N-甲基乙酰氧基乙酰苯胺的液谱分析

本文研究了高效液相色谱测定N－甲基乙酰氧基乙酰苯胺的方法。采用Hypersil C18柱，以甲醇：水＝60：40（V／V）为流动相。该方法的变异系数为0．43％，回收率为98．9％－100．6％。     

A multipurpose audio aggregation watermarking based on multistage vector quantization

Watermarking technology can achieve multipurpose such as copyright protection, copy protection, and integrity authentication. We propose a novel watermarking approach which involves robust watermark and fragile watermark in a two-stage quantization technique. Traditional watermarking algorithms mostly have poor performance in imperceptibility as the codeword selected from the modified codebook is not optimal. In our method, we select the codeword in the original codebook to ensure optimality. Furthermore, we use Huffman encoding to pick up property which is sensitive to many attacks in the entire aggregation. For copyright protection, the proposed scheme can resist attacks such as lossy compression, noise addition, and normalization. As for content authentication, the proposed scheme is sensitive to various attacks provided by Stirmark Benchmark for Audio. Experimental results show that the proposed method can be used respectively for protecting the copyright and authenticating the integrity of the audio aggregation.     

利用α-甲基苯乙烯合成佳乐麝香的研究

介绍一种新的佳乐麝香合成方法，并就反应的参数对反应过程的影响进行了探讨。     

Algebraic operations in fuzzy object-oriented databases

The fuzzy object-oriented databases have been proposed to meet the need of dealing with fuzzy as well as complex objects. In this paper, we present a formal fuzzy object-oriented database model. Based on the semantic measure of fuzzy data, we first identify two kinds of fuzzy object redundancies, which are inclusion redundancy and equivalence redundancy, and then define three kinds of merging operation for redundancy removal. On the basis, we define some fuzzy algebraic operations for fuzzy classes and fuzzy objects. Finally, in the paper, we discuss fuzzy querying strategies and give the form of SQL-like fuzzy querying for the fuzzy object-oriented databases.     

LLDPE在振动剪切复合场中挤出成型的流变行为

利用振动剪切挤出装置研究了线性低密度聚乙烯(LLDPE)在振动与旋转剪切复合力场中挤出成型时的流变行为。结果表明:LLDPE熔体在复合力场中的表观黏度受振动频率、振幅、剪切速率等影响很大。在复合力场中存在使黏度降低最大的振动频率和剪切速率的最佳搭配。     

水热法制备锰锌铁氧体纳米晶

以水热法制备了粒径为20－40nm的锰锌铁氧体纳米晶，以XRD、SEM、磁强计等对产物做了表征，分析了影响锰锌铁氧体纳米晶的因素。结果表明，在T≥150℃,t≥5h条件下，均能得到阵锌铁氧体纳米晶粉末。T＝450℃时制备的纳米晶的磁强度最高；添加剂能改善水热体系的均匀性，使产物分布均匀、晶相单一、团聚少。     

Ionomer-silica hybrids via sol-gel reaction

Ionomer-silica hybrid materials were made from polyethylene-co-acrylic acid neutralized by a zinc salt (PI) and tetraethoxy silane (TEOS) via the sol-gel reaction. The effects of various experimental parameters such as solvents, H₂O/Si ratio and the amount of TEOS in the ionomer solution on the hybrid structure and properties were examined. The spectroscopic results show that solvents do not affect the structure of the hybrids, but influence the thermal properties. The hybrids made using highly polar solvent exhibit better thermal stability and dynamic mechanical properties at high TEOS contents. The amount of water used for hydrolysis and subsequent condensation play a significant role in the network formation. The varying amount of TEOS in solutions gives rise to different silica content of the hybrid. Above 50 wt%, the sample becomes opaque due to silica aggregation. The high ratio of H₂O/Si leads to phase separation during the reaction. Transparent hybrid materials can only be obtained when the ratio of H₂O/Si is below 5.     

电力工程自动化系统故障分析的方法

由于电力工程自动化系统的操作程序不断复杂化,故障的出现频率也随之增加。因此,必须建立完善的故障分析和解决方案,方能保证电力工程的正常、顺利推进。在此基础上,就电力工程自动化系统故障分析方法进行分析、探讨。     

税收电子数据分析在煤炭企业税源管理工作中的研究与实践

随着信息技术的不断发展,利用先进技术成果挖掘和提炼税收电子数据信息,深化数据分析,为税源管理特别是重点税源管理工作服务,已经成为了现代税收发展的潮流。它是信息管税、风险控制的重要组成部分,也是各级税务机关、专家和学者在税源管理方面面临的重要课题之一。以朔州市国家税务局煤炭企业税收管理信息系统建设为背景,研究税收数据分析在税源管理工作中作用和意义。     

浅析手冢治虫对当今日本动漫创作的影响

手冢治虫的动漫作品对当时乃至现在都具有很深借鉴意义。手冢治虫在动画和漫画领域上创作的内容丰富,情节连续生动。文章通过解读他的作品灵感来源和有限动画的创举,从而进一步对比分析对后代动画工作者的深远影响。