二氧化硅基多孔块材的制备及其热稳定性

以非离子型表面活性剂P123和三甲基苯的微乳液为模板剂合成介孔SiO2粉体.以此粉体为原料,经干压成型、烧结制备多孔SiO2块材.分别用AlOOH溶胶和TiO2溶胶包覆多孔SiO2粉体,制成多孔SiO2/Al2O3块材和SiO2/TiO2块材.采用XRD、SEM、TEM、N2吸附法和阿基米德排水法对所制粉体和块材进行了表征,并研究了块材的热稳定性.结果表明,600～700℃烧结的多孔SiO2基块材的孔隙率为74%～76%.与多孔SiO2块材相比,在800～1000℃范围内,SiO2/Al2O3块材的热稳定性显著提高,SiO2/TiO2块材的热稳定性在800～900℃范围内有一定改善.     

A Rate-Dependent Crystal Plasticity Analysis of Orientation Stability in Biaxial Tension of Magnesium

The development of texture during plastic deformation plays an important role in determining the stretch formability of magnesium alloy sheets.In this study,the orientation stability during equibiaxial tension of magnesium was analyzed based on three dimensional lattice rotations calculated by using a rate-dependent crystal plasticity model and assuming five different combinations of slip modes.The results show that no orientations can satisfy the stability criteria with both zero rotation velocity and convergent orientation flow in all dimensions.However,relatively stable orientations with zero rotation velocity and an overall convergence are found.They are featured by characteristic alignments of specific crystallographic directions in the macroscopic axis of contraction,depending on the slip modes involved in the deformation.It is also shown that the orientation stability varies significantly with the deviation of deformation mode from equibiaxial tension.The simulation results are briefly discussed in comparison with pre-existing experiments.     

TiN/NbN纳米多层薄膜的交变应力场和超硬效应

为了研究纳米多层薄膜的超硬效应 ,采用反应溅射法制备从 1 4nm至 2 7nm不同调制周期的一系列TiN/NbN纳米多层膜。高分辨电子显微镜对薄膜的调制结构和界面生长方式的观察发现 ,TiN/NbN膜具有很好的调制结构 ,并呈现以面心立方晶体结构穿过调制界面外延生长的多晶超晶格结构特征。显微硬度测量表明 ,TiN/NbN纳米多层膜存在随调制周期变化的超硬效应。薄膜在调制周期为 8 3nm时达到HK39 0GPa的最高硬度。分析认为 ,两种不同晶格常数的晶体外延生长形成的交变应力场 ,对材料有强化作用 ,这是TiN/NbN纳米多层膜产生超硬效应的主要原因     

Morphology Control and Optical Absorption Properties of Ag Nanoparticles by Ion Implantation

Ion implantation is a powerful method for fabricating nanoparticles in dielectric.For the actual application of nanoparticle composites,a careful control of nanoparticles has to be achieved.In this letter,the size,distribution and morphology of Ag nanoparticles are controlled by controlling the ion current density,ion implantation sequence and ion irradiation dose.Single layer Ag nanoparticles are formed by Ag+ion implantation at current density of 2.5μA/cm2.By Ag and Cu ions sequential implantation,the siz...     

Synthesis of C_f/TiAl_3 Composite by Infiltration-In Situ Reaction

Infiltration-in situ reaction synthesis of Cf /TiAl3 composite was investigated. The as-cast material was obtained by titanium particles, carbon fibers and pure aluminum. Titanium particles and carbon fibers were mixed and pressed to form a preform firstly, and then molten pure aluminum was pressed into the preform, subsequently, cooled rapidly. In situ reaction samples were obtained by heating the as-cast material from 600 to 1000 °C for 1 h. The microstructural evolution of in situ reaction samples was an...     

Microstructure and Properties of Spray Deposited 2024-20Si-5Fe Alloy

In this paper, a rapidly solidified Al-Si-Fe-Cu-Mg alloy was prepared by spray deposition. The microstructure of the alloy includes silicon phase and δ-(Al,Fe,Si). Al8Si6Mg3Fe, FeAl2 and small FeSi2 phases. The reasons of the formation of silicon and δ-(Al,Fe,Si) phase were analyzed. The tensile properties at the temperatures of room to 350℃ were investigated, and the strengthening mechanism was suggested. The wear resistance and cutability of the alloy were measured as well.     

铠装热电偶分流误差模型与实验

铠装热电偶在高温使用时,常出现电分流而影响测量精度,本工作进行了以下研究：（１）热电偶分流模拟实验;（２）分流误差数学模型及计算公式;（３）影响分流误差因素分析。     

MH/Ni电池用泡沫式镍正极的进展

本文综述了近几年来有关Ni(OH)_2的制备、物理和化学性质以及对Ni(OH)_2电极活性有重要影响的添加剂方面的研究与应用的新进展,介绍了泡沫式镍电极的制备方法,探讨了获得高性能泡沫镍电极的工艺途径,指出当前我国泡沫镍电极产业化过程中存在的一些问题,并就泡沫镍及其电极的未来发展提出了一些看法。     

太赫兹波段电磁超介质的应用及研究进展

太赫兹波和电磁超介质是电磁学领域关注的热点.太赫兹波与电磁超介质相互作用可以实现对太赫兹波的操纵和调控,有望填补"太赫兹空白".介绍了太赫兹波段电磁超介质的研究进展,包括电磁超介质电磁性能可调谐的实施途径,电磁超介质在太赫兹功能器件方面的应用(调制器/开关、传感器/探测器、滤波器、偏振元件和吸波器),太赫兹波段表面等离...     

激光防护塑料材料的研制

对激光吸收剂IR10 60、5 3 0、5 80的激光吸收进行了比较,并确定其在材料中的比例。以聚碳酸酯为基材,搀杂激光吸收剂IR10 60、5 3 0、5 80制备了防波长为5 3 0nm和10 60nm激光、眩光的激光防护材料,并对其光学密度、抗激光能量损伤、可见光透过率和物理性能进行了测试,分析了激光吸收剂IRl0 60、5 3 0、5 80在材料中所占比例对其力学性能的影响。结果表明激光吸收剂的加入能提高材料的抗冲击强度。且比例的多少对材料的力学性能没明显影响,所制得的激光防护材料完全可以满足防激光、眩光的要求。