One step method of structure engineering porous graphitic carbon nitride for efficient visible-light photocatalytic reduction of Cr(Ⅵ)

Porous g-C3N4 nanosheets (PCN) were prepared by the nickel-assisted one-step thermal polymerization method.Hydrogen (H2) which was produced by the reaction between nickel (Ni) foam and ammonia (NH3) defined the structure and properties of PCN.During the formation of PCN,the participation of H2 not only enhanced the spacing between layers but also boosted the specific surface area that more active sites were exposed.Additionally,H2 promoted pores formation in the nanosheets,which was beneficial to the transfer of photons through lamellar structure and improved the absorption efficiency of visible light.Remarkably,the obtained PCN possessed better Cr(Ⅵ) photocatalytic reduction efficiency than pure g-C3N4.The reaction rate constant (k) of PCN (0.013 min-1) was approximately twice that of bare g-C3N4 (0.007 min-1).Furthermore,the effects of original pH and concentration of Cr(Ⅵ)-containing solution on removal efficiency of Cr(Ⅵ) were explored.A possible photocatalytic mechanism was proposed based on the experiments of radical scavengers and photoelectrochemical characterizations.     

坛紫菜蛋白质提取工艺优化及其特性分析

为了开展坛紫菜高值化加工利用，以坛紫菜为原料、蛋白质提取率为评价指标，通过考察提取溶剂、超声时间和功率、料液比、pH等单因素实验、正交试验设计优化超声波提取工艺，对其等电点、乳化性、起泡性等基础特性进行分析，并进行抗氧化活性测定。结果表明，在超声全程时间50 min、超声功率1350 W条件下，坛紫菜蛋白质提取率为60.98%±1.01%。同时通过对所提取的坛紫菜蛋白质特性分析结果显示，坛紫菜蛋白质的等电点为4.5，在等电点附近，坛紫菜蛋白质有较好的泡沫稳定性，可达80.84%±2.95%；抗氧化测定结果显示，坛紫菜蛋白质在5~50 mg/mL范围内具有较强的抗氧化活性，浓度为50 mg/mL时，总抗氧化能力为2.89±0.09 U/mL，ABTS+自由基清除能力相当于0.83±0.08 mmol/L Trolox，DPPH清除率在10 mg/mL时达到68.04%±0.73%。该研究可以为坛紫菜资源的开发利用提供一定的理论依据和技术支持。     

Generating Questions Based on Semi-Automated and End-to-End Neural Network

With the emergence of large-scale knowledge base, how to use triple information to generate natural questions is a key technology in question answering systems. The traditional way of generating questions require a lot of manual intervention and produce lots of noise. To solve these problems, we propose a joint model based on semi-automated model and End-to-End neural network to automatically generate questions. The semi-automated model can generate question templates and real questions combining the knowledge base and center graph. The End-to-End neural network directly sends the knowledge base and real questions to BiLSTM network. Meanwhile, the attention mechanism is utilized in the decoding layer, which makes the triples and generated questions more relevant. Finally, the experimental results on SimpleQuestions demonstrate the effectiveness of the proposed approach.     

An index structure supporting rule activation in pervasive applications

World Wide Web - Rule mechanism has been widely used in many areas, such as databases, artificial intelligent and pervasive computing. In a rule mechanism, rule activation decides which rules are...     

Evaluation of Scale and Corrosion Inhibition of Modified Polyaspartic Acid

Amino acid modified polyaspartic acids were evaluated as calcium-scale inhibitors. Feasibility of scale inhibition experiments was analyzed by molecular dynamics simulation and Gaussian optimization, and the scale inhibition mechanism was theoretically analyzed. Scale inhibition performance was studied by scanning electron microscopy, X-ray diffraction, X-ray photoelectron spectroscopy, static scale inhibition experiments, and electrochemical performance testing, which provided an experimental basis for the molecular dynamics simulation. The experimental results showed that Arg-SA-PASP has better scale inhibition and corrosion inhibition performance than His-SA-PASP. The scale inhibition effect increased with increasing concentration. Electrochemical tests indicated that Arg-SA-PASP is an excellent scale and corrosion inhibitor.     

总变差模型在书画打印宣纸印刷质量预测中的应用

为了建立适用于书画打印宣纸印刷质量的预测模型,本研究测量了14种书画打印宣纸的粗糙度、白度、不透明度、定量、光泽度和针对宣纸特别设定的帘纹深浅以及帘纹疏密度等表面物理参量,并在相同条件下,使用喷墨打印设备输出并测量印品色度值,利用总变差模型构建去除帘纹色差的测定方法,得到与人眼视觉特征相符的色差。运用GRNN广义回归神经网络结合书画打印宣纸表面物理参量与宣纸去帘纹后的色差值,建立预测模型。结果表明,该模型能够在仅测量书画打印宣纸表面物理参量的情况下,便能较为准确地预测书画打印宣纸印刷质量,为书画打印宣纸印刷前的选纸工作提供指导依据。     

定距螺旋桨对船用主机外特性的要求分析

为解决定距螺旋桨与船用主机在船舶运行工况的机桨匹配问题,结合船舶系泊和航行试验的相关标准,分析和归纳船舶运行数据,将实船测试与船机桨匹配理论计算相结合,得出运输船和拖轮在常用工况及特殊工况下定距螺旋桨对主机外特性的定量要求,为配套不同细分市场时船用主机的优化和开发提供参考依据。     

蛋类礼盒包装结构的缓冲性能研究

目的研究蛋类礼盒包装结构的缓冲性能。方法以蛋类尺寸为基础,建立可发性聚乙烯(expandable polyethylene. EPE)缓冲单元结构和组合结构,进行静态仿真分析和实验验证,比较结构在形状、叠合层数、组合形式等参数变化时的载荷与位移。结果结构层数变化相同时,单元结构的极限载荷从143N增加到236 N,组合结构的极限载荷从224 N增加到476 N,均呈近线性增长。结论蛋类礼盒包装中,组合结构的承载能力优于单元结构,通过单元结构的组合,可满足不同蛋类的包装要求。     

F-OFDM仿真系统设计与时频同步算法

针对新一代5G波形的F-OFDM技术开展了研究,通过把一个宽带分为若干个子带,对每个子带进行滤波处理以实现更好的通信效能。基于Simulink平台进行了F-OFDM仿真系统的搭建,重点对F-OFDM符号同步方法和频偏估计方法进行了研究与仿真分析。实验结果表明,基于Chu序列相比采用PN序列可以获得更好的同步效果,基于导频的Classen频偏估计算法相比基于CP的CFO估计算法和基于训练序列的Moose估计方法可以获得更好的频偏估计效果。