Losses of volatile compounds during fermentation

The ability of fermentative CO₂ to blow off the volatile compounds that are synthesized during fermentation has been studied. Model solutions simulating a fermenting must were purged at different CO₂ flow rates and temperatures, and the amount of volatile compounds blown off by the stream of CO₂ was recorded by high-resolution gas chromatography. Data showed that under normal fermenting conditions, fatty acid ethyl esters and some fusel alcohol acetates are blown off the solution at a high rate. The maximum loss rate was observed for ethyl decanoate. The purging speed is doubled when temperature increases from 17 °C to 27 °C. Losses can be interpreted by a linear model and are a function of the compound and the flow rate of CO₂. These models allow us to reconstruct the volatile synthesis vs time functions through graphic calculus and to estimate the proportion of volatile material retained, hydrolysed and purged. Synthesis takes place during the tumultuous period of fermentation together with CO₂ production that blows off the volatile material. Hydrolysis takes place in the last stages of fermentation. In a 10-1 open fermenter, up to 80% of volatile material can be blown off while an average of 10% is retained. Residual esterase activity accounts for about 20% of the total amount of ester synthesized.     

Improving process models by mining mappings of low-level events to high-level activities

While it is possible to analyze the run-time behavior of a business process through process mining techniques, in practice there is often a gap between the low-level nature of the events recorded in an event log and the high-level of abstraction at which the process is modeled. This makes it difficult to understand the recorded behavior in terms of the high-level activities in the process model. Also, it makes it difficult to improve the model based on run-time data about the process. In this work we present an approach to mine mappings between the events in the log and the activities in the model. These mappings can be used to generate suggestions of how the process model can be extended in order to capture the behavior recorded in the event log. Using a real-world and publicly available event log, we show how the approach can improve the model in a stepwise manner, until it covers all the behavior recorded in the event log.     

Development of ceramic floor tile compositions based on quartzite and granite sludges

In the present work, industrial sludges derived from cutting and polishing natural stones (granite and quartzite) were characterised in terms of particles size distribution, chemical and mineralogical composition, and thermal behaviour and their potential to be incorporated as main components in red-clay-based stoneware tiles was evaluated. High levels (60–70 wt.%) of incorporation were attempted aiming at designing new formulations intended to be less expensive and possess better final properties (lower water absorption and higher flexural strength) in comparison to an industrial reference body used in the production of rustic tiles by extrusion, characterised 8–9% water absorption and a flexural strength of 17–18 MPa. Extruded rods of different formulations were produced and fired at 1100 °C, 1125 °C, 1150 °C and 1200 °C. The experimental results showed that all the new formulations performed better with the most significant improvements being obtained with incorporation of granite sludge. Flexural strength values more than triplicate and water absorption decreased by more than one order of magnitude in comparison to the reference paste. The new products fulfil the requirements of the ISO 13006 standard, group BIa (porcelain tiles).     

Evolutionary robustness analysis for multi-objective optimization: benchmark problems

This paper presents a new approach to robustness analysis in multi-objective optimization problems aimed at obtaining the most robust Pareto front solutions and distributing the solutions along the most robust regions of the optimal Pareto set. A new set of test problems accounting for the different types of robustness cases is presented in this study. Non-dominated solutions are classified according to their degree of robustness and are distributed along the Pareto front according to specific algorithm parameter values. Verification of the proposed method is carried out using the developed test problems and artificial and real world benchmark test problems present in the literature.     

Obtaining condensed milk from a mixture of hydrosoluble extract of soybean powder and cow's milk]

Three formulations of mix concentrated milk with hydrosolubles extract of soybean powder and cow's milk were prepared. The products were condensed up to 31% and 33.65% of solids in a vacuum evaporator at temperature of 45 degrees and 58 degrees C with a vacuum pressure of 540 mmHg. The products obtained were compared with standard concentrated milk through sensory evaluation showing satisfactory characteristics.     

Boundary scan test,test methodology,and fault modeling

The test technique called boundary scan test (BST) offers new opportunities in testing but confronts users with new problems too. The implementation of BST in a chip has become an IEEE standard and users on board level are the next group to begin thinking about using the new possibilities. This article addresses some of the questions about changes in board-level testing and fault diagnosis. The fault model itself is also affected by using BST. Trivial items are extended with more sophisticated details in order to complete the fault model. Finally, BST appears to be a test technique that offers a high degree of detectability on board level, but for diagnosis, some additional effort has to be made.     

The corrosion of mild steel in simulated SO2 containing atmospheres

Electrochemical tests were carried out on steel/steel multi-laminar cells under thin layers of sulphate solution simulating atmospheres with contents of 20, 50 and 75 μg m⁻³ of SO₂ and a relative humidity of 85%. Measurements of the current flowing between the two electrodes of the cell vs drying time and impedance measurements for different times were taken. Potentiodynamic cathodic polarization plots were also obtained for one concentration of contaminant at various drying times using three electrode multi-laminar cells. The results showed that the multi-laminar cells allowed the drying process of the thin electrolyte films to be followed. The use of electrochemical techniques gave information on the kinetics and mechanism of the corrosion process occurring during the drying period. Initially the process is controlled by oxygen diffusion through the liquid film, but for longer periods the control changes to the anodic reaction.     

Characterizing peers communities and dynamics in a P2P live streaming system

Despite the large number of works devoted to understand P2P live streaming applications, most of them put forth so far rely on characterizing the static view of these systems. In this work, we characterize the SopCast, one of the most important P2P live streaming applications. We focus on its dynamics behavior as well as on the community formation phenomena. Our results show that SopCast presents a low overlay topology diameter and low end-to-end shortest path. In fact, diameter is smaller than 6 hops in almost 90 % of the observation time. More than 96 % of peers’ end-to-end connections present only 3 hops. These values combined may lead to low latencies and a fast streaming diffusion. Second, we show that communities in SopCast are well defined by the streaming data exchange process. Moreover, the SopCast protocol does not group peers according to their Autonomous System. In fact, the probability that a community contains 50 % of its members belonging to the same AS (when we observe the largest AS of our experiments) is lower then 10 %. Peers exchange more data with partners belonging to the same community instead of peers inside the same AS. For the largest AS we have, less than 18 % of peer traffic has been exchanged with another AS partners. Finally, our analysis provides important information to support the future design of more efficient P2P live streaming systems and new protocols that exploit communities’ relationships.