Physical solvent extraction of levulinic acid from dilute aqueous solution with 2-methyltetrahydrofuran

The results of the present investigation reveal that 2-methyltetrahydrofuran is a potential solvent for the extraction of levulinic acid from dilute aqueous solution. This conclusion is based on the relatively high values of distribution coefficient K_d (1.3-1.6) measured for the system of levulinic acid – water – 2-methyltetrahydrofuran at temperatures 298.2 K, 313.2 K, and 328.2 K, as well as encouraging performance of the continuous counter current Kühni column. The results give reason to believe, that 2-methyltetrahydrofuran can be considered for the extraction of other low molecular weight acids, such as formic or lactic acid, as well.     

Real-time effective density monitor (DENSMO) for aerosol nanoparticle production

A new instrument, density monitor (DENSMO), for aerosol particle size distribution characterization and monitoring has been developed. DENSMO is operationally simple and capable of measuring the effective density as well as the aerodynamic and the mobility median diameters with a time resolution of 1 s, from unimodal particle size distributions. The characterization is performed with a zeroth order mobility analyzer in series with a low pressure impactor and a filter stage. The operation of DENSMO was investigated with sensitivity analysis and, based on the results, optimal operation parameters were determined. DENSMO was also compared, in lab test measurements, against a reference method with several particle materials with bulk densities from 0.92 to 10.5 g/cm³. The results show that the deviation from the reference method was less than 25% for suitable materials.

Copyright © 2016 American Association for Aerosol Research     

A micropower analog-digital heart rate detector chip

A micropower detector chip integrated with CMOS technology has been developed for a hand-held heart rate monitoring instrument mainly used by professional athletes and others who exercise seriously to increase their endurance and overall performance. The chip uses linear bandpass filtering and threshold detection and is implemented with analog switched-capacitor (SC) and digital techniques. The bandpass filter transfer function is derived from the spectral contents of noisy ECG signals. The layout was designed in full custom style in order to minimize the silicon area. The chip achieves a detection rate of 90% with a simulated ECG signal corrupted with Gaussian noise (signal-to-noise ratio = 5) in the heart rate range 60-200 1/min with a total current consumption of less than 30µA from a 3-V supply. The detection rate is 96.9% for a noisy signal obtained from the MIT-BIH arrhythmia database.     

On-chip offset generator for accurate integral non-linearity testing of A/D converters and D/A-A/D converter pairs

It has recently shown how a constant dc offset between two low-quality test signals can be used to test the integral nonlinearity (INL) of A/D converters (ADCs) without an accurate test stimulus, and how the same method can be used to test the INL of D/A converters (DACs) as well. We propose here an on-chip offset generator for producing the constant offset and analyse its limitations. Experimental tests on the 122 × 22 μm² offset generator fabricated in 130 nm CMOS process show that it can be used to test the INL of 12-b DACs and ADCs. The generator is rail-to-rail capable so that almost the whole input/output range of converters can be tested. Moreover, if the proposed offset generator is used in a ratiometric test setup as proposed here as well, the influence of a reference voltage drift on measurement accuracy is cancelled out. Because of its small size, simple design, rail-to-rail capability and immunity to reference voltage changes, the proposed offset generator is well suited for built-in self-test usage.     

EOC: Electronic Building Blocks for Embedded Systems

The embedded-object concept, EOC, applies common object-oriented software methods to Lego-like hardware-software entities. These modular entities, representing objects in object-oriented design, function as electronic building blocks that can be assembled into new embedded systems. The goal of the EOC is to make embedded-system design faster and easier while preserving the commercial applicability of the resulting devices.