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991.
Investigations on white spirit and acetone permeation resistance of modified polyamide and nylon 6 clay (MPANYC) blends and their corresponding polyethylene/MPANYC bottles were reported in this study. The white spirit and acetone permeation resistance of MPANYC sheets improve consistently with increasing NYC contents present in MPANYC resins after blending nylon 6 clay (NYC) in modified polyamide (MPA) resins. However, the order of barrier improvement of the PE/MPANYC and PE/NYC bottle specimens is not corresponding to the order of barrier improvement of the MPANYC and/or NYC barrier resins added in PE. The blow-molded PE/NYC bottle specimen exhibits similarly worse white spirit and acetone solvent permeation resistance as the PE bottle specimen, wherein no clearly formed NYC laminas but only dispersed NYC droplets or agglomerates were found on the fracture surfaces of the PE/NYC bottles. However, after blending optimum compositions of MPANYC in PE, the PE/MPANYC bottles with demarcated MPANYC laminas exhibit significantly better white spirit and acetone permeation resistance than the PE/MPA bottle, wherein the white spirit and acetone permeation rates of the PE/MPA8NYC1 bottle are about 1.3 and 1.4 times slower than those of the PE/MPA bottle, respectively. In order to understand these interesting barrier properties of PE/MPANYC and PE/NYC bottles, rheological, thermal, wide angle X-ray diffraction and morphological properties of the base MPANYC and NYC resins and their corresponding morphology present in the blow-molded bottles were investigated. 相似文献
992.
The partial oxidation of methane to synthesis gas was studied at atmospheric pressure and in the temperature range of 550–800°C over -Al2O3-supported bimetallic Pt–Co, and monometallic Pt and Co catalysts, respectively. Both methane conversion and CO selectivity over a bimetallic Pt0.5Co1 catalyst were higher than those over monometallic Pt0.5 and Co1 catalysts. Furthermore, the addition of platinum in Pt–Co bimetallic catalysts effectively improved their resistance to carbon deposition with no coking occurring on Pt0.5Co1 during 80 h reaction. The FTIR study of CO adsorption observed only linearly bonded CO on bimetallic Pt–Co catalysts. TPR and XPS showed enhanced formation of a cobalt surface phase (CSP) in bimetallic Pt–Co catalysts. The origins of the good coking resistivity of bimetallic Pt–Co catalysts were discussed. 相似文献
993.
为了实现滇池流域截污效果的最大化,基于前期建立的东岸排水管网SWMM模型,结合该区域1995-2016年间降雨资料,研究环湖截污干渠的错峰调蓄技术。根据雨水干渠液位高度执行不同控制模式:当水位低于6.76 m时执行典型污染物浓度阈值控制模式;当水位高于6.76 m时执行典型污染物阈值控制的同时执行液位-污染物通量控制模式。采用SS和TN作为干渠截流的典型污染物控制指标,其控制浓度阈值分别取12和5 mg/L。模拟重现期为0.5~1 a降雨时SS、TN浓度-负荷通量调蓄方案下干渠负荷收集情况,结果表明两种调蓄方案均能有效提高雨水干渠的负荷收集率,提高污水干渠出口浓度,降低雨水径流对污水厂的高水量和低浓度冲击负荷。随着重现期增大,干渠对污染物的高效和最大化收集效果越明显。但是TN调控下污染负荷收集效果优于SS,因此选择TN作为干渠截流的最优典型污染物控制指标。 相似文献
994.
995.
A kind of novel superabsorbent hydrogel with high swelling ratio property that could be used for the development of water absorbing resin, soil water retention agent, and chemical sand‐fixing material was synthesized in this study. The hydrogels were prepared by the crosslinking reaction of polysuccinimide (PSI). The relationships between swelling ratio and volume of solvent as well as the concentration of crosslinking agent were investigated in detail. Several composites, such as starch, carrageenan, and polyacrylamide, were added into hydrogels to enhance the swelling ratio. It was found that the swelling ratio was significantly increased, which the maximum water absorbency was enhanced 2.46 times when the composite polyacrylamide (PAM) was added compared to the control. The effects of ionic strength and sensitivity of pH on hydrogels were also studied. The modified hydrogels products with swelling ratio less sensitivity to the salinity as well as relative high swelling ration in salinity system were also obtained by adding PAM. Through the Fourier transform infrared spectroscopy (FTIR) characterizations, the crosslinking reaction mechanism and the structure of composite were proposed. In addition, the transmission electron microscopy (TEM) examinations showed that some composite materials elevated the physical crosslinked and connected channels density substantially. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 550–557, 2006 相似文献
996.
The application of supercritical fluid chromatography (SFC) coupled with a UV variable-wavelength detector to isolate the
minor components (carotenes, vitamin E, sterols, and squalene) in crude palm oil (CPO) and the residual oil from palm-pressed
fiber is reported. SFC is a good technique for the isolation and analysis of these compounds from the sources mentioned. The
carotenes, vitamin E, sterols, and squalene were isolated in less than 20 min. The individual vitamin E isomers present in
palm oil were also isolated into their respective components, α-tocopherol, α-tocotrienol, γ-tocopherol, γ-tocotrienol, and
δ-tocotrienol. Calibration of all the minor components of palm as well as the individual components of palm vitamin E was
carried out and was found to be comparable to those analyzed by other established analytical methods. 相似文献
997.
Maria?Antonietta BresciaEmail author Vincenzo?Mazzilli Angela?Sgaramella Stefano?Ghelli Francesco?Paolo Fanizzi Antonio?Sacco 《Journal of the American Oil Chemists' Society》2004,81(5):431-436
Characterization of the lipid fraction of raw cow and buffalo milk samples, collected in different breeding areas in Apulia,
a region of southern Italy, were performed by means of 1H NMR. The aim of this work was to establish whether FA composition data obtained by 1H NMR can be used in the differentiation of buffalo and cow milk samples according to species. A complete assignment of the
signals present in the spectrum was attempted by COSY, heteronuclear coherence spectra. Quantification of FA was carried out
by inserting the integrals of particular peaks in suitable calculations. Multivariate statistical analysis, conducted on the
results of the quantification, permitted buffalo and cow milks to be distinguished. 相似文献
998.
Dalibor Petković Shahaboddin Shamshirband Hadi Saboohi Tan Fong Ang Nor Badrul Anuar Nenad D. Pavlović 《Applied Intelligence》2014,41(3):887-896
The prerequisite for new versatile grippers is the capability to locate and perceive protests in their surroundings. It is realized that automated controllers are profoundly nonlinear frameworks, and a faultless numerical model is hard to get, in this way making it troublesome to control utilizing tried and true procedure. Here, a design of an adaptive compliant gripper is presented. This design of the gripper has embedded sensors as part of its structure. The use of embedded sensors in a robot gripper gives the control system the ability to control input displacement of the gripper and to recognize specific shapes of the grasping objects. Since the conventional control strategy is a very challenging task, soft computing based controllers are considered as potential candidates for such an application. In this study, the polynomial and radial basis function (RBF) are applied as the kernel function of Support Vector Regression (SVR) to estimate and predict optimal inputs displacement of the gripper according to experimental tests and shapes of grasping objects. Instead of minimizing the observed training error, SVR poly and SVR rbf attempt to minimize the generalization error bound so as to achieve generalized performance. The experimental results show that an improvement in predictive accuracy and capability of generalization can be achieved by the SVR approach compared to other soft computing methodology. 相似文献
999.
Todd?L.?KurthEmail author Girma?Biresaw Atanu?Adhvaryu 《Journal of the American Oil Chemists' Society》2005,82(4):293-299
The frictional behaviors of methyl oleate (MO), methyl palmitate (MP), methyl laurate (ML), and methyl stearate (MSt) as additives
in hexadecane have been examined in a boundary lubrication test regime using steel contacts. It was found that the transient
attributes of coefficient of friction (COF)-time spectra are a sensitive measure of adsorption equilibria. Critical additive
concentrations were defined and used to perform novel and simple Langmuir analyses that provide an order of adsoprtion energies:
MSt>MP>MO≥ML. Application of Langmuir, Temkin, and Frumkin-Fowler-Guggenheim adsorption models via nonlinear fitting of a general cooperative model demonstrates the necessary inclusion of cooperative effects in the applied
model. In agreement with the qualitative features of steady-state COF-concentration plots, MSt modeling requires minimal cooperative
interaction terms. However, MO, MP, and ML data require large attractive interaction terms to be adequately fitted. Primary
adsorption energies calculated via the cooperative model are necessarily decreased, whereas total adsorption energies correlate well with values obtained via critical concentration analyses. These results and comparisons with previous adsorption studies of MO and MSt suggest that
primary (ester-surface) and secondary (alkyl-surface) adsorbate-adsorbent, adsorbate-adsorbare, and (free-additive) adsorpt-adsorpt
interactions collectively determine both the calculated primary and the cooperative interaction energies. 相似文献
1000.
Engineers of the concrete technology are increasingly concerned with the material passing through a sieve of the size under 0.149 mm. Materials called very fine aggregate or mineral filler may affect the performance of concrete in an either positive or a negative way. Discussions on aggregate containing very fine material are vitally important. Washing the aggregate residue has been the sole way to solve this matter to date. This is mainly based on the debatable opinion that materials of this kind are regarded as clay material. The goal of the study was to determine how the content of mineral filler might affect properties of concrete. Two types of aggregates with different amounts of cement and mineral filler were used. Basically, mineral filler replaced sand. The effect of applying different amounts of mineral filler on concrete was then determined. The addition of 7-10% of mineral filler to fine aggregate (0-2 mm) was found to considerably improve the properties of concrete. 相似文献