Subscript>3</Subscript> on coreduction roasting of blast furnace dust and high-phosphorus oolitic hematite

Iron was recovered from blast furnace dust and high-phosphorus oolitic hematite in the presence of Na₂CO₃ and CaCO₃ additives. The functions of Na₂CO₃ and CaCO₃ during the coreduction roasting process were investigated by XRD and SEM-EDS analyses. Results indicate that these additives not only hinder the reduction of fluorapatite, CaCO₃ also decreases the P content of direct reduced iron (DRI) by increasing the reduction alkalinity. P remains as fluorapatite in the slag, which can be removed by grinding and magnetic separation under optimal conditions. The Na₂CO₃ promotes hematite reduction and improves the iron recovery (ε_Fe) by replacing the FeO from fayalite, which results in quick growth and aggregation of metallic iron and improvement of ε_Fe in DRI. A DRI with 91.88 mass% Fe, and 0.065 mass% P can be achieved at a recovery of 87.86 mass% under the optimal condition.     

Innovation output and state ownership: empirical evidence from China’s listed firms

Abstract

China has experienced a surge in innovation output in which state-owned enterprises (SOE) play an essential role. Using panel data of Chinese listed firms, this paper examines the influence of state ownership on innovation output at the firm level. Controlling for size, we analyse the effects of central and local government control on the number of firms’ patent applications in different time periods. Doing so, standard assumptions on state ownership’s inhibiting character are confirmed. However, we then qualify these findings by running separate models for different regions and sectors finding that the impact of state-control on innovation performance depends on a number of conditions. More precisely, state control of firms has a negative impact on innovation output in particular in China’s Northeast region and in mid-tech sectors whereas under other circumstances it does either not matter or can even exert a positive influence.     

Preparation,ablation behavior and mechanism of C/C-ZrC-SiC and C/C-SiC composites

ZrC precursor was synthesized by a solution approach using ZrOCl₂·8H₂O, acetylacetonate, glycerol and boron-modified phenolic resin. A ZrC yield of ~ 40.56 wt% was obtained at 1500 °C in the C/Zr molar ratio of 1:1. C/C-ZrC-SiC composites were fabricated by a combined processes of chemical vapor infiltration (CVI) and precursor infiltration and pyrolysis (PIP) using the synthesized ZrC precursor. For comparison, C/C-SiC composites were prepared by CVI. Thermogravimetric analysis showed that C/C-ZrC-SiC composites exhibited better oxidation resistance than C/C-SiC composites. After oxyacetylene torch ablation, the mass ablation rate of C/C-ZrC-SiC composites was 9.23% lower than that of C/C-SiC composites. The porous ZrO₂ skeleton in the ablation center was prone to be peeled off by the flame flow, resulting in the higher linear ablation rate of C/C-ZrC-SiC composites. The oxide layers of ZrO₂ and SiO₂ were formed on the transition and brim region of C/C-ZrC-SiC composites and acted as effective heat and oxygen barriers. For C/C-SiC composites, the C-SiC matrix was severely depleted in the ablation center and the formed SiO₂ layer in the brim region could protect the matrix against further ablation.     

Research on corrosion performance of 6061 aluminum alloy in salt spray environment

Salt spray corrosion test was carried out on 6061 aluminum alloy, and quasi-static tensile test at room temperature was carried out on the sample with universal testing machine. The effect of salt spray corrosion on the mechanical properties of 6061 aluminum alloy was studied by scanning electron microscope (SEM), energy dispersive spectrometer (EDS) and electrochemistry. The corrosion rate of 6061 aluminum alloy was quantitatively characterized by different corrosion parameters. It was found that local corrosion of 6061 aluminum alloy occurred in salt spray environment, mainly pitting corrosion and intergranular corrosion. With the increase of corrosion time, the polarization resistance of 6061 aluminum alloy decreases, and the corrosion rate significantly increases. The average corrosion rate and the maximum corrosion rate of 6061 aluminum alloy were characterized by corrosion weight loss and corrosion pit depth. And they can be transformed into each other. The mechanical properties of 6061 aluminum alloy were mainly affected by the depth of corrosion pit. With the increase of corrosion time, the tensile strength and fracture strain decreased, resulting in poor plasticity of the sample. At the same time, the change of elongation of 6061 aluminum alloy can be accurately predicted by the depth of corrosion pit.     

600MW机组危急遮断装置故障分析与处理

针对漳山发电厂3号机组在汽轮机定速喷油试验时不成功的情况,分析了危急遮断装置存在的问题,提出了针对性的解决方法,从而提高了整个危急遮断装置的安全稳定性。     

Motivational,emotional, and behavioral correlates of fear of missing out

Social media utilities have made it easier than ever to know about the range of online or offline social activities one could be engaging. On the upside, these social resources provide a multitude of opportunities for interaction; on the downside, they often broadcast more options than can be pursued, given practical restrictions and limited time. This dual nature of social media has driven popular interest in the concept of Fear of Missing Out – popularly referred to as FoMO. Defined as a pervasive apprehension that others might be having rewarding experiences from which one is absent, FoMO is characterized by the desire to stay continually connected with what others are doing. The present research presents three studies conducted to advance an empirically based understanding of the fear of missing out phenomenon. The first study collected a diverse international sample of participants in order to create a robust individual differences measure of FoMO, the Fear of Missing Out scale (FoMOs); this study is the first to operationalize the construct. Study 2 recruited a nationally representative cohort to investigate how demographic, motivational and well-being factors relate to FoMO. Study 3 examined the behavioral and emotional correlates of fear of missing out in a sample of young adults. Implications of the FoMOs measure and for the future study of FoMO are discussed.     

Inverse Reconstruction of Fracture Splitting Connecting Rod and its Strength and Fatigue Life

Journal of Failure Analysis and Prevention - To investigate the strength and fatigue life of a fracture-split connecting rod, this study combines experiments on connecting rod fracture splitting,...