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Qiao Zhang Ming Lei Shuwen Huang Huili Fu Guoping Yan Liang Li 《Fullerenes, Nanotubes and Carbon Nanostructures》2017,25(6):386-390
Novel functionalized carbon nanotubes (CNTs) were prepared by grafting disulfide-containing polyethyleneimine (SSPEI) to CNTs. The SSPEI were synthesized by Michael addition between cystamine bisacrylamide and low molecular weight branched 1.8 kDa PEI. Three SSPEI grafted carbon nanotubes (CNTs-SSPEI) were successfully prepared through grafting SSPEI to CNTs. The grafted ratios were 32.26%, 43.11%, and 51.50%, respectively. Moreover, the grafted ratio could be tuned by adjusting the CNTs/SSPEI ratio during the process of preparation. The CNTs-SSPEI was characterized using Fourier transform infrared spectroscopy, scanning electron microscopy and thermogravimetric analysis. The CNTs-SSPEI showed better dispersability and stability in water than CNTs. In addition, the SSPEI on the surface of CNTs-SSPEI could be degraded in the presence of dithiothreitol. 相似文献
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Mu Lei Wang Yuan Zang Yong Araujo Stemler Pedro Malaquias 《Journal of Failure Analysis and Prevention》2017,17(2):321-329
This paper is a contribution to the prediction of edge fracture behavior using uncoupled ductile fracture models. A fully integrated simulation framework for the edge fracture prediction is proposed with the shear-induced pre-damage considered. User-defined material subroutines are coded with uncoupled ductile fracture models (Lou-Huh, Oh, Brozzo) incorporated, which are calibrated using the fracture strains of various loading paths. A series of 3D numerical simulations are performed and compared with the results of hole-expansion tests. The effects of pre-damage field and fracture models are analyzed and discussed.
相似文献998.
Principal component analysis (PCA) was extended to minimize the noise effect in digital image correlation (DIC) measurement under a high-temperature atmosphere environment. First, the principle of PCA was introduced, and the singular vectors and singular values for each component of the displacement fields from DIC were obtained. Then, the simulated high-temperature speckle images were developed to investigate the influences of noise on the DIC method under a high-temperature environment. Finally, the displacement fields of several special conditions were extracted from the simulated speckle images and experimental images; the effects of noise on the PCA were also analyzed. 相似文献
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Yan-kun Tang Qian Yang Xiao-fei Si Jin-kang Han Wei-wei Cao Ya-fei Li Fang Liu Xiaoyan Yao Ya Zhai 《Journal of Superconductivity and Novel Magnetism》2017,30(6):1527-1531
In this study, we report the results of an investigation into the sintering temperature dependence of magnetic and transport properties for GdBaCo2 O 5 + δ synthesized through a sol-gel method. The lowering of sintering temperature leads to the increase of oxygen content and the reduction of grain size. The increase of oxygen content results in the enhancement of magnetic interactions and the weakening of Coulomb repulsion effect, while the reduction of grain size improves the magnetoresistance effect. Metal-insulator transition accompanied with spin-state transition is observed in all samples. 相似文献
1000.
Reducing Hysteresis and Enhancing Performance of Perovskite Solar Cells Using Low‐Temperature Processed Y‐Doped SnO2 Nanosheets as Electron Selective Layers 下载免费PDF全文
Guang Yang Hongwei Lei Hong Tao Xiaolu Zheng Junjie Ma Qin Liu Weijun Ke Zhiliang Chen Liangbin Xiong Pingli Qin Zhao Chen Minchao Qin Xinhui Lu Yanfa Yan Guojia Fang 《Small (Weinheim an der Bergstrasse, Germany)》2017,13(2)
Despite the rapid increase of efficiency, perovskite solar cells (PSCs) still face some challenges, one of which is the current–voltage hysteresis. Herein, it is reported that yttrium‐doped tin dioxide (Y‐SnO2) electron selective layer (ESL) synthesized by an in situ hydrothermal growth process at 95 °C can significantly reduce the hysteresis and improve the performance of PSCs. Comparison studies reveal two main effects of Y doping of SnO2 ESLs: (1) it promotes the formation of well‐aligned and more homogeneous distribution of SnO2 nanosheet arrays (NSAs), which allows better perovskite infiltration, better contacts of perovskite with SnO2 nanosheets, and improves electron transfer from perovskite to ESL; (2) it enlarges the band gap and upshifts the band energy levels, resulting in better energy level alignment with perovskite and reduced charge recombination at NSA/perovskite interfaces. As a result, PSCs using Y‐SnO2 NSA ESLs exhibit much less hysteresis and better performance compared with the cells using pristine SnO2 NSA ESLs. The champion cell using Y‐SnO2 NSA ESL achieves a photovoltaic conversion efficiency of 17.29% (16.97%) when measured under reverse (forward) voltage scanning and a steady‐state efficiency of 16.25%. The results suggest that low‐temperature hydrothermal‐synthesized Y‐SnO2 NSA is a promising ESL for fabricating efficient and hysteresis‐less PSC. 相似文献