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排序方式: 共有1494条查询结果,搜索用时 15 毫秒
101.
Maryam Jahan Biglari Rouhollah Semnani Rahbar Meisam Shabanian Hossein Ali Khonakdar 《Polymer-Plastics Technology and Engineering》2019,58(8):879-888
New polyamide 66/graphene oxide (GO)-grafted aliphatic-aromatic polyamide (polyamide-imide) (PAI) (PA66/GOF) composites nanofibers were successfully prepared via electrospinning method for the first time. An polyamide imide (PAI) was synthesized using polycondensation reaction from a dicarboxylic acid and a diamine based on 4,4′-(4,4′-isopropylidenediphenyl-1,1′-diyldioxy) dianiline, and characterized by 1HNMR and FTIR. Morphological, structural, thermal and mechanical characteristics of the nanocomposite fibers were investigated by means of SEM, TEM, WAXD, DMTA and TGA techniques. Composites nanofibers of PA66/GO, PA66/PAI and PA66/GOF with smooth surface, uniform structure as well as with diameter ranging from 195 to 784 nm were obtained. The GO incorporation caused a reduction in the nanofibers diameters. The TEM images showed that the GO was well dispersed in the PA66 nanofibers without significant aggregation. An approximately 10 °C temperature increase in the glass transition temperature of PA66 was achieved by addition of 0.5 wt% of PAI, resulting from aliphatic-aromatic structure of PAI. By the TGA results, an increase about 40 °C was observed in the thermal stability of PA66/PAI composite nanofibers in comparison with that of pure PA66 nanofibers. 相似文献
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This study investigates the effect of clay addition on the broadband dielectric properties of multi‐walled carbon nanotube/polyvinylidene fluoride (MWCNT/PVDF) composites, that is, frequency range of 101−106 Hz. Different loadings of MWCNT and clay were used for the preparation of three‐phase (MWCNT/Clay/PVDF) nanocomposites via melt‐mixing method. The crystalline structure and morphology of nanocomposites were examined by employing characterization techniques such as X‐ray diffraction, transmission electron microscopy, and differential scanning calorimetry. The dielectric spectroscopy showed that introducing clay into the MWCNT/PVDF nanocomposites at a critical MWCNT concentration improved dielectric properties tremendously. It was interestingly observed that the incorporation of a specific amount of clay, that is, 1.0 wt%, into the (MWCNT/PVDF) nanocomposite at a critical MWCNT loading, that is, 0.5 wt% MWCNT, resulted in a huge increase in the dielectric permittivity (670% at 100 Hz) and a considerable reduction in the dissipation factor (68% at 100 Hz). POLYM. COMPOS., 161–167, 2016. © 2014 Society of Plastics Engineers 相似文献
105.
Investigating the effect of paper properties on color reproduction of digital printing 总被引:1,自引:0,他引:1
Digital printing is affected by several parameters including printer and paper type which determine the final printed color gamut and the quality of reproduction. For investigation of those effects, tests were done on the three types of laser printer and six types of paper with different properties of whiteness, roughness, and gloss. The gamut volume was generated by Eye-One spectrophotometer, ProfileMaker, and ColorThink software. Properties of the different types of paper were measured by the atomic force microscopy, spectrophotometer and, goniophotometer. Results showed that the reproducibility was considerably dependent on the type of printer and type of paper. High whiteness and gloss increased the color gamut volume, while high roughness decreased the reproducibility of the printer. Tests on paper properties showed that whiteness had the most significant effect on color gamut volume. 相似文献
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Farshid Hassanzadeh Sahar Maaleki Jaleh Varshosaz Ghadam Ali Khodarahmi Maryam Farzan Mahboubeh Rostami 《Iranian Polymer Journal》2016,25(11):967-976
A novel thermosensitive folic acid (FA)-targeted succinylated poly (ethylene-co-vinyl alcohol) (EVOH) (EVOHS-FA) nanocarrier was synthesized for the specific delivery of epirubicin (EPI) to MCF-7 breast cancer cell line. Three different ratios of synthesized EVOH-Suc were reacted with FA. The structure of the desired products (EVOHS40-FA, EVOHS60-FA and EVOHS80-FA) was confirmed by 1H NMR and FTIR techniques. Nanoparticles were obtained by nano-precipitation procedure using DMSO/H2O as solvent/anti-solvent. The particle size, zeta potential, entrapment efficacy and in vitro release profile of the final formulations in different temperatures were measured. The optimized nanoparticles had the particle size of 214 ± 8.5 nm, zeta potential of ?29.6 mV, PDI of 0.198 ± 0.04, and a high encapsulation efficiency that released the drug efficiently within 450 h at the temperature of 40 °C compared to 37 °C. The morphology of nanoparticles was studied by scanning electron microscopy. The in vitro cytotoxicity was evaluated using the MTT assay on MCF-7 cell lines in response to temperatures of 37 and 40 °C. The MTT assay indicated that the targeted nanoparticles carrying EPI were significantly more cytotoxic than the non-targeted nanoparticles and the free drug at 40 °C. 相似文献
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Polyester composite water uptake and organic contaminant release affected by carbon nanofiber reinforcements 下载免费PDF全文
Maryam Salehi Ajay Krishnamurthy Aaron M. Forster Kuang–Ting Hsiao Andrew J. Whelton 《应用聚合物科学杂志》2016,133(30)
The incorporation of carbon nanofiber (CNF) into glass fiber (GF) composites is a potential route to extend polymer composite service‐life and enhance mechanical properties. Under nonstatic conditions, only limited information concerning water uptake and contaminant release properties of nanocomposite materials is currently available. Polyester composites containing GF and oxidized CNF were immersed in water for 30 days under nominal pressure at 23 °C, below the polymer's glass‐transition temperature. Water was analyzed and changed every three days to simulate water chemistry regeneration similar to exposures in flowing systems. Composites with oxidized CNF had greater water sorption capacity and leaching rates than CNF‐free composites. The total mass of organic contaminant released correlated with the amount of water sorbed by each composite (r2 = 0.91), although CNF dispersion was found to vary greatly within composites. The greatest and least contaminant release rates were found for the polyester‐CNF and the polyester‐GF composites, respectively. While volatile aromatic resin solvents and stabilizer compounds were detected, their concentrations declined over the 30 day exposure period. We hypothesize that the hydrophilic nature of the oxidized CNF increased the water sorption capacity of the polyester composites. Additional studies are warranted that examine the impact of this phenomenon on composite mechanical and long‐term durability properties. © 2016 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2016 , 133, 43724. 相似文献
110.
Ali Shokuhi Rad Mehri Esfahanian Sina Maleki Gelare Gharati 《Journal of Sulfur Chemistry》2016,37(2):176-188
We studied the adsorption of SOx (x?=?2,3) molecules on the surface of pristine graphene (PG) and N-doped graphene (NDG) by density functional theory (DFT) calculations at the B3LYP/6-31G(d) level. We used Mulliken and NBO charge analysis to calculate the net charge transfer of adsorbed SOx on pristine and defected graphene systems. Our calculations reveal much higher adsorption energy and higher net charge transfer by using NDG instead of pristine graphene. Furthermore, the density of state (DOS) graphs point to major orbital hybridization between the SOx and NDG, while there is no evidence of hybridization by using pristine graphene. Based on our results, it is found that SO2 and SO3 molecules can be adsorbed on the surface of NDG physically and chemically with adsorption energies (Eads) of ?27.5 and 65.2?kJ?mol?1 (19.6 and 51.4?kJ?mol?1 BSSE), respectively, while low adsorption energies were calculated in the case of using pristine graphene. So we introduced NDG as a sensitive adsorbent/sensor for detection of SO2 and SO3. 相似文献