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11.
Initial geopolymeric reaction processes governing dissolution of solid aluminosilicate particles in alkali solutions have
been investigated using conventional experimental techniques, and the data analysed by speciation predictions of the partial
charge model (PCM). For metakaolin powders activated with 5.0 M NaOH, solid-state nuclear magnetic resonance (NMR) spectra
disclose the existence of monomeric [Al(OH)4]− species after two hours of dissolution, consistent with PCM predictions. However, no equivalent monomeric silicate species
were observed for 5.0–10.0 M NaOH activator solutions characteristic of systems with nominal Si/Al ≤ 1. The apparent absence
of monomeric silicate species suggest rapid condensation of silicate units with [Al(OH)4]− to generate aluminosilicate species, as indicated by the evolution of the shoulder at around −87 ppm in the 29Si NMR spectra. Of the two possible stable silicate species [SiO2(OH)2]2− and [SiO(OH)3]−, the latter appears most likely to condense with [Al(OH)4]− to produce aluminosilicate oligomers, from which larger oligomers subsequently form through further condensation with [Al(OH)4]− leading to a gradual build up of aluminosilicate networks and a lowering of system alkalinity. This dissolution and hydrolysis
sequence at the early stages of synthesis suggests a reaction path wholly consistent with predictions of the partial charge
model. 相似文献
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缓蚀技术是减轻石油化学工业中各类油、气、水储罐内腐蚀的有效方法,但国内目前应用尚不普遍,原因之一是尚未找到较适宜的加入方法,使缓蚀剂的应用可以经济地和长时间地起作用,本文综述了储罐内缓蚀剂的各种应用技术,重点介绍在涂层中加缓蚀剂的技术,基于其溶解性或离子置换特性,在实际使用时缓蚀剂可持久、稳定地释放出来。这后一类技术可能是在储罐内应用缓蚀剂的最好方式之一。 相似文献
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Pressures produced during a final impression have been discussed from the standpoint of where they should be applied and where they should be reduced. Areas of the edentulous mouth requiring little pressure are: the palate, residual ridges, and areas of easily displaced gingiva. More pressure is needed in the border seal, on the buccal shelf, and against the retromylohyoid fossa. A clear processed acrylic resin tray with escape holes has been shown to meet the requirements for selective pressure application. Zinc oxide paste is the final impression material of choice in most instances. 相似文献
18.
Qing-Huo Liu Anderson B. Weng Cho Chew 《Geoscience and Remote Sensing, IEEE Transactions on》1994,32(3):494-498
The authors formulate and implement a numerical mode-matching (NMM) method to model electrode-type resistivity tools in invaded thin beds. The authors derive the low-frequency approximation of the Maxwell's equations to obtain the partial differential equation for the potential field. The new NMM program is validated by comparing the numerical results with those obtained from other dc programs. It is found that this new program is much faster than the program using the finite-element method (FEM), and hence is useful for routine interpretation of resistivity logs and for inversion 相似文献
19.
The effect of tetramethylammonium cations (TMA+) on TiO2 crystal morphology in hydrothermal conditions has been studied. The as-synthesized samples were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM) and scanning electron microscopy (SEM) methods. The morphologies including besom-like particle, nanosheet and nanotube have been observed. The different ways TMA+ cations in the hydrothermal bases affect the crystal growth manner are suggested to be responsible for the different morphologies of the as-synthesized samples. 相似文献
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