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21.
Summary The synthesis of telechelic monodispersed diols produced from the radical telomerization of an excess of undecylenol with commercialy available , -dithiols HSC2H4XC2H4SH (X=0, S or CH2) initiated by peroxides is presented. In each case, the diols were obtained selectively and quantitatively and they were characterized by both 1H and 13C NMR. Their physical characteristics (Tg, Tm and decomposition temperatures) were determined. Such compounds are thermally more stable than polydispersed telechelic commercially available diols. 相似文献
22.
Styrene-butadiene-styrene (SBS) modified asphalt (SMA) has been widely used in road engineering for decade. However, the phase separation of SMA was obvious during the transport and SBS degraded after aging. To resolve these problems, β-cyclodextrin (β-CD) was used to modify SMA in this work. Conventional properties, storage stability, the effect of short-term aging on the morphology, and rheological property for SMA and β-CD/SMA were investigated. The softening point of modified asphalt reached to the maximum of 66.7°C when 1 wt% β-CD was added to SMA, where the penetration had shown the minimum of 80.8 dmm. In addition, the ductility of β-CD/SMA increased to the maximum of 797 mm when the content of β-CD was increased to 5 wt%. Furthermore, incorporation of β-CD improved the storage stability of SMA. Importantly, the aggregation of SBS was observed in β-CD/SMA, but modifiers distributed uniformly after a short-term aging. The rutting resistance and antiaging performances of SMA were also improved by the addition of β-CD. Considering the comprehensive properties of modified asphalt, the optimum content of β-CD was found to be 2 wt%. 相似文献
23.
随着人民生活水平的提高,人们对电器设备的要求也越来越高,如要求操作更便利、更美观,触摸按键作为人机交互的界面,有向大尺寸、超大尺寸发展的趋势.通过对电容式超大触摸按键的可靠性进行研究,主要包括防静电(ESD)问题、超大触摸按键的群脉冲(EFT)实验和传导抗扰度(CS)实验的抗干扰实验问题,并通过应用案例进行验证,达到了预期效果.研究结果表明:设计的超大按键防静电安装结构,能彻底解决触摸防静电问题;设计的增加抗干扰处理的软件方法,能有解决超大触摸按键在做群脉冲(EFT)实验和传导抗扰度(CS)实验时实验失效的问题. 相似文献
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Rajivgandhi Govindan Nadar Chenthis Kanisha Chelliah Vijayakumar Sekar Alharbi Naiyf S. Kadaikunnan Shine Khaled Jamal M. Alanzi Khalid F. Li Wen-Jun 《Journal of Inorganic and Organometallic Polymers and Materials》2021,31(10):3921-3933
Journal of Inorganic and Organometallic Polymers and Materials - The silver oxide nanoparticle was successfully synthesized using floral waste by simple one pot, cost effective method. The complete... 相似文献
26.
An open-source multi-DOF articulated robotic educational platform for autonomous object manipulation
This research presents an autonomous robotic framework for academic, vocational and training purpose. The platform is centred on a 6 Degree Of Freedom (DOF) serial robotic arm. The kinematic and dynamic models of the robot have been derived to facilitate controller design. An on-board camera to scan the arm workspace permits autonomous applications development. The sensory system consists of position feedback from each joint of the robot and a force sensor mounted at the arm gripper. External devices can be interfaced with the platform through digital and analog I/O ports of the robot controller. To enhance the learning outcome for beginners, higher level commands have been provided. Advanced users can tailor the platform by exploiting the open-source custom-developed hardware and software architectures. The efficacy of the proposed platform has been demonstrated by implementing two experiments; autonomous sorting of objects and controller design. The proposed platform finds its potential to teach technical courses (like Robotics, Control, Electronics, Image-processing and Computer vision) and to implement and validate advanced algorithms for object manipulation and grasping, trajectory generation, path planning, etc. It can also be employed in an industrial environment to test various strategies prior to their execution on actual manipulators. 相似文献
27.
A novel high strength graphitic foam was produced through the incorporation of carbon nanofibers into a pitch based precursor. The nanofiber reinforced cellular foams were mechanically tested both from a localized and bulk perspective with results indicating enhanced foam performance with nanofiber addition. The magnitude of increased performance was a result of both the nanofiber itself as well as its heat treatment as an increase in each was found to cause an associated increase in foam performance. The increase in mechanical capability is attributed to the formation of a zigzag structure in the ligaments and nodes of the foam. This zigzag structure serves as an interlocking mechanism, preventing easy shearing of the graphene layers. The in situ fracture mechanics experiment shows brittle behavior of a single ligament indicating that only reinforced foam behaves like that of a carbon fiber. 相似文献
28.
With various emerging applications ranging from medicine to materials and electronics, the risk of exposure to nanomaterials is rapidly increasing. Several routes of exposure to nanomaterials exist; the most important being dermal contact and inhalation. In this dermal toxicity study, the cellular effects of carbon-based materials with diameters ranging from micro- to nano-dimension were investigated using mouse keratinocytes (HEL-30). The carbon materials tested included carbon fibers (CF; 10 μm diameter), carbon nanofibers (CNF; 100 nm diameter), multi-walled carbon nanotubes (MWCNT; 10 nm diameter), and single-walled carbon nanotubes (SWCNT; 1 nm diameter). CF and CNF did not significantly affect cell viability; however, MWCNT and SWCNT reduced cell viability in a time-dependent manner up to 48 h, with full recovery of mitochondrial function by the 72 h time point. After a 24 h exposure, cells exposed to MWCNT produced up to 3-fold higher increase in reactive oxygen species than those exposed to SWCNT. The results of this study suggest that high-aspect ratio carbon material toxicity is dependent on dimension and composition. 相似文献
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计算机网络技术的出现,全球信息化改变着人们的生活方式,世界各国高度重视发展电子政务,它是一个国家及城市竞争力水平的标志之一.在这样严峻的社会形势下,建立一个高效的电子政务系统是十分必要的.首先,分析了建立电子政务系统的必要性、特点、功能;然后,提出了电子政务系统的体系模型,设计出了功能结构图和网络结构图,详细地描述了方案思路;最后,把此模型应用到商洛市旅游行业中,经过调查数据研究分析,政务系统的出现给旅游业带来巨大的变化,整个城市的经济、影响力大幅度上升. 相似文献