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91.
以TDT、TMP、N-220、3010、为主要原料合成聚醚型聚氨酯预聚物,达到塑胶漆的性能要求。本文探讨了不同的合成条件对预聚物的影响。 相似文献
92.
93.
通过细乳液聚合方法制备自交联型有机硅乳液 总被引:3,自引:0,他引:3
苯乙烯与甲基丙烯酸-3-三甲氧基硅丙酯(M PS)经细乳液聚合,制得了稳定的自交联型的水分散涂料,用透射电子显微镜(TEM)、动态光散射仪(DLS)和红外光谱(IR)表征了乳胶粒的形态和结构。发现与传统乳液聚合相比,细乳液聚合法可显著提高乳液的稳定性,且M PS加入量的增加会导致乳液稳定性降低。 相似文献
94.
The electrochemical reduction of nitrate ion was studied by cyclic voltammetry on Pt(1 1 1) and [n(1 1 1) × (1 1 1)] stepped Pt surfaces, where n (=14, 10, 7, 6, 5, 4, 3, 2) is the number of terrace atoms, in 0.1 M HClO4 + 10 mM KNO3. The electrocatalytic nitrate reduction was found to hardly proceed on Pt(1 1 1) in the hydrogen adsorption region, while the electrocatalytic activity was improved with the increase in the step density. Inactivation was observed in the presence of adsorbed hydrogen or nitrate-derived reduced adsorbate, i.e. adsorbed NO, on (1 1 1) step sites. It was, therefore, concluded that the electrocatalytically active NO3− species does not adsorb on the (1 1 1) terraces but on the (1 1 1) monoatomic steps. The nitrate reduction current increased with the step density in a non-linear relationship. The overall current density at 0.21 V (RHE) corresponding to the peak potential of the main electrocatalytic nitrate reduction wave which was maximum at n = 2, abruptly increased with short terraces, i.e. n < 5, where the current wave of adsorbed hydrogen on the Pt stepped surface with comparatively narrow (1 1 1) terraces, denoted as Hnt, also appeared unmodified for n < 5 on voltammograms recorded in 0.1 M HClO4 in the absence of nitrate. 相似文献
95.
Jorge González-Domínguez Osni A. Marques María J. Martín Juan Touriño 《The Journal of supercomputing》2014,70(2):816-829
This paper examines four different strategies, each one with its own data distribution, for implementing the parallel conjugate gradient (CG) method and how they impact communication and overall performance. Firstly, typical 1D and 2D distributions of the matrix involved in CG computations are considered. Then, a new 2D version of the CG method with asymmetric workload, based on leaving some threads idle during part of the computation to reduce communication, is proposed. The four strategies are independent of sparse storage schemes and are implemented using Unified Parallel C (UPC), a Partitioned Global Address Space (PGAS) language. The strategies are evaluated on two different platforms through a set of matrices that exhibit distinct sparse patterns, demonstrating that our asymmetric proposal outperforms the others except for one matrix on one platform. 相似文献
96.
A series of pH‐sensitive and thermosensitive polymer networks were first obtained by copolymerization of telechelic poly(1,3‐dioxolane) (PDXL) with acrylic acid (AA), acrylamide (AM), and N‐isopropylacrylamide (NIPAM), respectively. The copolymerization of PDXL diacrylate (PDXLDA) with AA, AM, or NIPAM is expected to lead to polymer networks in which homopolymeric segments of the monomer are connected by polyacetal segments. As a combination of these two parts, these polymer networks can have some interesting physical properties. For example, the copolymer networks of poly(AA‐b‐DXL) showed pH sensitivity, and both the copolymer networks of poly(AM‐b‐DXL) and poly(NIPAM‐b‐DXL) showed temperature sensitivity. Moreover, because of the low ceiling temperature of polyDXL, the networks containing polyacetal segments (PDXL) can degrade by treatment with a trace of appropriate cationic initiator. The polymer networks prepared were characterized by Fourier transform infrared, differential scanning calorimetry, and swelling data. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 3002–3006, 2002; DOI 10.1002/app.2329 相似文献
97.
This paper addresses the problem of designing controllers that are robust to a great uncertainty in a time constant of the plant. Plants must be represented by minimum phase rational transfer functions of an arbitrary order. The design specifications are: (1) a phase margin for the nominal plant, (2) a gain crossover frequency for the nominal plant, (3) zero steady state error to step commands, and (4) a constant phase margin for all the possible values of the time constant (T): 0<T<∞. We propose a theorem that defines the structure of the set of controllers that fulfil these specifications and show that it is necessary for these robust controllers to include a fractional-order PI term. Examples are developed for both stable and unstable plants, and the results are compared with a standard PI controller and a robust controller designed using the QFT methodology. 相似文献
98.
Effect of the nature and structure of pillared clays in the catalytic behaviour of supported manganese oxide 总被引:3,自引:0,他引:3
In the present work, the complete oxidation of acetone has been studied over a series of supported manganese oxide catalysts on the unpillared and the Al- and Zr-pillared forms of two natural clays, a montmorillonite and a saponite. A significant influence of the clay supports characteristics on the catalytic performance has been found. The following order of improving catalytic performance is established with respect to the pillars composition: Al-pillared clays < unpillared clays < Zr-pillared clays. 相似文献
99.
Kenton O’Hara Gerardo Gonzalez Graeme Penney Abigail Sellen Robert Corish Helena Mentis Andreas Varnavas Antonio Criminisi Mark Rouncefield Neville Dastur Tom Carrell 《Computer Supported Cooperative Work (CSCW)》2014,23(3):299-337
While surgical practices are increasingly reliant on a range of digital imaging technologies, the ability for clinicians to interact and manipulate these digital representations in the operating theatre using traditional touch based interaction devices is constrained by the need to maintain sterility. To overcome these concerns with sterility, a number of researchers are have been developing ways of enabling interaction in the operating theatre using touchless interaction techniques such as gesture and voice to allow clinicians control of the systems. While there have been important technical strides in the area, there has been little in the way of understanding the use of these touchless systems in practice. With this in mind we present a touchless system developed for use during vascular surgery. We deployed the system in the endovascular suite of a large hospital for use in the context of real procedures. We present findings from a study of the system in use focusing on how, with touchless interaction, the visual resources were embedded and made meaningful in the collaborative practices of surgery. In particular we discuss the importance of direct and dynamic control of the images by the clinicians in the context of talk and in the context of other artefact use as well as the work performed by members of the clinical team to make themselves sensable by the system. We discuss the broader implications of these findings for how we think about the design, evaluation and use of these systems. 相似文献
100.
硅酸镓镧结构的新型压电晶体的研究进展 总被引:7,自引:0,他引:7
新型压电晶体La3Ga5SiO14因其低声速、零温度切向和良好的高温稳定性受到关注,但是昂贵的Ga2O3原料阻碍了它的工业应用。通过离子置换可获得具有langasite结构的多种新型压电晶体。综述介绍了置换La,Ga,Si形成的新型压电晶体的最新研究进展,比较分析了不同晶体的优势及其存在的问题。在这些新晶体中,由于Sr3Ga2Ge4O14(SGG)具有熔点较低、性能较高的综合优势,它有可能成为新一代表面波器件的重要候选材料。与提拉法相比,采用增蜗密封的下降法生长SGG单晶;可以显著提高晶体产率,降低成本。 相似文献