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61.
Magorzata Jastrzbska-Glapa Jacek Mochowski Wanda liwa 《Advanced Synthesis \u0026amp; Catalysis》1977,319(6):883-889
The synthesis of seven diazaphenanthrene aldehydes and their oximes via oxidation of corresponding methylderivatives is given and the n.m.r. spectra of the aldehydes are discussed. The synthesis of three new methyl diazaphenanthrenes by the Skraup method is presented. 相似文献
62.
Krystian Kloc Jacek Mlochowski Zdzislaw Szulc 《Advanced Synthesis \u0026amp; Catalysis》1977,319(6):959-967
Syntheses of azafluorenones from monoazaphenanthrenes and phenanthrolines has ben investigated. 1- and 4-monoazaphenanthrenes have been oxidized by J2O5 in acetic acid to give quinones which were converted to 4- and 1-azafluoren-9-ones in alkaline media. Phenanthrolines can be oxidized directly by means of permanganate in alkaline medium to 1,5-, 1,6-, 1,8-, 2,5- and 3,5-diazafluoren-9-ones. From 1-, 4-azaphenanthrene- and 1,8-phenanthrolinequinones new benzopyrido- and dipyridophenazines have been synthesized. 相似文献
63.
Charles Musca Jaroslaw Antoszewski John Dell Lorenzo Faraone Józef Piotrowski Zenon Nowak 《Journal of Electronic Materials》1998,27(6):740-746
This paper describes a new multi-heterojunction n
+pp photovoltaic infrared photodetector. The device has been developed specifically for operation at temperatures of 200–300K
in the long wavelength (8–14 μm) range of the infrared spectrum. The new structure solves the perennial problems of poor quantum
efficiency and low dynamic resistance found in conventional long wavelength infrared photovoltaic detectors when operated
near room temperature. Computer simulations show that devices with properly optimized multiple heterojunctions are capable
of achieving the performance limits imposed by the statistical nature of thermal generation-recombination processes. In order
to demonstrate the technology, multiple heterojunction devices have been fabricated on epilayers grown by isothermal vapor
phase epitaxy of HgCdTe and in situ As p-type doping. The detector structures were formed using a combination of conventional dry etching, angled ion milling,
and angled thermal evaporation for contact metal deposition. These multi-junction n
+pp HgCdTe heterostructure devices exhibit performances which make them useful for many applications. D* of optically immersed
multiple heterostructure photovoltaic detectors exceeding 108cmHz1/2/W were measured at λ=10.6 μm and T=300K. 相似文献
64.
Karolina Grabowska Marcin Sosnowski Jaroslaw Krzywanski Karol Sztekler Wojciech Kalawa Anna Zylka Wojciech Nowak 《热科学学报(英文版)》2018,27(5):421-426
Ecological adsorption technology is becoming a focus of attention by industry due to the utilization of low grade thermal energy sources for cooling production. It can be a promising part of sustainable development concept of the global economy. Therefore, research aiming at improving their performance i.e. Coefficient of Performance (COP) by optimizing the construction of sorption beds with a built in heat exchanger system is crucial. The heat transfer characteristics between the bed of porous media (sorbent) and surface of the heat exchanger system determine the heating power of an adsorption chiller. The HP increase can be obtained by heat transfer intensification due to the increase in the thermal conductivity of the sorbent layer in the vicinity of the heat exchanger’s surface. The novel modification of the sorbent layer structure is proposed in the paper in order to improve the heat transfer processes in the heat exchanger boundary layer. The analysis of desorption process conditions in the parametric model of a coated and fixed adsorption bed design is presented in the paper. The computational fluid dynamics (CFD) with conjugate heat transfer analysis is used to determine the crucial input parameters (temperature distribution in the sorbent bed) for further analytical calculations. The commercial code Ansys Fluent was used to perform numerical simulations. The developed computational model consisted of three subdomains representing heating water, heat exchanger material (copper) and sorbent (silica gel). The comparison of a novel coated design and a conventional fixed bed is discussed in the paper. The numerical analysis is based on experimental thermal conductivity measurements of the sorbent layer in different configurations, which were performed using Laser Flash Method. 相似文献
65.
Does office space occupation matter? The role of the number of persons per enclosed office space,psychosocial work characteristics,and environmental satisfaction in the physical and mental health of employees
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The study examined the effects of office space occupation, psychosocial work characteristics, and environmental satisfaction on physical and mental health of office workers in small‐sized and open‐plan offices as well as possible underlying mechanisms. Office space occupation was characterized as number of persons per one enclosed office space. A total of 207 office employees with similar jobs in offices with different space occupation were surveyed regarding their work situation (psychosocial work characteristics, satisfaction with privacy, acoustics, and control) and health (psychosomatic complaints, irritation, mental well‐being, and work ability). Binary logistic and linear regression analyses as well as bootstrapped mediation analyses were used to determine associations and underlying mechanisms. Employee health was significantly associated with all work characteristics. Psychosocial work stressors had the strongest relation to physical and mental health (OR range: 1.66–3.72). The effect of office space occupation on employee health was mediated by stressors and environmental satisfaction, but not by psychosocial work resources. As assumed by sociotechnical approaches, a higher number of persons per enclosed office space was associated with adverse health effects. However, the strongest associations were found with psychosocial work stressors. When revising office design, a holistic approach to work (re)design is needed. 相似文献
66.
Ethernet passive optical networks (EPONs) have attracted considerable attention from the industry, as they offer a simple, highly flexible and cost-effective solution to the problem of providing broadband access to a customer. The authors present a new approach to bandwidth allocation in EPONs where the optical line terminator (OLT) has full control over the access mechanism. This results in much simpler optical network unit (ONU) architecture. It is shown that such an OLT-centric architecture offers full support for differentiated services and makes enforcement of service level agreements possible. Extensive simulation experiments show that bandwidth allocation algorithms deployed in such a centralised environment can deliver good performance in terms of average and maximum packet delay. The authors introduce two new algorithms that target SLA-aware EPONs and provide a good protection of offered quality of service against interference from other sources. 相似文献
67.
68.
We propose a method for the assessment of the state of welded joints in terms of arc voltage signals and feed rate appraisal. The signals were recorded during laboratory tests. For the appraisal of the signals, we applied numerical parameters such as, for instance, kurtosis. On the basis of analysis results, we developed diagnostic rules which were written in the binary diagnostic matrix. The proposed method has been implemented in the form of software, the correctness of which has been verified on experimental data. 相似文献
69.
70.
Vibration analysis of machines operating under non-stationary operational conditions requires special attention. This refers to the necessity of use of order tracking algorithms together with additional advanced signal processing methods, especially when faults indicators of interest are located in resonance frequency ranges. 相似文献