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41.
Vinamrita Singh Swati Arora P. K. Bhatnagar Manoj Arora R. P. Tandon 《Journal of Polymer Research》2012,19(6):1-6
We have investigated the degradation of P3HT:PCBM (poly(3-hexylthiophene):6,6-phenylC61 butyric acid methyl ester) solar cell beyond 150?h of fabrication in continuation to our earlier reported work up to 150?h of fabrication. The current- voltage characteristics of degraded Indium tin oxide/poly(3,4-ethylenedioxythiopene):poly(styrenesulfonate)/poly(3-hexylthiophene):6,6-phenylC61 butyric acid methyl ester/Aluminum (ITO/PEDOT:PSS/P3HT:PCBM/Al) solar cell can be explained by considering the tunneling current through electrode interfaces, increase in both the interface states density and the thickness of interface with time for150-200?h. Beyond 200?h of fabrication, a significant reduction in the occupation probability at the electrode interfaces explains the experimental results up to 300?h fairly well. Calculations based on realistic parameters and activity at both the electrode interfaces (ITO/PEDOT:PSS and P3HT:PCBM/Al) confirm that degradation at P3HT:PCBM/Al interface is more prominent than that at ITO/PEDOT:PSS interface. 相似文献
42.
Jomy Joseph Prithvi Raj Munda Manoj Kumar Ajay M. Sidpara 《Polymer-Plastics Technology and Engineering》2020,59(10):1088-1099
ABSTRACTBall milled jute fiber (JF) was added to Polyvinyl Alcohol (PVA)/20 wt.% multi-layer graphene (MLG) composites in various proportions (0, 5, 10, 15 and 20 wt.%) to prepare sustainable and biodegradable conducting polymer composites. Also, PVA/17.5wt.%MLG/2.5wt.%MWCNT/20wt.% JF composite was prepared for comparison purpose. A dynamic mechanical analysis of the composites was conducted to analyze their viscoelastic nature. The electrical conductivity of the composites was measured to study their suitability for various applications. Jute reinforcement increased the electrical conductivity of PVA/MLG nanocomposites. The PVA/20wt.%JF/17.5wt.%MLG/2.5wt.%MWCNT hybrid composite had the highest electrical conductivity of 3.64 × 10?4 S/cm among all the composites prepared. Multilayered structures of the hybrid composite films were made by hot-pressing, and their effectiveness in electromagnetic interference shielding was tested. The shielding effectiveness of the composites decreased with jute addition. The wear resistance of PVA/MLG/JF composites increased with an increase in the jute content up to an optimum value of 10 wt.%, and then it started deteriorating. 相似文献
43.
Manoj K. Mahapatra 《International Journal of Applied Ceramic Technology》2020,17(2):606-615
Advancing high temperature technologies pushes the envelope of the service conditions to new extremes. However, corrosion of refractories substantially decreases the service life and causes unscheduled shutdown of manufacturing and processing plants. In this paper, corrosion of refractories in gaseous environments is reviewed. The corrosion mechanisms of alumina refractories, including alumino-silicates and zirconia as oxide, and silicon carbide as non-oxide refractory are emphasized due to their broad array of applications. It is shown that carbonaceous atmosphere and water vapor are detrimental for the oxide refractories. Interaction with water vapor leads to formation of the volatile species and subsequent recession of the refractories. Carbonaceous atmosphere leads to the decomposition of even mullite, which is categorized as neutral refractory due to its excellent thermochemical stability. Oxidizing atmosphere with water vapor dominates the corrosion of non-oxide refractories. Presence of impurities, even parts per million level, in the gas stream such as alkali vapor and halogens can alter the corrosion mechanisms and favor “hot corrosion.” 相似文献
44.
Manoj Karakoti Ritu Jangra Sandeep Pandey Pawan Singh Dhapola Sunil Dhali Suman Mahendia Pramod K Singh Nanda Gopal Sahoo 《International Journal of Applied Ceramic Technology》2020,17(4):1899-1908
This study deals with the utility of mini spray dryer process to improve the dispersibility, of graphene oxide(GO) and its application for high-performance supercapacitor. Initially, the neutral solution of GO was obtained using the modified Hummer's method. After this, the prepared GO solution was processed by mini spray dryer to obtain a more purified, lighter, and dispersed form of GO which is named as spray dryer processed GO (SPGO). The SPGO thus obtained showed excellent dispersibility behavior with various solvents, which is not found in case of conventional oven drying. Furthermore, utility of SPGO and its reduced form (r-SPGO) for supercapacitor applications have been investigated. Results obtained from the cyclic voltammetry(CV) analysis, impedance, and charge-discharge behavior of supercapacitor fabricated using r-SPGO shows enhanced features. Therefore, the simple spray dried GO and its reduced form, that is, r-SPGO can be utilized as a potential candidate for the supercapacitor application. Herein, as synthesized SPGO exhibited the specific capacitance of 12.07 and 37.6 F/g with PVA-H3PO4 and 1 mol/L H3PO4, respectively, at a scan rate of 5 mV/s. On the other hand, reduced form of SPGO, that is, r-SPGO showed the specific capacitance of 27.16 and 230 F/g with PVA-H3PO4 and 1 mol/L H3PO4, respectively. 相似文献
45.
Arun K. Verma V. Rajkumar Ravindra Kumar K. Gururaj Tarun Pal Singh Manoj K. Singh 《European Journal of Lipid Science and Technology》2023,125(10):2300143
This study investigated the effect of supplementing omega fatty acids-rich oil blend, composed of sunflower oil (1.5% and 3.0%), linseed oil (1.5% and 3.0%), and FineXNV1810 (20 g) on the carcass, meat quality, fatty acid profile, and genes (peroxisome proliferator-activated receptor-α, stearoyl-CoA desaturase, acetyl-CoA carboxylase, hydroxy-3-methylglutaryl coenzyme A, and leptin) of Barbari goats. The goat kids (n = 18) were divided into three groups, namely, group A: basal diet; group B: basal diet + oil blend level 1; and group C: basal diet + oil blend level 2, and subjected to the feeding trial for 120 days followed by slaughter and meat quality studies. No treatment effect was recorded in carcass characteristics, pH, water holding capacity, and proximate composition of meat. However, a significant (p < 0.05) treatment effect was observed in cooking loss, lightness, yellowness, and shear force values of meat. There were significant differences (p < 0.05) in linoleic acid, α-linolenic acids, conjugated linoleic acid (CLA), polyunsaturated fatty acids (PUFA), n − 3 and n − 6 PUFA, PUFA/saturated fatty acids and n − 6/n − 3 ratios, and thrombogenic index among groups. An upregulation of the studied genes in the supplemented groups was observed. There were upregulations in the studied genes in the supplemented groups. Practical applications: Goat meat is in great demand the world over, especially in tropical countries, including India, and does not carry any social or religious prohibition. Although goat meat has relatively less fat, consumers express their concern over the presence of undesirable fatty acids. The present study shows that the fatty acid configuration of goat meat can be improved by a dietary supplementation of an oil blend rich in omega fatty acids. The amount of n − 3 PUFA, n − 6 PUFA, and CLA in goat meat was significantly increased due to the dietary oil blend making it healthy for the consumers. Moreover, the dietary oil blend at the studied levels did not significantly affect the growth and meat quality parameters of the goats. Thus, the studied approach can be successfully followed to produce healthier goat meat. 相似文献
46.
Foaming of rigid polyvinyl chloride (PVC) is studied as a function of high molecular weight acrylic processing aids. The industrial process to evaluate quality of foam is discussed in detail. The role of acrylic processing aids to improve melt strength and hence foaming of PVC is explained. It is demonstrated that increase in molecular weight of acrylic processing aids increases its effectiveness. It is found that ultra-high molecular weight processing aids is 25%–30% more efficient than relatively lower, but still high, molecular weight acrylic processing aids. The higher molecular weight processing aids provided comparable foaming performance at lower loading levels. Foaming reduced the density of PVC compounds to 0.32–0.34 g/cm3. More than 1000% expansion is achieved in the melt extrusion process using a chemical blowing agent. Fusion characteristics are also studied. Fusion times for initial fusion peaks are in the range of 42–44 s while the fusion times of the second fusion peaks are in the range of 74–94 s. The higher molecular weight processing aids maintained fusion characteristics of PVC compounds, warranting no significant changes in commercial process. 相似文献
47.
Shukla Anshuman; Raje Manoj; Guptasarma Purnananda 《Protein engineering, design & selection : PEDS》2003,16(12):875-879
The backbone-reversed or retro, form of a modelall-ß-sheet protein, Escherichia coli CspA, was producedfrom a synthetic gene in E.coli in fusion with an N-terminalaffinity tag. Following purification under denaturing conditionsand dialysis-based removal of urea, the protein was found tofold into a soluble, poorly structured multimer. Upon concentration,this state readily transformed into amyloid nanofibres. CongoRed-binding amorphous forms were also observed. Since a ß-sheet-formingsequence is expected to retain high ß-sheet-formingpropensity even after backbone reversal and given the fact thatfolding of retro-CspA occurs only to a poorly structured form,we conclude that the increase effected in protein concentrationmay be responsible for the formation of intermolecular ß-sheets,facilitating the bleeding away of the proteins conformationalequilibrium into aggregates that generate well-formed fibres.Since every molecule in these fibres contains a peptide tagfor binding Ni2+, the fibres may provide a template for depositionof nickel to generate novel materials. Received April 1, 2003; revised October 27, 2003; accepted October 30, 2003 相似文献
48.
49.
Phase Evolution,Magnetic, Optical,and Dielectric Properties of Zr‐Substituted Bi0.9Gd0.1FeO3 Multiferroics 下载免费PDF全文
Prakash Chandra Sati Manoj Kumar Sandeep Chhoker 《Journal of the American Ceramic Society》2015,98(6):1884-1890
Polycrystalline BiFeO3 (BFO) and Bi0.90Gd0.10Fe1?xZrxO3 (x = 0.0–0.10; BGFZx) ceramics were synthesized by solid‐state reaction method. Rietveld analysis of X‐ray diffraction patterns showed that BFO and BGFZx = 0.0 samples are stabilized in rhombohedral structure (space group R3c), whereas a small fraction of orthorhombic phase (space group Pn21a) is observed for BGFZx = 0.03–0.10 samples. Suppression and disappearance of some Raman modes indicated a structural phase transition with addition of Zr dopant at Fe site. Magnetic measurements exhibited weak ferromagnetic behavior of BGFZx samples with increasing Zr+4 concentrations. The insertion of Gd+3 ions at Bi+3 sites and nonmagnetic Zr+4 ions at Fe+3 sites in Fe–O–Fe network suppressed the spin cycloid structure of BFO which in turn enhanced the magnetization of these ceramics. Electron spin resonance spectra revealed the breaking of spin cycloid of BFO due to the development of free spins with addition of Zr+4 dopants at Fe sites. UV–Visible diffuse reflectance spectra showed one d–d crystal field transition and two charge‐transfer (C–T) transitions along with a sharp absorption of light in visible region for all samples. Almost frequency‐independent dielectric constant and dielectric loss along with very low values of dielectric loss indicated greatly improved dielectric properties for BGFZx = 0.03–0.10 samples. 相似文献
50.
Broadband dielectric spectroscopy of Nafion‐117, sulfonated polysulfone (sPSF) and sulfonated polyether ketone (sPEK) membranes 下载免费PDF全文
Wasim F. G. Saleha Rahul Ramesh Naresh Nalajala Arup Chakraborty Bradley P. Ladewig Manoj Neergat 《应用聚合物科学杂志》2017,134(18)
Nafion®‐117, sulfonated polysulfone (sPSF) and sulfonated polyetherketone (sPEK) are characterized using broadband dielectric spectroscopy in the frequency range of 10 MHz–100 mHz. Overall, there are 4–5 relaxation processes in these sulfonated membranes and a comparison of their spectral features allows assigning the relaxation processes. At an optimum amplitude of ~100 mVrms, all the relaxations are clearly defined as the electrode polarization is minimized. At low temperatures (?130 °C), these membranes show a broad relaxation peak in the mid‐frequency region, which quickly shifts towards the high‐frequency region as the temperature is increased to ?90 °C. This peak is observed in proton exchange membranes for the first time due to the use of low ac amplitude, and it is assigned to the relaxation of the confined water in the micro‐pores. With all the membranes, the peak associated with ? SO3H group relaxation is observed in the same frequency range at a temperature of ~?80 °C. © 2017 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2017 , 134 , 44790. 相似文献