土钉加锚杆联合支护基坑的失稳分析及处理

根据具体工程实例,介绍了在基坑开挖时采用土钉加锚杆的联合支护方式后在施工过程中出现坍塌裂缝的现象,针对这一现象,分析了施工条件与环境,得出了事故发生的原因,并结合实际情况提出了处理措施.     

厦门市气源转换的技术分析

分析了气源转换时原有输配系统的管道、调压设备、计量设备、用气设备与天然气系统相适应的问题，提出了相应的措施。     

Fivefold symmetry in real and reciprocal spaces

Tetrahedrally close-packed structures with juxtaposed pentagonal antiprisms, such as the μ, C14 Laves and the newly found C phases, were studied by means of HREM and SAD. It was found that each bright spot in the structural image corresponds to an antiprism. Differently oriented domains of these phases intergrow frequently with a fairly good match at the interphase boundary. All diffraction patterns of these phases show a fivefold distribution of spot-pairs, and it is shown that this fivefold symmetry comes from the pentagons and spot-pairs from two pentagonal prisms superposed in antisymmetrical positions.     

鄱阳湖湖底沉积物放射性水平

本文报道了1985年鄱阳湖湖底沉积物放射性水平的调查结果。沉积物中 U、Th、~(226)Ra、~(40)(?)和~(137)Cs 的比活度分别为64.8、67.9,58.9、676.1和3.5Bq/kg;用~(137)Cs 测龄方法作了沉积物泥芯垂直深度的年代定位,由此得知1985—1958年对应深度沉积物中 U、Th、~(226)Ra 和~(40)K 的比活度与1957—1930年对应深度沉积物比较无显著性差异;U、Th 和~(226)Ra 的浓集因予分别为5.2×10~413.9×10~4和4.8×10~4L/kg。     

Feature Reduction via Generalized Uncorrelated Linear Discriminant Analysis

High-dimensional data appear in many applications of data mining, machine learning, and bioinformatics. Feature reduction is commonly applied as a preprocessing step to overcome the curse of dimensionality. Uncorrelated Linear Discriminant Analysis (ULDA) was recently proposed for feature reduction. The extracted features via ULDA were shown to be statistically uncorrelated, which is desirable for many applications. In this paper, an algorithm called ULDA/QR is proposed to simplify the previous implementation of ULDA. Then, the ULDA/GSVD algorithm is proposed, based on a novel optimization criterion, to address the singularity problem which occurs in undersampled problems, where the data dimension is larger than the sample size. The criterion used is the regularized version of the one in ULDA/QR. Surprisingly, our theoretical result shows that the solution to ULDA/GSVD is independent of the value of the regularization parameter. Experimental results on various types of data sets are reported to show the effectiveness of the proposed algorithm and to compare it with other commonly used feature reduction algorithms.     

Microstructure investigations of ball milled materials

HREM and FEG TEM were emphasized and extensively used to follow the most subtle changes in the structure and composition of ball-milled Cu, Fe-Cu, and thermally decomposed Fe60Cu40. Some significant results are obtained and summarized as follows: HREM shows that the deformation of ball-milled copper proceeds mainly by twinning and shear bands (SBs) formation. The nano-grains formed during ball milling (BM) contain a high density of dislocations. The grain boundaries (GBs) of nanocrystalline (NC) Cu prepared by BM are ordered, curved, and strained, but disordering, lattice distortion, and nanovoids in local regions were frequently observed. Nanoscale composition analysis on mechanically alloyed Fe16Cu84 shows that the average Fe content in both the interior of grains and the GBs is close to the designed composition, which proves that a supersaturated solid solution has really formed. However, the Fe content is rather inhomogeneous between the larger and smaller grains, which infers the inhomogeneous mixing of Fe and Cu during mechanical alloying (MA). NC structure and the mechanical force-enhanced fast diffusion are the reasons of the formation of supersaturated solid solutions in immiscible systems with positive enthalpy of mixing. HREM observations carried out with the thermally decomposed Fe60Cu40 solid solution show that the Nishiyama (N-W) or Kurdyumov-Sachs (K-S) orientation relationships exist between alpha-Fe and Cu. Energy dispersive X-ray spectra (EDXS) results show that the Cu content in these alpha-Fe grains reaches as high as 9.5 at.% even after heating to 1,400 degrees C, which is even higher than the maximum solubility of Cu in gamma-Fe at 1,094 degrees C.     

硝基联苯、氨基联苯及啶酰菌胺的高效液相色谱分析方法

建立了一种高效液相色谱定量方法,测定以4-氯-2'-硝基联苯制备4-氯-2'-氨基联苯合成啶酰菌胺路线各步反应中的有效成分含量.采用InertSustain ODS-C18不锈钢柱(250 mm×4.6 mm i.d.×5μm)和二极管阵列检测器,以乙腈和0.02％磷酸水为流动相,流速为1.0 mL/min,在220 nm波长下对中间体4-氯-2'-硝基联苯进行分离和定量分析;在254 nm波长下对中间体4-氯-2'-氨基联苯进行分离和定量分析;在254 nm波长下对啶酰菌胺进行分离和定量.分析结果表明,4-氯-2'-硝基联苯保留时间约24.3 min,线性相关系数为1.0000,标准偏差为0.04,变异系数为0.34％,平均回收率为100.04％;4-氯-2'-氨基联苯保留时间约18.0 min,线性相关系数为1.0000,标准偏差为0.05,变异系数为0.33％,平均回收率为99.94％;啶酰菌胺保留时间约11.9 min,线性相关系数为1.0000,标准偏差为0.21,变异系数为0.32％,平均回收率为100.09％.方法 操作简便,精密度与准确度较高,满足定量分析要求.