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Mamiko Hori Cécile Pagnoux Jean-François Baumard Masayuki Nogami 《Journal of Materials Science》2007,42(1):80-86
A new method is proposed to produce gold nanoparticles (GNP) by in situ reduction of a gold salt dissolved in water. The reducing
agent used is Tiron instead of the citrate anion most often mentioned in literature. The influence of various parameters has
been investigated, such as the content of Tiron with respect to that of the precursor of gold HAuCl4, or the initial pH of the solution after mixing of reactants. It is shown that Tiron also exerts a positive influence as
a dispersant, which impedes agglomeration of gold nanoparticles. The typical average size of GNP synthesized in the present
work is close to 7 nm. 相似文献
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LiFePO4 is a potential candidate for the cathode material of the lithium secondary batteries. A co-precipitation method was adopted to prepare LiFePO4 because it is simple and cheap. Nitrogen gas was needed to prevent oxidation of Fe2+ in the aqueous solution. The co-precipitated precursor shows the high reactivity with the reductive gas, and the single phase of LiFePO4 is successfully synthesized with the aid of carbon under less reductive conditions. LiFePO4 fine powder prepared by co-precipitation method shows high rate capability, impressive specific capacity and cycle property. 相似文献
128.
A practical resource management method that can significantly reduce cochannel interference (CCI) and improve spectrum utilisation in FH-OFDMA packet-based cellular networks is presented. The proposed method seeks an effective combination of dynamic resource allocation with fractional coding and bit loading to respectively minimise CCI and maximise system throughput for a desired performance. 相似文献
129.
M. K. Bakhadyrkhanov O. É. Sattarov Kh. M. Iliev K. S. Ayupov Tuérdi Umaier 《Semiconductors》2005,39(7):789-791
It is experimentally ascertained that light stimulates the negative magnetoresistance observed in a high electric field in silicon doped with boron and manganese. The optimum conditions (the electric field, temperature, illumination, and resistivity of the material) for observation of the largest magnitude of negative magnetoresistance in (Si:B):Mn are determined. The dependence of the negative magnetoresistance on the concentration of compensating impurity is established. 相似文献
130.
The stress intensity factors for a short crack partially penetrating an inclusion of arbitrary shape
Some approximate solutions for predicting the stress intensity factor of a short crack penetrating an inclusion of arbitrary
shape have been developed under mode I and mode II loading conditions. The derivation of the fundamental formula is based
on the transformation toughening theory. The transformation strains in the inclusion are induced by the crack-tip field and
remotely applied stresses, and approximately evaluated by the Eshelby equivalent inclusion theory. As validated by detailed
finite element (FE) analyses, the developed solutions have good accuracy for different inclusion shape and for a wide range
of modulus ratio between inclusion and matrix material. 相似文献