Computational models of a nano probe tip for static behaviors

It is difficult to predict the measurement bias arising from the compliance of the atomic force microscope (AFM) probe. The issue becomes particularly important in this situation where nanometer uncertainties are sought for measurements with dimensional probes composed of flexible carbon nanotubes mounted on AFM cantilevers. We have developed a finite element model for simulating the mechanical behavior of AFM cantilevers with carbon nanotubes attached. Spring constants of both the nanotube and cantilever in two directions are calculated using the finite element method with known Young's moduli of both silicon and multiwall nanotube as input data. Compliance of the nanotube-attached AFM probe tip may be calculated from the set of spring constants. This paper presents static models that together provide a basis to estimate uncertainties in linewidth measurement using nanotubes. In particular, the interaction between a multiwall nanotube tip and a silicon sample is modeled using the Lennard-Jones theory. Snap-in and snap-out of the probe tip in a scanning mode are calculated by integrating the compliance of the probe and the sample-tip interacting force model. Cantilever and probe tip deflections and points of contact are derived for both horizontal scanning of a plateau and vertically scanning of a wall. The finite element method and the Lennard-Jones model provide a means to analyze the interaction of the probe and sample and measurement uncertainty, including actual deflection and the gap between the probe tip and the measured sample surface.     

采用径向射流冲击与钎焊砂轮解决磨削烧伤的研究

在分析高效磨削烧伤机理的基础上，提出了两项对策：一是采用高压径向射流冲击强化磨削弧区换热，以最大限度地疏导已经产生的积聚在弧区的磨削热；二是采用钎焊超硬磨料砂轮取代传统电镀砂轮，以提高砂轮的锋利度降低磨削比能，减少磨削热的产生。缓进给断续磨削试验结果表明，该两项对策对解决难加工材料磨削烧伤问题效果十分明显，具有广阔的应用前景。     

Three-dimensional image correction of tilted samples through coordinate transformation

In scanned probe measurements of micrometer- or nanometer-scale lines, it is nearly impossible to maintain the sample in a perfectly level position, and even a small amount of tilt can contribute to the accuracy of the result of the measure such as linewidth or step height. The current practice in image processing to deal with this problem is to conduct a line-by-line analysis to find the best fit of the substrate profile and subtract this background from all data points, thus describing 3D plane turns as a series of lines and processing them in succession in the x- or y-direction.In this paper a coordinate transformation method is proposed. The new coordinate system can be established on the basis of the inclined angle of the sample as well as the translation of three axes between the old coordinate system and the new coordinate system. The method can mathematically derive and hence correct all tilts around the x-, y- and z-axes and produce a leveled image simultaneously. Feature dimensions such as width, height, sidewall angle and pitch are calculated on the basis of simulated images using the coordinate transformation method and other methods. The result shows the advantage of the proposed method.     

热喷涂焊层车削加工工艺的探讨

本文针对轴类热喷涂焊层中喷涂层、喷焊层的车削加工工艺进行分析 ,从设备调整、刀具牌号选择、刀具几何参数选择三个方面进行研究 ,对加工工艺进行改进 ,在实际生产中具有一定的价值     

3104铝合金的流变应力行为与动态再结晶

对3104铝合金在350-500℃以0．005-0．1s^-1的形变速率进行压缩，真应变为50％，随后立即水冷。采用真应力一真应变曲线和TEM研究其高温压缩变形中的流变应力行为和它的动态再结晶过程。结果表明：3104铝合金为正应变速率敏感材料，具有稳态流变的特征。流变应力随着变形速率的增加而增加，随着变形温度的升高而降低。在低形变温度(350℃)和低形变速率(0．035s^-1)下，该合金发生动态再结晶。     

自制活动镗床拉刀改造

自制活动镗床是加氢公司粗加工关键设备，由于缺少拉刀机构而无法满足机床的正常运行，我通过实际调查计算及设计测绘，恢复了拉刀功能，有利地保证了生产需求。     

纳米加工和材料去除机理研究

针对钠米技术、微型机械在未来工程应用中对纳米级加工的要求,提出将扫描探针显微镜的技术和原理应用于纳米机械加工过程,实现纳米量级加工的可控性和加工结果的可观察性。给出了采用该方法进行纳米切削加工的试验结果,表明这一方法具有稳定、可靠的微加工性能。观察结果显示了材料去除加工的微观过程,被去除材料在刃前发生剪切变形前,与之约成90°的前刀面方向上切屑已充分变形。     

小流量灰浆泵组合密封设计

用于输送含有细小颗粒流体的小流量（0．5～5t／h）氢氧化钙浆液泵的机械密封，极易被溶液中含有的固体颗粒磨损而丧失密封性能。针对这一问题，提出了一种背叶片加上橡胶波纹管机械密封组合的密封结构，并辅之以溢流结构来保护电机，从而解决了灰浆泵的密封问题，延长了泵的使用寿命，使泵装置的体积大大缩小，且易于维修。本文阐述了这种组合密封结构的原理及尺寸设计。     

挤压轮失效分析及热处理工艺改进

挤压轮（H13钢）的早期破坏是影响连续挤压生产成本及效率的重要因素。对挤压轮的破坏方式及原因进行了分析，研究了不同M/B下组织的力学性能，并根据挤压轮内外组织的差异，对挤压轮的热处理工艺进行了改进，使挤压轮的寿命提高了1.5倍。     

国际上LIMS的最新进展与发展趋势

本文介绍了在经济全球化和IT热潮下国际上实验室信息管理系统（LIMS）的最新进展和发展趋势，在仪器联结、仪器控制、光谱采集、光谱处理和化学结构方面的突破，以及生物科学与IT结合诞生出来的新学科－－生物信息学（Bioinformatics）。