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11.
The deactivation characteristics of Pd/SiO2 in the selective hydrogenation of acetylene were correlated with changes in the amount of the C4 species produced. The amounts of butenes produced changed in parallel with the catalyst activity, indicating that the rate limiting step for butene production was the same as that for acetylene hydrogenation. On the other hand, the amount of 1,3-butadiene produced changed, showing a maximum with catalyst deactivation because 1,3-butadiene is an intermediate in the sequential reaction process which involves both the production and consumption of 1,3-butadiene. This was verified by a simultaneous TG/reaction experiment showing that 1,3-butadiene was a precursor of green oil. The catalyst showed a self-regenerative behavior in its activity and the amounts of C4 species produced during the early stage of deactivation because two opposite factors, which contributed to either the lowering or the promotion of activity, were involved in the process. A specific type of polymer species, produced during the initial period of deactivation, is proposed to be responsible for the promotion of catalyst activity. 相似文献
12.
For multi-step heterogeneous consecutive reactions affected entirely by interphase diffusion under isothermal condition, the
equations for the effectiveness factors, the surface concentrations and the point yields were derived in terms of the Damkoehler
numbers or the measurables from the mass balances set up on the assumption that the mass-transfer rate balances the surface-reaction
rate at steady state.
From the analyses of the equations derived, the effectiveness factors for the intermediate steps and the surface concentrations
of intermediates were understood to be enhanced by the measurables inclusive of the concentrations and the mass-transfer coefficients.
Then the effect of the concentrations was concluded to be most significant. The effects of these measurables to the effectiveness
factors and the surface concentrations were qualitatively discussed for simple consecutive reactions and also for additive
consecutive reactions. Especially, as for two-step additive consecutive reactions, the effects of measurables η Da and the
concentrations to the effectiveness factors were examined with graphical presentations.
Finally, the brief discussion of the dependency of the Damkoehler number upon reaction time and the effect of the Renolds
number and diffusivity to the extent of the mass-transfer resistance were presented. 相似文献
13.
14.
Dongho Chae O. Yu. Imanuvilov Sang Moon Kim 《Journal of Dynamical and Control Systems》1996,2(4):449-483
This paper studies the problem of exact boundary controllability of second-order semilinear parabolic equations when the control is under Neumann's boundary conditions. For a nonlinear term with a sublinear growth we prove the global null-controllability and for the superlinear growth case we prove the local exact controllability of the equations. 相似文献
15.
Thirteen scenarios were used to measure and compare the perceptions of elder abuse and help-seeking behaviors of African-American, Caucasian American, and Korean-American elderly women. Significant group differences existed in their perceptions of elder abuse with regard to six scenarios, and the Korean-American women were substantially less likely to perceive a given situation as abusive than the other groups. The three groups also showed significant differences in their intended use of formal and informal sources of help in the case of elder abuse. 相似文献
16.
17.
Core–shell type nanoparticles of poly(L ‐lactide)/poly(ethylene glycol) (LE) diblock copolymer were prepared by a dialysis technique. Their size was confirmed as 40–70 nm using photon correlation spectroscopy. The 1H‐NMR analysis confirmed the formation of core–shell type nanoparticles and drug loading. The particle size, drug loading, and drug release rate of the LE nanoparticles were slightly changed by the initial solvents that were used. The drug release behavior of LE core–shell type nanoparticles showed an initial burst during the first 12 h and then a sustained release until 100 h. The degradation behavior of LE block copolymer nanoparticles was divided into three phases: the initial rapid degradation phase, the stationary phase, and the rapid degradation phase until complete degradation. It was suggested that lidocaine release kinetics were predominantly governed by the diffusion mechanism in the initial burst phase and after that by both of the diffusion and degradation mechanisms. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 85: 2625–2634, 2002 相似文献
18.
V. P. Il’ina 《Glass and Ceramics》2007,64(9-10):318-321
Facing and decorative glass crystal materials were developed from mineral feedstock and technogenic wastes. The effect of the components present in the mineral feedstock in liquation and crystallization of the glasses was investigated. The materials obtained can be used in construction for facing walls. 相似文献
19.
A new method to predict the critical heat flux (CHF) is proposed, based on the fuzzy clustering and artificial neural network. The fuzzy clustering classifies the experimental CHF data into a few data clusters (data groups) according to the data characteristics. After classification of the experimental data, the characteristics of the resulting clusters are discussed with emphasis on the distribution of the experimental conditions and physical mechanism. The CHF data in each group are trained in an artificial neural network to predict the CHF. The artificial neural network adjusts the weight so as to minimize the prediction error within the corresponding cluster. Application of the proposed method to the KAIST CHF data bank shows good prediction capability of the CHF, better than other existing methods. 相似文献
20.
This paper deals with the pricing and investment decision problem of multi-modal transportation systems in which the congestion
is a significant factor in the assessment of system costs. This study approaches this congestion pricing problem with a number
of social welfare maximization problems, all of which have the identical structure except financial constraints. One welfare
maximization problem examined in this study yields the pricing and investment decision, which can attain the first-best social
optimality for multi-modal transportation systems. Other welfare maximization problems show he second-best optimal solutions
that can address two policy questions in transportation economics, namely, the cross-subsidy between competing modes and peak-period
congestion charges on a single highway link.
Received: February 2001/Accepted: December 2001
This work was supported in part by funds from BK21 Research Division of Seoul National University for Social Infrastructure
and Construction Technology. 相似文献