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91.
Sapana Guru Deepti Mishra Manju Singh Sudhir Sitaram Amritphale Smita Joshi 《Protection of Metals and Physical Chemistry of Surfaces》2016,52(4):627-631
In the present work iron oxide nanoparticles have been prepared by microwave assisted synthesis with the influence of different precursor salts and synthesis of magnetite, hematite, Iron oxide hydroxide and maghemite nanoparticles. Synthesized iron oxide nanoparticles were characterized with Infrared Spectroscopy (FTIR), Field Emission Scanning Electron Microscopy (FESEM), and Energy-dispersive X-ray Spectroscopy (EDX). XRD measurements show that the peaks of diffractogram are in agreement with the theoretical data of magnetite, hematite, FeO(OH) (Iron oxide hydroxide) and maghemite. Crystallite size of the particles was found to be 33, 45, 36 and 43.5 nm for Fe3O4, α-Fe2O3, FeO(OH) and γ-Fe2O3. FESEM studies indicated that size of the particles is observed in the range of about 19.4 to 46.7 nm (Fig. 2a, average 32 nm), 29.1 to 67.6 nm (Fig. 2b average 45 nm), 29.1 to 40.8 (Fig. 2c average 36.6 nm), 29.1 to 80 nm (Fig. 2d average 43.5) for Fe3O4, α-Fe2O3, FeO(OH) and γ-Fe2O3 respectively. EDX spectral analysis reveals the presence of carbon, oxygen, iron in the synthesized nanoparticles. The FTIR graphs indicated absorption bands due to O–H stretching, C–O bending, C–H stretching and Fe–O stretching vibrations. 相似文献
92.
Sarika Verma Mishra Deepti Sanghi S. K. Srivastava A. K. Amritphale S. S. 《Protection of Metals and Physical Chemistry of Surfaces》2019,55(1):65-71
Protection of Metals and Physical Chemistry of Surfaces - We report a facile and reproducible method to synthesize advanced, homogenized, hybrid, nanoflower of thorium oxide and thorium oxalate... 相似文献
93.
Oil-in-water emulsions are used as metalworking fluids (MWFs). Considering the environmental issues and operator's health, the amount of oil-in-MWFs is one of the important parameters. In the present study, paraffin oil is used for emulsion formulation and possibilities to minimize the amount of paraffin oil-in-MWFs are explored. Physical characterization of emulsions is done using dynamic light scattering and goniometer. The tribological response of emulsions is recorded using the Four-ball tester. Results indicate that the amount of oil can be brought down to a level of 0.5% v/v to achieve the standard friction level. Droplet size and distribution seems to control the lubricity of emulsions, smaller droplets are desired for better lubrication. 相似文献
94.
95.
The diesel engines are energy efficient (1), but their particulate matter (soot) emissions are still a matter of concern even though major advances in their control are being made. For soot abatement, catalytic diesel particulate filter (DPF) technique is widely employed to trap and burn the soot. Many types of catalysts have been investigated for the soot combustion i.e. platinum group metal (PGM) based, perovskite-type oxides, spinel-type oxides, rare earth metal oxides, and mixed transient metal oxides etc. The cost of PGM catalysts is high and their availability is questionable. Further they are susceptible to poisoning and have low thermal stability. On the other hand perovskite catalysts show potential as effective soot oxidation catalyst for the DPF because of their low cost, high thermal stability and tailoring flexibility. Many papers related to soot oxidation over perovskite catalysts have been published but no review paper appears in the literature that is dedicated to soot oxidation. Thus, this article provides a summary of published information regarding pure and substituted perovskite catalyst, preparation methods, properties, and their application for diesel soot emission control. 相似文献
96.
Navinchandra G. Shimpi Ananda D. Mali Harishchandra A. Sonawane Satyendra Mishra 《Polymer Bulletin》2014,71(8):2067-2080
Isotactic polypropylene (iPP): ethylene propylene diene monomer (EPDM) blend is one of the most suited compatible and miscible blends. The blends of iPP and EPDM (80:20) filled with BaCO3 nanoparticles (0.5, 1.5, 2.5 and 3 wt%) were prepared on Brabender Plasticorder, which was then subjected to injection molding to get dumbbell-shaped specimens. Meanwhile, BaCO3 nanoparticles (nBaCO3) were prepared using ultrasonic cavitation technique. The size and shape of nBaCO3 particle was confirmed using transmission electron microscope and found to be capsule shape of diameter ~40–60 nm with aspect ratio (l/d) of 2.2–2.5. The reduction in particle size of nBaCO3 leads to formation of uniform suspension. The solution was kept as such for long time so as to nullify the charges developed over the surface of nanoparticles. The mechanical properties of nBaCO3-reinforced iPP-EPDM blends were studied using universal testing machine and impact tester. Moreover, thermal properties were studied using flammability tester, vicat softening temperature, thermo gravimetric analyzer and differential scanning calorimeter (DSC). Dispersion of nBaCO3 in iPP-EPDM matrix was studied using scanning electron microscope and X-ray diffractometer. The mechanical and thermal properties of iPP-EPDM/nBaCO3 blends were found to be improved significantly with increasing amount of nBaCO3 up to 2.5 wt%, which is due to good compatibility in between iPP and EPDM with uniform dispersion of nBaCO3. Moreover, due to agglomeration at 3 wt% loading of nBaCO3 few of the properties found to be decreased marginally. 相似文献
97.
Sandeep Panda Pradeep Chandra Rout Chinmaya Kumar Sarangi Srabani Mishra Nilotpala Pradhan Umaballav Mohapatra Tondepu Subbaiah Lala Behari Sukla Barada Kanta Mishra 《Korean Journal of Chemical Engineering》2014,31(3):452-460
Bioleaching studies for chalcopyrite contained ball mill spillages are very scarce in the literature. We developed a process flow sheet for the recovery of copper metal from surface activated (600 °C, 15 min) ball mill spillage through bio-hydrometallurgical processing route. Bioleaching of the activated sample using a mixed meso-acidophilic bacterial consortium predominantly A. ferrooxidans strains was found to be effective at a lixiviant flow rate of 1.5 L/h, enabling a maximum 72.36% copper recovery in 20 days. Mineralogical as well as morphological changes over the sample surface were seen to trigger the bioleaching efficiency of meso-acidophiles, thereby contributing towards an enhanced copper recovery from the ball mill spillage. The bio-leach liquor containing 1.84 g/L Cu was purified through solvent extraction using LIX 84I in kerosene prior to the recovery of copper metal by electrowinning. Purity of the copper produced through this process was 99.99%. 相似文献
98.
99.
正Ground control is the science of studying and controlling the behavior of rock strata in response to mining operations.Ground-control-related research has seen significant advancements over the last 40 years, and these accomplishments are well documented in the proceedings of the annual International Conference on Ground Control in Mining (ICGCM)[1]. 相似文献
100.