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71.
72.
Shunjiro Ogawa Hideyo Suzuki Masatake Toyoda Yoshio Ito Masahiro Iwaida Hiroko Nonogi Tazu Fuke Kazuo Obara Tadao Adachi Koichi Fujita Makiko Ikuzawa Tetsuo Izumi Takashi Hamano Yukimasa Mitsuhashi Yukio Matsuki 《Zeitschrift für Lebensmitteluntersuchung und -Forschung A》1979,168(4):293-298
Summary Detection and determination of traces of sulphites in foods was attempted by use of the modified Rankine apparatus and pararosaniline colorimetry. Replacement of alkaline titration reported previously by pararosaniline colorimetry lowered the absolute detection limit from 30 g (titration method) to 2 g. In view of clean analysis, in the color developing system, 0.1 N-sodium hydroxide was used in place of mercuric chloride solution commonly used as an absorbant of sulphites. In order to prevent oxidative decomposition of sulphites during operation, nitrogen gas was used as carrier instead of air. Dimedone and sodium azide were used for the elimination of aldehydes and nitrites, respecitvely, in the sample, which will disturb the color development of sulphites with pararosaniline-formaldehyde reagents. With this improved method, it was possible to determine the residual sulphites in frozen peeled shrimps, sugared beans and other foods with low sulphite contents accurately.
Studies on the Analyses of Sulphites in Foods (IV) 相似文献
Colorimetrische Mikrobestimmung von Sulfiten in Lebensmitteln bei Anwendung der modifizierten IV. Rankine Apparatur
Zusammenfassung Geringe Sulfitmengen in Lebensmitteln (geschälte Garnelen, gezuckerte Bohnen) können colorimetrisch bestimmt werden. Die neuentwickelte Methode beruht auf einer Kombination von colorimetrischer Bestimmung mittels p-Rosanilin und der Bestimmungsmethode nach Rankine. Auf diese Weise lassen sich Gehalte von 2 g noch genau bestimmen. Bei der Farbentwicklung wurde das giftige Quecksilbertetrachlorid durch 0.1 n-NaOH ersetzt, anstelle von Luft Stickstoff als Trägergas verwendet und somit eine Oxydation des Sulfits während der Bestimmung vermieden. Da Nitrit und Aldehyde die Farbentwicklung stören, wurde ihr Einfluß durch Dimedon und Natriumazid ausgeschaltet.
Studies on the Analyses of Sulphites in Foods (IV) 相似文献
73.
Atsunori Matsuda Yugo Higashi Kiyoharu Tadanaga Masahiro Tatsumisago 《Journal of Materials Science》2006,41(24):8101-8108
SiO2–TiO2 spherical microparticles of about 0.7 μm in diameter were prepared by the sol–gel method. Anatase nanocrystals were formed in the microparticles and their specific surface area was increased after a hot-water treatment at 90 °C. From the changes in the concentration of I2 photocatalytically generated from KI aqueous solution, the activity of the SiO2–TiO2 microparticles was found to increase with increasing the hot-water treatment time. Particulate, thick films were electrophoretically deposited on indium tin oxide (ITO)-coated glass substrates using the anatase nanocrystal-precipitated SiO2–TiO2 microparticles. The thickness of the electrophoretically deposited particulate film increased to be approximately 10 μm with an increase in applied voltage. The resultant thick film showed a high photocatalytic activity. 相似文献
74.
Effect of heparin on high glucose induced proliferation and expression of matrix metalloproteinases in normal human mesangial cells 总被引:1,自引:0,他引:1
Zhou Qiao-ling Yasumoto Yuichiro Tsukamoto Masatoshi Nozaki Tsuyoshi Sogabe Atsushi Harada Kouji Zhang Yi-xiang Lin Xiao-yan Zhang Yang-de Arima Terukatsu 《中南工业大学学报(英文版)》2005,12(1):359-364
Background The pathogenesis of diabetic nephropathy (DN) is a complex pathophysiological process. Its precise mechanism is not fully
known. In recent years it has been recognized that synthesis of various extracelluar matrix (ECM) components may increase,
and that degradation of ECM may decrease in DN. It was reported heparin could inhibit mesangial cells proliferation in vitro.
The main aim of this study is to explore whether heparin inhibits proliferation of mesangial cells grown in high glucose concentration
and to measure the effect of heparin on matrix metalloproteinases (MMPs) expression in mesangial cells. Methods The medium contained either low glucose (5 mmol/L) or high glucose (25 mmol/L). The concentrations of heparin in the culture
medium were 0, 25, 50, 100, 200 or 400 μg/mL. A metabolic (WST-1) assay was used to measure mesangial cell proliferation and
Western blot analysis was used to measure MMPs expression of mesangial cells. Results Normal human mesangial cell (NHMC) proliferation was higher in high glucose (HG) medium than in low glucose (LG) medium.
They showed a 1.93 fold expansion after 72 h in high glucose in contrast to a 1.63 fold expansion in low glucose. In the presence
of heparin, mesangial cells proliferation was inhibited, which was more obvious at high glucose concentrations than at low
glucose concentrations. In high glucose, with heparin concentration of 50, 100, 200 and 400 μg/mL, the mesangial cells showed
a 0.61 fold, 0.52 fold, 0.52 fold and 0.41 fold reductions in cell number compared to cells grown without heparin. In low
glucose, only concentrations of 200 μg/mL and 400 μg/mL showed reduction in cell number, namely 0.54 fold and 0.45 fold, when
compared to cells grown without heparin. In Western blot analysis, MMP1, MMP2, MMP3 and MMP9 was expressed by mesangial cells expressed in both high and low glucose concentrations, which was more prominent in high
glucose medium. Incubation of heparin further increased expression of MMP1, MMP2, MMP3 and MMP9. Conclusions This study suggests that glucose can accelerate mesangial cell proliferation while heparin can reduce proliferation, being
more obvious at high glucose concentrations. Higher glucose concentrations led to increased MMP expression, which may take
part in the regulation of mesangial matrix synthesis and degradation. Addition of heparin resulted in a corresponding increase
in MMP expression, most notably at high glucose concentrations, indicating a potentially renoprotective role in DN.
Foundation item: Project (30370663) supported by the National Natural Science Foundation of China 相似文献
75.
Chuanyong Gui Akihiro Sato Yuefeng Gu Hiroshi Harada 《Metallurgical and Materials Transactions A》2005,36(11):2921-2927
We proposed a new method for developing Ni-base turbine disc alloy for application at temperatures above 700 °C by mixing
a Ni-base superalloy U720LI with a two-phase alloy Co-16.9 wt pct Ti in various contents. The microstructure and phase stability
of the alloys were analyzed using an optical microscope, a scanning electron microscope, energy-dispersive spectroscopy, and
an X-ray diffractometer. The yield strength was studied by compression tests at temperatures ranging from 25 °C to 1200 °C.
The results show that all the alloys had a dendritic structure. Ni3Ti (η) phase was formed in the interdendritic region in the alloys with the addition of Co-16.9 wt pct Ti, and its volume fraction
increased with the increase in the addition of Co-16.9 wt pct Ti. The results of exposure at 750 °C show that the addition
of Co-16.9 wt pct Ti to U720LI had a great effect on suppressing the formation of σ phase due to the reduced Cr content in the γ matrix. Compared to U720LI, the alloys with the addition of Co-16.9 wt pct Ti possessed higher yield strength. The solid-solution
strengthening of γ and γ′ and higher volume fraction of γ′ were assumed to cause this strength increase. 相似文献
76.
C. Huang Y. Yamabe-Mitarai S. Nakazawa H. Harada X. H. Yu 《Metallurgical and Materials Transactions A》2005,36(3):539-545
Two quanternary systems, Ir-Nb-Ni-Al and Ir-Nb-Pt-Al, were successively investigated to assess their possible use in ultra-high-temperature
applications. The phase relationships concentrated on the fcc/L12 two-phase region were primarily established, and the mechanical properties were studied. Ir-Nb-Ni-Al quaternary alloys around
the Ir-rich or Ni-rich corners of the Ir-Nb-Ni-Al tetrahedron showed a coherent fcc/L12 two-phase structure, analogous to that of Ni-base superalloys; however, most of the alloys presented three or four phases
with two types of L12 phases. Although these alloys showed a high compressive strength at high temperature, they exhibited a higher creep rate
than Ir-base binary and ternary alloys. Another quanternary system, Ir-Nb-Pt-Al, showed promising results. Only an fcc/L12 two-phase structure was found in all the alloys investigated with compositions ranging from the Ir-rich side to the Pt-rich
side, and the lattice misfit between the fcc and L12 phases was small. The high-temperature strength at 1200 °C of Ir-Nb-Pt-Al alloys was higher than that of Ir-Nb-Ni-Al alloys
with the same Ir content (at. pct). Moreover, Ir-Nb-Pt-Al alloys exhibited excellent creep resistance at 1400 °C and 100 MPa.
This article is based on a presentation made in the symposium entitled “Beyond Nickel-Base Superalloys,” which took place
March 14–18, 2004, at the TMS Spring meeting in Charlotte, NC, under the auspices of the SMD-Corrosion and Environmental Effects
Committee, the SMD-High Temperature Alloys Committee, the SMD-Mechanical Behavior of Materials Committee, and the SMD-Refractory
Metals Committee. 相似文献
77.
Y. Yamabe-Mitarai Y. Gu H. Harada C. Huang 《Metallurgical and Materials Transactions A》2005,36(3):547-557
Ir-base alloys with the fcc and L12-Ir3X (X = Nb, Zr) two-phase structure have been developed as next-generation high-temperature materials. The compressive creep
behavior of Ir-Nb and Ir-Zr alloys was investigated at 2073 K under 137 MPa. The effect of addition of the third element,
Zr, on the creep behavior of an Ir-Nb alloy was also investigated at 2073 K for 137 MPa. The creep rate became two orders
lower by addition of a small amount of Zr. The lattice misfit change between the fcc and L12 two phase by addition of Zr and the deformation structure in binary and ternary alloys after a creep test were also investigated.
The creep behavior is discussed in terms of the lattice misfit, precipitate shape, and their distribution.
This article is based on a presentation made in the symposium entitled “Beyond Nickel-Base Superalloys,” which took place
March 14–18, 2004, at the TMS Spring meeting in Charlotte, NC, under the auspices of the SMD-Corrosion and Environmental Effects
Committee, the SMD-High Temperature Alloys Committee, the SMD-Mechanical Behavior of Materials Committee, and the SMD-Refractory
Metals Committee. 相似文献
78.
Satellite-Based Energy Balance to Assess Within-Population Variance of Crop Coefficient Curves 总被引:5,自引:0,他引:5
Masahiro Tasumi Richard G. Allen Ricardo Trezza James L. Wright 《Canadian Metallurgical Quarterly》2005,131(1):94-109
Quantifying evapotranspiration (ET) from agricultural fields is important for field water management, water resources planning, and water regulation. Traditionally, ET from agricultural fields has been estimated by multiplying the weather-based reference ET by crop coefficients (Kc) determined according to the crop type and the crop growth stage. Recent development of satellite remote sensing ET models has enabled us to estimate ET and Kc for large populations of fields. This study evaluated the distribution of Kc over space and time for a large number of individual fields by crop type using ET maps created by a satellite based energy balance (EB) model. Variation of Kc curves was found to be substantially larger than that for the normalized difference vegetation index because of the impacts of random wetting events on Kc, especially during initial and development growth stages. Two traditional Kc curves that are widely used in Idaho for crop management and water rights regulation were compared against the satellite-derived Kc curves. Simple adjustment of the traditional Kc curves by shifting dates for emergence, effective full cover, and termination enabled the traditional curves to better fit Kc curves as determined by the EB model. Applicability of the presented techniques in humid regions having higher chances of cloudy dates was discussed. 相似文献
79.
Nobuyoshi Koshino Masayuki Harada Yasuji Morita Toshiaki Kiikuchi Yasuhisa Ikeda 《Progress in Nuclear Energy》2005,47(1-4):406-413
We have developed a simple reprocessing process for spent FBR fuels using N-cyclohexyl-2-pyrrolidone (NCP) which has selective precipitation ability for UO22+ ions. It was confirmed that NCP has sufficient precipitation ability for UO22+ ions, decontamination capability (separation of UO22+ from simulated fission products), and resistance to γ-ray radiation in nitric acid solutions. These findings indicate that NCP is applicable to our reprocessing process. We have also evaluated performances of other precipitants such as N-n-propyl-2-pyrrolidone (NProP), N-n-butyl-2-pyrrolidone (NBP), and N-n-butyl-2-pyridone (NBPyr). It was found that higher decontamination factors (DFs) are obtained by using NProP and NBP. This can be interpreted that the hydrophobicity of NProP and NBP is lower than that of NCP. Furthermore, we have obtained an experimental result that the resistance of NBPyr to γ-ray radiation is superior to that of NCP. 相似文献
80.
A simultaneous detecting circuit system of centers and lengths of some lines in one dimension is presented applying an electronic circuit model of the nervous axon with respect to signal transmission. This model consists of series of one basic section, and has functions of Neuristor. The circuit system has a paralell processing function. It is constructed by three layers. In the first layer each visual signal of lines is changed to electric pulse signal. In the second layer edges of each line are detected, and in the third layer these detected signals are converted into voltages which correspond to lengths of the lines. These functions were confirmed experimentally using its hardware. 相似文献