Sol-Gel Synthesis of Palladium-Doped Silica Nanocomposite Fiber Using Triton X-100 Micelle Template and the Application for Hydrogen Gas Sensing

Palladium-doped silica nanocomposites were synthesized via a sol-gel technique combined with a template of Triton X-100 micelle. The freshly prepared sol sample of Pd-doped silica nanocomposites was investigated by TEM. Determined from the TEM image, the sizes of the Pd nanoparticles are narrowly distributed, which are around 30 nm in diameter. The prepared sol solution of the sample was injected into a Tygon Microbore Autoanalysis tubing. After 14 days gelatinization, a transparent porous optical fiber was obtained. The response of the fiber to hydrogen gas was tested by using a fiber-optic spectrometric method. The palladium-doped silica nanocomposite fiber is sensitive upon exposure to hydrogen gas and the response is reversible. This palladium-doped silica nanocomposite fiber can be applied as a new kind of hydrogen gas sensor     

糖化酶制剂辐照性能研究

研究了工业糖化酶制剂经辐照处理后各项性能的变化。结果表明,经2kGy以下剂量的γ射线处理后,可提高其贮存稳定性,改善卫生品质,不影响其正常使用。     

石油系油浆与煤系闪蒸油的焦化性能——I．热解条件的影响

通过偏光显微镜观察了石油系油浆（LH）与煤系闪蒸油（SN）焦化后所得焦块的光学结构。结果表明，在较宽条件下两种原料单独焦化均得不到取向度高的流线型结构。将两种原料以一定比例混合后先热解丙焦化所得焦块的光学结构明显好于二者混合后直接焦化所得焦块的光学结构，其中LH和SN以3：2的重量比混合后在440℃、1MPa下热解3．5h然后再在530℃、1MPa下焦化8h所得焦块为具有较高取向度的流线型结构，适合于作为针状焦的起始原料。     

北京谱仪端盖簇射计数器工作气体的研究

为使北京谱仪端盖族射计数器更好地工作在自猝灭流光ＳＱＳ模式下，提高其能量分辨以及线性等指标，用Ａｒ，ＣＯ２，Ｌｓｏｂｕｔａｎｅ三元工作气体对探测器的工作性能进行了仔细研究，找出了一适合于主雇地数器的工作气体，此外，还研究了异丁的纯度对探测器性能的影响。     

辐射制备缓释抗癌药阿糖胞苷的研究

报告了甲基丙烯酸酯类在室温下进行辐射聚合制备缓释抗癌药阿糖胞苷（Ａｒａ－Ｃ）的研究结果。结果表明，不仅亲水性单体，而且疏水性单体（包括ＭＭＡ、ＥＭＡ和ＢＭＡ等）都可用于辐射固化。加入到亲水性基质中的疏水性单体可以延缓药物的离体释放，其顺序是ＭＭＡ＜ＥＭＡ＜ＢＭＡ，央ＭＭＡ－ＨＥＭＡ共聚物中，Ａｒａ－Ｃ释放率随着基质中的ＭＭＡ含量增加而降低。药物的离体释放还受许多困素的控制，结果显示：药物释放量随着     

Ka-band solid-state pulsed Gunn oscillator and power combiner

GaAs Gunn diodes were fabricated for pulse source application at 8 mm wave band and operated with pulsewidths of 0.05 to 2.0 microseconds and duty cycles of 0.001 to 0.01. Peak pulse output power levels of 0.8–1.2W are achieved and the maximum available power is 1.6W with the highest efficiency of 6.5 percent. A simple and compact pulsed power combiner is also given in this paper.     

27keV Ar~+斜入射时的Cu-Au合金溅射实验角分布

用27keV Ar~+分别在垂直和倾斜入射情况下,轰击了Cu-Au(30wt％)合金样品,测量了Cu和Au原子的溅射角分布。角分布是用卢瑟福背散射(RBS)技术分析Al捕获膜上的Cu-Au沉积成分而定量得到的。结果表明:(1)在Ar~+倾斜(θ=40°)入射时,Cu原子择优发射,且程度比垂直入射(θ_r=O°)时增强:(2)倾斜入射时,Cu原子的角分布显示出在接近于样品表面法线方向的发射角范围内(θ<45°),发射机率比垂直入射时减小。     

A vectorial boundary element method analysis of integrated optical waveguides

In this paper, a new vectorial boundary element method is introduced and applied to the modal analysis of dielectric waveguides with piecewise homogeneous refractive indexes. The procedure, which is free of spurious modes, determines the full field distribution from the longitudinal fields at the refractive index boundaries. Singular kernels are evaluated through series solutions while the electric field discontinuity at corners is accommodated through either a grid refinement technique or a semianalytic approach. Our formalism generates propagation constants and modal field distributions for several representative refractive index profiles with far higher accuracy than standard finite-difference or finite-element procedures.