富氧氮氧化硅薄膜退火的研究

利用红外吸收(IR)谱和X射线光电子谱(XPS)对富氧氮氧化硅(oxygen-rich SiOxNy)及其在600、750和900℃下退火后样品的微结构进行了研究.实验中除观察到N、H的释放外,首次发现退火会导致SiOxNy中O的释放,同时还发现退火温度不同,H、O、N元素的释放量以及微结构的变化都不相同,根据这些现象,提出了5个化学反应过程并予以解释.     

核电厂管系振动鉴定

本文介绍了核电厂管道振动鉴定概况,讨论了目前使用的管系振动的鉴定方法,给出了鉴定准则。     

Development of nano indium tin oxide (ITO) grains by alkaline hydrolysis of In(III) and Sn(IV) salts

Indium tin oxide (ITO) nano powders of different compositions (In: Sn = 90: 10, 70: 30 and 50: 50) were prepared by heat treatment (300-450°C) of mixed hydroxides of In(III) and Sn(IV). The hydroxides were obtained by the reaction of aq. NH₃ with mixed aq. solutions of In(NO₃)₃ and SnCl₄. FTIR and TG/DTA studies revealed that powders existed as In(OH)₃H₂O—SnO₃H₂H₂O in the solid state and then they transformed to In₂O₃—SnO₂ via some metastable intermediates after 300°C. Cubic phase of In₂O₃ was identified by XRD for the oxides up to 30% of Sn. Particle size measurements of the solid dispersed in acetone and SEM study for microstructure showed that the oxides were in the nano range (55-75 nm) whereas the size range determined from Debye-Scherrer equation were 11–24 nm.     

凝析气藏物质平衡方程的改进与应用

为了提高凝析气藏油气采收率，通常采用目前最有效的循环注气保持地层压力的开采方式。在此开采方式下，直接采用气藏物质平衡方程进行地质储量计算将出现很大偏差。针对这种情况，将气藏物质平衡方程进行了改进，得到凝析气藏在注气开发方式下的物质平衡方程。     

A computational study of LP-based heuristic algorithms for two-dimensional guillotine cutting stock problems

In this paper we develop and compare several heuristic methods for solving the general two-dimensional cutting stock problem. We follow the Gilmore-Gomory column generation scheme in which at each iteration a new cutting pattern is obtained as the solution of a subproblem on one stock sheet. For solving this subproblem, in addition to classical dynamic programming, we have developed three heuristic procedures of increasing complexity, based on GRASP and Tabu Search techniques, producing solutions differing in quality and in time requirements. In order to obtain integer solutions from the fractional solutions of the Gilmore-Gomory process, we compare three rounding procedures, rounding up, truncated branch and bound and the solution of a residual problem. We have coded and tested all the combinations of algorithms and rounding procedures. The computational results obtained on a set of randomly generated test problems show their relative efficiency and allow the potential user to choose from among them, according to the available computing time. Rceived: January 9, 2001 / Accepted: December 10, 2001     

用于铁谱分析磁化液使用规范的研究

本文简述了铁谱分析技术和磁化液的基本原理。在大量试验的基础上，建立了用于铁谱分析技术磁化液的使用规范。     

小型静压桩压桩力系数取值方法的探讨

由于《建筑桩基技术规范》 (JGJ94 - 94 )和《锚杆静压桩技术规程》 (YBJ2 2 7- 91)表达的不少概念和立足点有着根本区别 ,因此目前在小型静压桩设计、施工、质量检测和施工验收时相关人员在引用规范和规程时出现了不尽统一的现象。本文根据相应规范、规程的有关规定 ,结合现场试验 ,进行分析探讨 ,提出了小型静压桩压桩力系数的取值方法。     

STUDY ON GIS BASED PREDICTION SYSTEM FOR RADIO WAVE PROPAGATION IN UBAN REGION

In this letter, an integrated application of the prediction for radio wave propagation with the Geographic Information System (GIS) is presented and a real prediction system based on GIS is implemented.     

Fuel management of the HTR-10 including the equilibrium state and the running-in phase

The mode of fuel management of the HTR-10 was studied, including the simulation of the fuel shuffling process and the measurement of the burnup of a fuel element. The prior consideration was the design of the equilibrium state. Based on this the fuel loading of the initial core and the fuel shuffling mode from the initial core through the running-in phase into the equilibrium state were studied. The code system VSOP was used for the physical layout of the HTR-10 at the equilibrium state and in the running-in phase. For the equilibrium state, in order to lessen the difference between the peak and the average burnup, 5-fuel-passage-through-the-core was chosen for the fuel management. The average burnup of the spent fuel for the equilibrium core is 80 000 MWd t⁻¹, and the peak value of it is less than 100 000 MWd t⁻¹ when the burnup of the recycled fuel element is under 72 000 MWd t⁻¹. The mixture of fuel element and graphite element was used for the initial core loading, the volume fractions of the fuel and the graphite elements were 0.57 and 0.43, respectively. During the running-in phase, the volume fraction of graphite will decrease with the fresh fuel elements being loaded from the top of the core and the graphite elements discharged from the bottom of the core. The fuel shuffling mode is similar to that of the equilibrium state. The burnup limit of recycled fuel element is also 72 000 MWd t⁻¹ and the peak burnup is less than 100 000 MWd t⁻¹. Finally the core will be full of fuel elements with a certain profile of burnup and reaches the equilibrium state. According to the characteristics of the pebble-bed high temperature gas-cooled reactor, a calibrating method of concentration of ¹³⁷Cs was proposed for the measurement of fuel burnup.