Characterization of micromachined ultrasonic transducers using light diffraction tomography

This paper demonstrates that light diffraction tomography can be used to measure the acoustic field of micromachined ultrasonic transducers (MUT) in cases in which standard methods like hydrophone and microphone measurements fail. Two types of MUTs have been characterized with the method, one air-coupled capacitive MUT (cMUT) and one waterloaded continuous wave (CW) miniature multilayer lead zirconate titanate (PZT) transducer. Light diffraction tomography is an ultrasound measurement method with some special characteristics. Based on the interaction of light and ultrasound, it combines light intensity measurements with tomography algorithms to produce a measurement system. The method offers nonperturbing pressure measurements with high spatial resolution. It has been shown that, under certain circumstances, light diffraction tomography can be used as an absolute pressure measurement method with accuracy in the order of 10% in water and 13% in air. The results show that air-coupled cMUTs in the frequency range of about 1 MHz as well as the extreme near field of a miniaturized CW 10 MHz water-loaded transducer were successfully characterized with light diffraction tomography.     

Charge trapping in carbon nanotube loops demonstrated by electrostatic force microscopy

Electronic devices made from carbon nanotubes (CNTs) can be greatly affected by substrate charges, which, for instance, induce strong hysteresis in CNT field effect transistors. In this work, electrostatic force microscopy (EFM) is employed to investigate single-walled nanotubes grown by chemical vapor deposition on SiO2 substrates. We demonstrate the use of this technique to gain quantitative information on the substrate charges. It is found that charge pools with densities around 10(-8) C/cm2 can be trapped inside nanotube loops for extended periods of time, showing that nanotubes can act as confining barriers for substrate charges. The trapped charges can be removed by scanning probe manipulation.     

Electrical transport through a single nanoscale semiconductor branch point

Semiconductor tetrapods are three-dimensional (3D) branched nanostructures, representing a new class of materials for electrical conduction. We employ the single-electron transistor approach to investigate how charge carriers migrate through single nanoscale branch points of tetrapods. We find that carriers can delocalize across the branches or localize and hop between arms depending on their coupling strength. In addition, we demonstrate a new single-electron transistor operation scheme enabled by the multiple branched arms of a tetrapod: one arm can be used as a sensitive arm-gate to control the electrical transport through the whole system.     

Tunable double quantum dots in InAs nanowires defined by local gate electrodes

We report on low-temperature transport measurements on single and double quantum dots defined using local gates to electrostatically deplete InAs nanowires grown by chemical beam epitaxy. This technique allows us to define multiple quantum dots along a semiconducting nanowire and tune the coupling between them.     

An integrated analysis of ergonomics and time consumption in Swedish 'craft-type' car disassembly

Car disassembly is at the edge of extensive rationalization due to increased legislative demands for recycling. This study focused on (1) assessing current mechanical exposures (physical work loads) for comparison with future rationalised systems, with particular emphasis on time aspects, (2) analysing disassembly work in terms of time consumption and exposures in constituent tasks as defined by a loss analysis technique, and (3) predicting the consequences of car disassembly rationalisation for mechanical exposures. The study showed that disassembly implied pronounced circulatory loads, and that more walking and higher lumbar peak loads were found than in studies of assembly work. Value-adding tasks comprised 30% of the total working time, and implied higher postural exposures for the head, arm, trunk and wrist, as well as less opportunities to recover, as compared to non-value-adding tasks. Organisational-type rationalization can be expected to increase the time spent in value-adding work, thus increasing local exposures for the average worker, while a concurrent increase in mechanization level might reduce circulatory exposures, the amount of walking, and peak lumbar loads.     

Multivalent HSA conjugates of 3'-sialyllactose are potent inhibitors of adenoviral cell attachment and infection

Adenoviruses of serotypes 8, 19 and 37 are the major cause of the severe eye infection EKC (epidemic keratoconjunctivitis). In general, all adenoviruses interact with their cellular receptors through the fibre proteins, which extend from the virus particle. Recently, adenovirus type 37 (Ad37) was found to bind and infect human corneal cells through attachment to carbohydrate structures that carry terminal alpha-(2-3)-linked sialic acids. Herein we present a synthetic route to a 3'-sialyllactose derivative and corresponding multivalent HSA conjugates with varying orders of valency. The potential of these compounds as inhibitors of EKC-causing adenovirus of serotype Ad37, was studied with both a binding assay and an infectivity assay. The results revealed that these compounds effectively prevent Ad37 from binding to and infecting human corneal epithelial (HCE) cells. Moreover, the inhibition is significantly increased with higher orders of multivalency.     

Influence of sous vide processing, steaming and boiling on vitamin retention and sensory quality in broccoli florets

In this study the effect of sous vide processing, steaming and traditional boiling of broccoli florets on retention of ascorbic acid, vitamin B₆ and folacin was investigated. Freshly prepared samples were also sensorily evaluated. In all heat treatments ascorbic acid was found to have the highest retention, and was therefore judged not to be suitable as an indicator for vitamin retention in general. When the three types of heat treatment were compared, boiling showed lowest retention of all the vitamins examined (45–64% in 5 min), whereas sous-vide processing gave the highest retentions (97–100% in 5 min). Retentions during steaming were a little lower (83–100% in 5 min). Sensory evaluation showed that sous-vide cooked and steamed broccoli florets generally had higher acceptability than boiled.

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Bedeutung des Sous-Vide-Kochens, Dämpfens und des üblichen Kochens für die Vitaminerhaltung und die sensorische Qualität in Broccoli-Sträußchen

Zusammenfassung Bei dieser Untersuchung wurde untersucht, in welchem Ausmaß das Sous-Vide-Kochen, Dämpfen und das übliche Kochen von Broccoli-Sträußchen einen Einfluß auf die Retention der Ascorbinsäure bzw. Vitamin-B₆ und Folsäure hat. Frisch hergestellte Proben wurden ebenfalls sensorisch beurteilt. Bei allen Arten der Wärmebehandlung ergab sich, daß die Ascorbinsäure die höchste Retention hatte und daher als ungeeigneter Indikator einer Vitaminretention im allgemeinen ist. Bei Vergleich der drei Arten der Wärmebehandlung hat sich erwiesen, daß das Kochen die niedrigste Retention aller geprüften Vitamine (45–64% in 5 min) ergab, das Sous-Vide-Kochen dagegen die höchste Retention (97–100% in 5 min). Beim Dämpfen war die Retention etwas niedriger (83–100% in 5 min). Die sensorischen Bewertungen zeigten, daß sous-vide-gekochte sowie gedämpfte Broccoli-Sträußchen allgemein von besserer Qualität waren als die gekochten.

     

Ghanaian Cocoa Bean Fermentation Characterized by Spectroscopic and Chromatographic Methods and Chemometrics

Abstract: Export of cocoa beans is of great economic importance in Ghana and several other tropical countries. Raw cocoa has an astringent, unpleasant taste, and flavor, and has to be fermented, dried, and roasted to obtain the characteristic cocoa flavor and taste. In an attempt to obtain a deeper understanding of the changes in the cocoa beans during fermentation and investigate the possibility of future development of objective methods for assessing the degree of fermentation, a novel combination of methods including cut test, colorimetry, fluorescence spectroscopy, NIR spectroscopy, and GC-MS evaluated by chemometric methods was used to examine cocoa beans sampled at different durations of fermentation and samples representing fully fermented and dried beans from all cocoa growing regions of Ghana. Using colorimetry it was found that samples moved towards higher a* and b* values as fermentation progressed. Furthermore, the degree of fermentation could, in general, be well described by the spectroscopic methods used. In addition, it was possible to link analysis of volatile compounds with predictions of fermentation time. Fermented and dried cocoa beans from the Volta and the Western regions clustered separately in the score plots based on colorimetric, fluorescence, NIR, and GC-MS indicating regional differences in the composition of Ghanaian cocoa beans. The study demonstrates the potential of colorimetry and spectroscopic methods as valuable tools for determining the fermentation degree of cocoa beans. Using GC-MS it was possible to demonstrate the formation of several important aroma compounds such 2-phenylethyl acetate, propionic acid, and acetoin and the breakdown of others like diacetyl during fermentation. Practical Application: The present study demonstrates the potential of using colorimetry and spectroscopic methods as objective methods for determining cocoa bean quality along the processing chain. Development of objective methods for determining cocoa bean quality will be of great importance for quality insurance within the fields of cocoa processing and raw material control in chocolate producing companies.     

Preparation of thermoset composites from natural fibres and acrylate modified soybean oil resins

Structural composites with a high content of renewable material were produced from natural fibres and an acrylated epoxidized soybean oil resin. Composites were prepared by spray impregnation followed by compression moulding at elevated temperature. The resulting composites had good mechanical properties in terms of tensile strength and flexural strength. Tensile testing as well as dynamical mechanical thermal analysis showed that increasing the fibre content, increased the mechanical properties. The resin can be reinforced with up to 70 wt % fibre without sacrifice in processability. The tensile modulus ranged between 5.8 and 9.7 GPa depending on the type of fibre mat. The study of the adhesion by low vacuum scanning electron microscopy shows that the fibres are well impregnated in the matrix. The aging properties were finally evaluated. This study shows that composites with a very high content of renewable constituents can be produced from soy bean oil resins and natural fibres. © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2009