Two-stage nuclear demagnetization refrigerator

Two-stage nuclear demagnetization has been performed using PrCu₆ and Cu as coolants. The Cu nuclear stage reached temperatures as low as 10 K with a rate of temperature rise of less than a few K/h. The corresponding conduction electron temperature is estimated to be less than 50 K. A nuclear orientation thermometer of Al ⁵⁴Mn has been successfully used to measure temperatures down to 10 K.Supported by the Japan Society for the Promotion of Science.     

Electrical and thermal magnetoconductivities of single-crystal beryllium at low temperatures and its use as a heat switch

The effects of transverse magnetic fields up to 955 kA/m (12 kOe) on the electrical and thermal conductivities of single-crystal beryllium have been measured between 2 and 300 K. Most of the measurements were made on a sample with a resistance ratio of1340. This sample was pure enough so that the intrinsic electronic thermal resistivity could be measured for the first time. It was found to have the usual T² behavior. The current and heat flow were along the hexagonalc axis of the crystal, while the thermal and electrical conductivities were studied as a function of the angle of the magnetic field in the basal plane. Below about 50 K the thermal conductivity could be reduced by several orders of magnitude by applying the magnetic field. The lattice conductivity, extrapolated from the measurements in the magnetic field, is given by k =T², where =1.6×10^–4 W/cm K³. This value is in reasonable agreement with that obtained from measurements of beryllium alloys. The use of single-crystal beryllium as a heat switch for temperatures below about 30 K is discussed.This research was supported by the Advanced Research Projects Agency of the Department of Defense and was monitored by ONR under Government Order Number NAonr-1-75.     

The effects of time-compressed instruction and redundancy on learning and learners’ perceptions of cognitive load

Can increasing the speed of audio narration in multimedia instruction decrease training time and still maintain learning? The purpose of this study was to examine the effects of time-compressed instruction and redundancy on learning and learners’ perceptions of cognitive load. 154 university students were placed into conditions that consisted of time-compression (0%, 25%, or 50%) and redundancy (redundant text and narration or narration only). Participants were presented with multimedia instruction on the human heart and its parts then given factual and problem solving knowledge tests, a cognitive load measure, and a review behavior (back and replay buttons) measure. Results of the study indicated that participants who were presented 0% and 25% compression obtained similar scores on both the factual and problem solving measures. Additionally, they indicated similar levels of cognitive load. Participants who were presented redundant instruction were not able to perform as well as participants presented non-redundant instruction.     

Clump splitting via bottleneck detection and shape classification

Under-segmentation of an image with multiple objects is a common problem in image segmentation algorithms. This paper presents a novel approach for splitting clumps formed by multiple objects due to under-segmentation. The proposed algorithm includes three steps: (1) decide whether to split a candidate connected component by application-specific shape classification; (2) find a pair of points for clump splitting and (3) join the pair of selected points. In the first step, a shape classifier is applied to determine whether a connected component should be split. In the second step, a pair of points for splitting is detected using a bottleneck rule, under the assumption that the desired objects have roughly a convex shape. In the third step, the selected splitting points from step two are joined by finding the optimal splitting line between them, based on minimizing an image energy. The shape classifier is built offline via various shape features and a support vector machine. Steps two and three are application-independent. The performance of this method is evaluated using images from various applications. Experimental results show that the proposed approach outperforms the state-of-the-art algorithms for the clump splitting problem.     

Maintaining awareness using policies; Enabling agents to identify relevance of information

The field of computer supported cooperative work aims at providing information technology models, methods, and tools that assist individuals to cooperate. The presented paper is based on three main observations from literature. First, one of the problems in utilizing information technology for cooperation is to identify the relevance of information, called awareness. Second, research in computer supported cooperative work proposes the use of agent technologies to aid individuals to maintain their awareness. Third, literature lacks the formalized methods on how software agents can identify awareness. This paper addresses the problem of awareness identification. The main contribution of this paper is to propose and evaluate a formalized structure, called Policy-based Awareness Management (PAM). PAM extends the logic of general awareness in order to identify relevance of information. PAM formalizes existing policies into Directory Enabled Networks-next generation structure and uses them as a source for awareness identification. The formalism is demonstrated by applying PAM to the space shuttle Columbia disaster occurred in 2003. The paper also argues that efficacy and cost-efficiency of the logic of general awareness will be increased by PAM. This is evaluated by simulation of hypothetical scenarios as well as a case study.     

Mechanochemically assisted room temperature solid state metathesis reaction for the synthesis of MMoO4 (M = Ca, Sr and Ba)

This communication reports a novel mechanochemically assisted room temperature solid state metathesis reaction for the synthesis of submicron-size alkaline-earth molybdates crystallizing in a tetragonal Scheelite structure. The solids were characterized by powder XRD, FTIR, TGA, DTA, SEM, EDAX and TEM to ascertain their composition, phase homogeneity and morphology.     

Low temperature synthesis and characterisation of lecontite, (NH4)Na(SO4)·2H20

Lecontite, (NH₄)Na(SO₄).2H₂O, was synthesised at room temperature in high purity compared to earlier work with a minor impurity of mascagnite, (NH₄)₂SO₄. Rietveld refinement of the XRD results confirmed the crystal structure and unit cell dimensions as published earlier. Raman and Infrared spectroscopy, in conjunction with factor group analysis, resulted in a complex pattern of overlapping sulphate, NH and OH modes. The NH modes υ₁ was observed around 2880 cm⁻¹, υ₂ around 1700 cm⁻¹ overlapping with water OH-bending modes, υ₃ around 3300 cm⁻¹ overlapping with water OH-stretching modes around 3023, 3185 and 3422 cm⁻¹, and υ₄ around 1432, 1447 and 1462 cm⁻¹. The sulphate group in the crystal structure displays a decrease in symmetry from T_d as evidenced by the activation of the ν₁ mode at 982 cm⁻¹ and the ν₂ mode around 452 cm⁻¹ in the Infrared spectrum. The υ₃ mode shows clear splitting in the infrared spectra with a strong band at 1064 cm⁻¹ accompanied by two shoulders at 1107 and 1139 cm⁻¹. The Raman spectra show three weak bands at 1068, 1109 and 1135 cm⁻¹ with a shoulder at 1155 cm⁻¹. Similar splitting was observed for the υ₄ mode around 611 and 632 cm⁻¹ in the Infrared and Raman spectra, respectively.     

Indium oxide thin film based ammonia gas and ethanol vapour sensor

A sensor for ammonia gas and ethanol vapour has been fabricated using indium oxide thin film as sensing layer and indium tin oxide thin film encapsulated in poly(methyl methacrylate) (PMMA) as a miniature heater. For the fabrication of miniature heater indium tin oxide thin film was grown on special high temperature corning glass substrate by flash evaporation method. Gold was deposited on the film using thermal evaporation technique under high vacuum. The film was then annealed at 700 K for an hour. The thermocouple attached on sensing surface measures the appropriate operating temperature. The thin film gas sensor for ammonia was operated at different concentrations in the temperature range 323–493 K. At 473 K the sensitivity of the sensor was found to be saturate. The detrimental effect of humidity on ammonia sensing is removed by intermittent periodic heating of the sensor at the two temperatures 323K and 448 K, respectively. The indium oxide ethanol vapour sensor operated at fixed concentration of 400 ppm in the temperature range 293–393 K. Above 373 K, the sensor conductance was found to be saturate. With various thicknesses from 150–300 nm of indium oxide sensor there was no variation in the sensitivity measurements of ethanol vapour. The block diagram of circuits for detecting the ammonia gas and ethanol vapour has been included in this paper.     

DAE for Frictional Contact Modeling of Constrained Multi-Flexible Body Systems

A general formulation for modeling frictional contact interactions in a constrained multi-flexible body system is outlined in this paper. The governing differential-algebraic equations (DAE) for the constrained motion contains not only a frictional term but also, the unknown contact conditions. These contact conditions are characterized by a set of nonlinear complementarity equations. To demonstrate the model, a falling-spinning beam impacting a rough elastic ground with damping is solved and comparison with Stewart-Trinkles' results provided.     

On glass formation for a Na2O·4TeO2 melt: Effect of melting temperature, time, and raw material

The effect of melting temperature, time, and the type of raw material, NaNO₃ or Na₂CO₃, as a source for Na₂O on the glass formation for a Na₂O·4TeO₂(NT₄) melt was investigated. Melting with NaNO₃ at 750°C for a short time (15 min) produced a glass that is slightly more chemically durable and more resistant to crystallization than glasses melted at a higher temperature (800°C), or for a longer time (60 min), or using Na₂CO₃. A thin surface layer (<1.5 nm) that contains some nitrogen and a higher concentration of bridging oxygen is suspected to be the reason for the higher chemical durability and higher resistance to crystallization for this glass. However, melting at 800°C for 60 min produced a glass, whose properties were independent of the type of raw material, NaNO₃ or Na₂CO₃, used.