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91.
Okihashi M Kitagawa Y Akutsu K Obana H Hori S 《Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan》2002,43(6):389-393
Residues of 17 pesticides in agricultural products were determined by LC/MS with an atmospheric pressure chemical ionization (APCI) interface in both positive and negative ion modes. Pesticides were extracted with acetonitrile, and the extracts were cleaned-up with a primary and secondary amine (PSA) mini-column eluted with acetone-hexane (1:1). Rice, orange and potato were spiked with the 17 pesticides at 0.1 microgram/g and analyzed by the proposed method. The average recoveries of these pesticides usually ranged from 70 to 98% and the relative standard deviations were usually around 10%. These results suggested that LC/MS with APCI could be used to determine the residue levels of the 17 pesticides in these crops. 相似文献
92.
Chien DN Tanaka M Tanaka K 《Journal of the Optical Society of America. A, Optics, image science, and vision》2002,19(8):1649-1657
The scattering phenomenon from an arbitrary-shaped end of a asymmetrical slab waveguide for the cases of TE and TM guided modes is simulated by means of boundary integral equations that are called guided-mode extracted integral equations. The integral equations that we derive can be solved by the conventional boundary-element method. Numerical results are presented for problems of three-layer asymmetrical waveguides with tilted ends. The reflection coefficient, reflected and scattered powers, and radiation patterns are calculated numerically for the cases of incident TE and TM guided modes. 相似文献
93.
Samura K Hashimoto S Kawasaki M Hayashida A Kagi E Ishiwata T Matsumi Y 《Applied optics》2002,41(12):2349-2354
Two optical methods, cavity ring-down spectroscopy and photoacoustic spectroscopy, are applied to the measurement of the isotope ratio 18O/16O in water-vapor samples with a Nd3+:YAG pumped-dye laser. The combination band of (2v1 + v3) in the 960-nm region of water molecules is investigated for two standard water samples, the Vienna Standard Mean Ocean Water and the Standard Light Antarctic Precipitation. The results demonstrate that the two methods have the potential of compact systems for in-situ measurements of H2O isotope ratio in the environment. 相似文献
94.
Kimura M 《Neural computation》2002,14(12):2981-2996
This article extends previous mathematical studies on elucidating the redundancy for describing functions by feedforward neural networks (FNNs) to the elucidation of redundancy for describing dynamical systems (DSs) by continuous-time recurrent neural networks (RNNs). In order to approximate a DS on R(n) using an RNN with n visible units, an n-dimensional affine neural dynamical system (A-NDS) can be used as the DS actually produced by the above RNN under an affine map from its visible state-space R(n) to its hidden state-space. Therefore, we consider the problem of clarifying the redundancy for describing A-NDSs by RNNs and affine maps. We clarify to what extent a pair of an RNN and an affine map is uniquely determined by its corresponding A-NDS and also give a nonredundant sufficient search set for the DS approximation problem based on A-NDS. 相似文献
95.
The fundamental goal of the GeoVISTA Studio project is to improve geoscientific analysis by providing an environment that operationally integrates a wide range of analysis activities, including those both computationally and visually based. Improving the infrastructure used in analysis has far-reaching potential to better integrate human-based and computationally based expertise, and so ultimately improve scientific outcomes. To address these challenges, some difficult system design and software engineering problems must be overcome.This paper illustrates the design of a component-oriented system, GeoVISTA Studio, as a means to overcome such difficulties by using state-of-the-art component-based software engineering techniques. Advantages described include: ease of program construction (visual programming), an open (non-proprietary) architecture, simple component-based integration and advanced deployment methods. This versatility has the potential to change the nature of systems development for the geosciences, providing better mechanisms to coordinate complex functionality, and as a consequence, to improve analysis by closer integration of software tools and better engagement of the human expert. Two example applications are presented to illustrate the potential of the Studio environment for exploring and better understanding large, complex geographical datasets and for supporting complex visual and computational analysis. 相似文献
96.
Ryosuke Ueyama Masahiro Harada Tamotu Ueyama Takashi Yamamoto Tadashi Shiosaki Kiyoshi Kuribayashi Kunihito Koumoto Won Son Seo 《Journal of Materials Science: Materials in Electronics》2000,11(2):139-143
Ultrafine BaTiO3 particles were prepared by a micro-emulsion charring (MEC) method. The MEC method consisted of two steps. The first step is the preparation of a water/oil micro-emulsion with BaTiO3 elements, and the second is a low temperature firing process in N2 atmosphere, which includes charring of oil in an emulsion and powdering BaTiO3 particles with the char. The char formed around BaTiO3 particles prevents an agglomeration of BaTiO3 particles during firing. In the present experiment, the W/O ratio and the amount of emulsifier greatly influenced the size of droplets of the emulsion. The charring temperature was another important experimental factor in order to obtain the desired BaTiO3 particles. The finally obtained BaTiO3 charring powders were monodispersed spherical particles and the particle size was 0.1 m to 0.5 m. 相似文献
97.
98.
H Takenaka T Yoneda Masahiro YA Fu A Kobayashi M Ikuno K Tsukaguchi Y Okamoto C Yamamoto N Narita 《Canadian Metallurgical Quarterly》1998,36(8):653-658
In this study we utilized bioelectrical impedance analysis (BIA) to compare the body composition of 36 stable pulmonary emphysema (PE) patients with 19 healthy controls. We compared the PE patients and healthy controls in terms of fat-free mass (FFM) and body fat (BF) as percentages of ideal body weight (FFM/IBW, BF/IBW). FFM/IBW and BF/IBW were significantly lower in the PE patients than in the controls (75.0 +/- 9.8% vs. 85.2 +/- 7.3%, p < 0.001 and 11.8 +/- 6.4% vs. 16.7 +/- 7.7%, p < 0.05, respectively). We divided the PE patients into two subgroups according to FFM, then investigated the relationships between FFM and skeletal muscle strength, and between FFM and respiratory muscle strength. In patients with reduced FFM (FFM < 43.5 kg) grip strength as an index of skeletal muscle strength was significantly lower than in patients without reduced FFM (FFM > or = 43.5 kg) (25.7 +/- 7.8 kg vs. 36.2 +/- 7.2 kg, p < 0.005). As indexes of respiratory muscle strength, maximal expiratory pressure (PEmax) and maximal inspiratory pressure (PImax) were lower in the patients with reduced of FFM, but not to a statistically significant degree (49.6 +/- 20.8 cm H2O vs. 58.7 +/- 23.9 cm H2O and 40.5 +/- 19.2 cm H2O vs. 50.2 +/- 22.1 cm H2O, respectively). In the PE patients, FFM correlated closely with vital capacity (r = 0.528, p < 0.001), forced vital capacity (FVC) (r = 0.531, p < 0.001), FEV1.0 (r = 0.554, p < 0.001), FEV1.0/FVC (r = 0.467, p < 0.005), RV/TLC (r = -0.395, p < 0.05), DLco (r = 0.770, p < 0.001), and DLco/VA (r = 0.622, p < 0.001). However no correlation was observed between BF and any of the measures of lung function. The findings of our study suggest that FFM correlates with skeletal muscle strength, respiratory muscle strength and some measures of lung function in patients with PE, and that assessments of body composition are valuable to their clinical management. 相似文献
99.
Miyuki Hayashi Masahiro Susa Toshio Maruyama Kazuhiro Nagata 《Journal of Electronic Materials》1995,24(8):983-989
The annealing of 20CaO·20SiO2·7Fe2O3·6FeO glasses at 973K in vacuo produced clusters of iron oxide, the shape of which was nearly spherical and the diameter distributed in the narrow range 25–115Å. The phase of clusters was identified to be Fe3+(Fe3+ poststagger|1.30Fe2+ poststagger|0.55V0.15)·O4 in the inverse spinel structure based upon the Mössbauer spectra and x-ray diffraction profiles. The clusters exhibited superparamagnetism and their effective anisotropy energy constant was inversely proportional to the cluster diameter. The magnetization of the glasses measured by a vibrating sample magnetometer was 7.2 × 10-6 Wbmkg-1 at 10 kOe at room temperature and smaller than the value calculated assuming that the whole clusters have superparamagnetism. These results suggest the pinning of spins near the cluster surface. 相似文献
100.
Masahiro Sugaya Masakazu Takeshi Tomoji Yamashiki Toshio Oikawa Kan-Ichi Fujii 《Electromagnetic Compatibility, IEEE Transactions on》1982,(1):20-25
Correlation of light emission, discharge structure, waveform of the discharge current, electrode configuration, and electromagnetic radiation is examined with the intent of obtaining an effective means for preventing electromagnetic interference (EMI) due to a short-gap discharge. The electromagnetic radiation (EMR) level resulting from a current step which, in turn, was formed by a discrete movement of a cathode spot was clearly recognized. A combination of needle rotor and needle post gave the smallest electromagnetic radiation level in the experiments. 相似文献