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71.
Novel lamellar mesostructured hydroxyapatites have firstly been synthesized by template-assisted technique. The mild and nontoxic surfactant, phosphoric acid monododecyl ester (MAP), is used to act as a structure-directing template. The structure of sample was characterized by X-ray diffraction, Fourier transform infrared spectroscopy, Scanning electron microscope and Transmission electron microscopy. The results indicate that the obtained sample is a well-organized lamellar mesostructured hydroxyapatite with a uniform layer spacing of 3.64 nm. 相似文献
72.
73.
Analytical expressions involving both system parameters and step-size are proposed to represent the local simulation error for the symmetrized split-step Fourier (SSSF) simulation method. This analytical expression can be used for a step-size selection rule to achieve comparable local simulation accuracy for SSSF simulations. This can lead to computational savings since there is no waste of computation in each simulation step. Furthermore, based on the local error expression, scaling rules are derived to achieve comparable global simulation accuracy for wide ranges of key system parameter values. This is significant in enhancing the computational efficiency in optical fiber communication system design and optimization. Extensive validation tests were performed to explore the application range of the proposed step-size selection and scaling rules. The desired global accuracy can be achieved with the use of our local error expression and scaling rules by only a couple of test trial simulation runs for a variety of practical applications. 相似文献
74.
研究了用黄磷渣代替部分粘土作陶瓷原料,既可以解决磷渣对环境的污染和堆放占用耕地问题,使该固体废弃物资源化,又能缓解陶瓷原料的短缺。 相似文献
75.
Yu‐Qing Cao Zhan Zhang Yan‐Xin Guo 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(10):1441-1444
A new efficient method for synthesising nitriles, important organic reagents, is reported in this paper. In an environmentally benign solvent‐free system, aryl carboxylic acids were converted into the corresponding nitriles via one‐pot reactions, by amidation with ethyl carbamate followed by dehydration with thionyl chloride, in excellent yields. The results showed that the method has the advantages of lower cost, higher yield, less pollution and greater ease of work‐up. Copyright © 2008 Society of Chemical Industry 相似文献
76.
本文介绍了一个用户接口管理系统NUUIMS的设计和实现.重点叙述了该系统基于规范化目标用户接口模型的设计思想,系统组成及描述方法.文章也讨论了使用NUUIMS设计而成的用户接口的特点. 相似文献
77.
Aimin Xiang Zhongjie Du Qinghua Zeng Chen Zhang Hangquan Li 《Polymer International》2005,54(10):1366-1370
This paper presents recent efforts on the preparation of flexible polyhedral particles via concentrated emulsion templating polymerization in which the hydrophilic monomer (acrylamide) and hydrophobic monomer (butyl acrylate) are polymerized simultaneously in the continuous and dispersed phase, respectively. Such templating polymerization has been enhanced in our systems owing to the introduction of acrylamide monomer and their higher polymerization rate in continuous phase as compared with butyl acrylate in dispersed phase. Diffusion between the different phases was also inhibited. Furthermore, the stability of the concentrated emulsion and the molecular weight of the produced poly(butyl acrylate) were found to be significantly affected by the amount of redox initiator. The morphology of the particles could be controlled by varying the volume fraction of the dispersed phase and the polyhedral particles were achieved at higher volume fraction. Copyright © 2005 Society of Chemical Industry 相似文献
78.
Ying Ding Chunqing Wang Yanhong Tian Binbin Zhang 《Metallurgical and Materials Transactions A》2006,37(12):1017-1025
in-situ transmission electron microscopy (TEM) tensile tests on as-cast and aged 63Sn37Pb solder alloys were conducted, and the fracture
behavior in nanometer scale ahead of the crack tip was inspected and discussed. Results show that the fracture was completed
by connecting the discontinuous cracks or voids. Dislocation behavior was concentrated along the grain boundaries for as-cast
samples, and displayed mainly as dislocation climb. The crack was intergranular dominated under the lower strain rate. While
remarkable mutual dislocation emission was detected in the aged solder. Transgranular cracks were dominant in the fractured
area, and they propagated by linking up with the nanometer scale cracks ahead of the crack tips under the effective promotion
of the inverse dislocation emission. At the same time, the partial interphase or intergranular cracks in the thinned area
were also found. Under this condition, a new critical stress intensity factor K
c
′ to define the mutual dislocation emission was proposed. 相似文献
79.
On structural and high temperature electrochemical properties of ZrO2 thin film coating on Zr metal produced by carbonate melt 总被引:1,自引:0,他引:1
Melt of NaCO3 can favor oxidation of Zr to form ZrO2 thin film on Zr surface, which is used to make Zr/ZrO2 oxidation/reduction electrode of pH sensor for testing elevated temperature aqueous solutions. Using SEM, EPMA, XPS, EXAFS
and HRTEM, we found that ZrO2 film is tightness and solid with 20 μm thickness composed by nanometer-sized monoclinic crystals. Zr/ZrO2 interface is characterized of zoning structure according to topography and chemical composition in five zones: oxygen-rich
ZrO2, ZrO2, oxygen-rich Zr metal, oxygen-bearing Zr and Zr from outmost to center. Melt oxidation process of Zr involved oxidation time,
air and temperature. The air is important effect on structural and electrochemical properties of ZrO2 thin film for making elevate temperature electrochemical sensor. If oxygen air largely presented in carbonate melting process,
ZrO2 thin film is not tightness and not for oxidation/reduction electrode. 相似文献
80.