一种性能可调的新型节能材料－电致变色膜

本文介绍了一种性能可调的新型节能材料—电致色薄膜，描述了以其为核心的全固态灵巧窗结构、工作原理和光学调节性能，回顾了电致色材料、离子存储层和固态锂离子导体及其性质，并展望了这种新型节能材料的应用。     

Phenogenetic analysis of prenatal development of the glucocorticoid function of the adrenals in silver foxes after long-term selection for domesticated behavior

The level of cortisol in serum and adrenals and its production by adrenals in vitro was studied by the radioimmune method in male and female silver fox embryos, starting from day 30 of pregnancy every five days. Pregnant females from a commercial population and an experimental population, which had been selected for domestic behavior, was used. It was shown that, at the end of the prenatal developmental stage, all investigated parameters of the glucocorticoid function of adrenals were significantly lower in embryos from selected mothers as compared to the unselected control group. The addition of adrenocorticotropic hormone into the incubation medium increased cortisol biosynthesis at all embryogenesis stages, but in the selected population the increase was less than that in the control group.     

Determination of organochlorine pesticide and polychlorinated biphenyl residues in fatty fish by tandem solid-phase extraction cleanup

A rapid, multiresidue solid-phase extraction (SPE) technique for determination of organochlorine pesticide and polychlorinated biphenyl (PCB) residues in nonfatty fish was modified for use with fatty fish. In the modified procedures, samples are extracted with acetonitrile, and the extract is cleaned up with both C18 and Florisil SPE columns. Residues are determined by gas chromatography with electron capture detection. The original method was modified for use with fatty fish by reducing the amount of tissue extracted and by using an improved Florisil SPE cleanup. Recovery data are presented for 24 fortified organochlorine pesticide residues (0.12 ppm) and 3 fortified PCB residues (0.80 ppm) from flounder, bluefish, and shad samples, which contained 0.8, 5.4, and 22.6% fat, respectively. For the 3 types of fish, recoveries of 23 of 24 fortified organochlorine pesticide residues ranged from 55 to 129%, and recoveries of 3 fortified PCB residues ranged from 55 to 104%. There were no significant differences in recovery based on fish species and/or fat content for the majority of residues studied. This SPE method and the official AOAC method yielded comparable results for fish containing incurred organochlorine residues.     

m,m′-二氨基二苯酮与均苯四酸二酐的微波辐射聚合

研究 m,m′-二氨基二苯酮 (m,m′- DABP)与均苯四酸二酐 (PMDA)的缩聚及亚酰化 ,并运用微波辐射和常规加热两种方式对反应进行了比较。考察了微波辐射时间 (功率 )、单体浓度、单体配比和温度等因素对缩聚物的特性粘数、转化率的影响。用红外光谱对亚酰化度进行了表征 ,并用简并四波混频技术首次测量了该缩聚物的三阶光学非线性极化率系数及其响应时间。实验结果表明 ,微波辐射对提高聚合物的特性粘数和转化率都有显著作用 ;合成的缩聚物具有较大的三阶光学非线性极化率系数 (聚酰亚胺的 χ(3) =1.642× 10 -13 esu)和较快的时间响应 (19ps     

脉冲化学沉积非晶态Ni—P合金原子分布函数研究

采用Ｘ射线衍射分析技术，研究了脉冲化学镀非晶态Ｎｉ－Ｐ合金的原子分布和函数，得出其短程有序原子集团的尺度为０．７５４ｎｍ，约为熔体激冷法获得的非晶态Ｎｉ－Ｐ合金短程有序畴的１／２。并利用脉冲化学沉积非晶态合金的微机制择这一结果进行了解释。     

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本文介绍了采用复合吸收剂净化天然气的试验结果,在现有三甘醇等脱水剂中添加单乙醇胺,在脱水的同时脱除H_2S,在保证净化气露点低于-21℃的条件下,使净化气中H_2S含量亦低于5mg/m～3。     

激光扫描共焦荧光显微镜的电子控制系统研究

介绍了激光扫描共焦荧光显微镜的电子控制系统，为了提高激光扫描器的定位精度，在系统中提出采用基于闭环象素时钟发生器的检流计振镜所固有的扫描非线性失真补偿方案，减少输出图象的枕形畸变，实现行扫描空间位置的均匀性。在以细分梯形波电流驱动反应式步进电机情况下，根据实测θｉ曲线，用反插法求得与步进电机运行非均匀性相补偿的相电流波，从而获得在小电流情况下高角度均匀的步进电机细分运行特性。     

ATM局域网仿真体系结构的研究

本文在简要叙述了基于ＡＴＭ技术进行局域网仿真的原理后，对局域网仿真体系结构作了一些探讨。考虑的重点是无连接服务和群播功能的实现