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121.
Two AlMnZn alloys in melt-spun condition have been studied by transmission electron microscopy. The Al24Mn5Zn alloy was found to be fully icosahedral, while the Al12Mn2.9Zn alloy gave rise to decagonal quasicrystal. The decagonal phase grew in clusters with an orientation relationship between the grains suggesting nucleation on an icosahedral seed. On annealing at 500–600°C, the quasicrystalline phase transformed to a body centered orthorhombic phase L (a = 1.24, b = 1.26 andc = 3.05nm) with a high density of planar defects. This phase transforms to an ordered and defect free monoclinic phase M, a superlattice structure of L (a = c = 1.77, b = 3.05nm and β = 89.1°). The L phase is shown to be a rational approximant of the icosahedral phase. The interrelationship among quasicrystalline phases and their rational approximants in AlMnZn system are highlighted. 相似文献
122.
Jogender Singh Douglas E. Wolfe 《Journal of Materials Engineering and Performance》2005,14(4):448-459
Fabrication of cost-effective, nano-grained net-shaped components has brought considerable interest to Department of Defense,
National Aeronautics and Space Administration, and Department of Energy. The objective of this paper is to demonstrate the
versatility of electron beam-physical vapor deposition (EB-PVD) technology in engineering new nanostructured materials with
controlled microstructure and microchemistry in the form of coatings and net-shaped components for many applications including
the space, turbine, optical, biomedical, and auto industries. Coatings are often applied on components to extent their performance
and life under severe environmental conditions including thermal, corrosion, wear, and oxidation. Performance and properties
of the coatings depend upon their composition, microstructure, and deposition condition. Simultaneous co-evaporation of multiple
ingots of different compositions in the high energy EB-PVD chamber has brought considerable interest in the architecture of
functional graded coatings, nano-laminated coatings, and design of new structural materials that could not be produced economically
by conventional methods. In addition, high evaporation and condensate rates allowed fabricating precision net-shaped components
with nanograined microstructure for various applications. Using EB-PVD, nano-grained rhenium (Re) coatings and net-shaped
components with tailored microstructure and properties were fabricated in the form of tubes, plates, and Re-coated spherical
graphite cores. This paper will also present the results of various metallic and ceramic coatings including chromium, titanium
carbide (TiC), titanium diboride (TiB2), hafnium nitride (HfN), titanium-boron-carbonitride (TiBCN), and partially yttria stabilized zirconia (YSZ) TBC coatings
deposited by EB-PVD for various applications.
This paper was presented at the International Symposium on Manufacturing, Properties, and Applications of Nanocrystalline
Materials sponsored by the ASM International Nanotechnology Task Force and TMS Powder Materials Committee, October 18–20,
2004, Columbus, OH. 相似文献
123.
Shalu Kataria Yogendra L. Verma Himani Gupta Shishir K. Singh Nitin Srivastava Ravindra Dhar 《Polymer-Plastics Technology and Engineering》2020,59(9):952-958
ABSTRACTNano-composite polymer gel electrolytes (NPGEs) based on polymer poly(vinylidene fluoride-co-hexafluoropropylene) PVdF-HFP, ionic liquid, 1-butyl-3- methylimidazolium bis(trifluoromethanesulfonyl)imide BMIMTFSI, Li-salt along with the addition of SiO2 nanoparticles have been synthesized and characterized by various techniques. Prepared NPGEs show high room temperature ionic conductivity (~10?3 S/cm) and have a wide electrochemical window (ECW) (~3.3–3.5 V). The galvanostatic charge/discharge profile was studied by sandwiching best performing NPGEs between a LiFePO4 cathode and lithium metal anode. The specific discharge capacity of the cell (Li/NPGE/LiFePO4) room temperature at 0.1C rate is found to be 138 mAh/g. 相似文献
124.
V. Shukla M. Singh D. K. Singh Ri Shukla 《Surface Coatings International Part B: Coatings Transactions》2005,88(3):217-220
Summary Over the past few years, the challenges of globalisation, consolidation and economical point of view have meant that manufacturers
of epoxy formulations have to constantly improve their capability to meet the needs of customers. An active area for advancement
is that of epoxy and polyamide resin with castor oil. Generally, people working in the coating industries are familiar with
castor oil, but this paper provides information on the new use of castor oil in epoxy and polyamide resin. This novel product
(castor oil-modified epoxy resin/castor oil-modified polyamide) provides a previously unattainable combination and improved
flexibility and toughness to a variety of ambient cure applications. This communication will review the performance of these
castor oil-modified epoxy and polyamide resin surface coatings and adhesives. Based on the results of this study, these systems
offer some advantages without much affecting the traditional properties of epoxy and polyamide resin in a variety of applications. 相似文献
125.
R. P. Singh 《Polymer Bulletin》1981,6(3-4):175-181
An investigation of the photo-oxidative degradation and stabilization of IIR and SBR in the temperature range of 258 to 313°K in air with a monochromatic light of 366 nm in the absence and presence of various concentrations of the different copper chelates has been described. The stabilizer performance in IIR and SBR was accessed by carbonyl index and quantum yield measurements. The changes of IIR and SBR during the irradiation with an ultra-violet light (366 nm) have been conducted by viscometrically and actinometric techniques. Irradiations were conducted on the films at 0, 2, 4, 6, 8, 10, 12 and 14 hours and various parameters were obtained. 相似文献
126.
Number of blends were prepared by intergrinding clinker, gypsum, fly ash, calcined clay, microsilica and limestone in laboratory ball mill in varying percentages, and their physical properties such as fineness, consistency, setting time and compressive strength have been determined. The durability tests on selected compositions were also conducted by exposing the mortar cubes separately in 5% Na2SO4 and 5% NaCl solutions till the age of 90 and 180 days. The performance was observed by compressive strength development criteria after various length of exposure. Results have been discussed and found that the durability of blended cement is higher than the ordinary Portland cement. 相似文献
127.
A comprehensive experimental investigation was performed to understand the pullout behavior of polypropylene fibers from a cementitious matrix. The effect of embedded length on the pullout characteristics, the development of the interfacial bond with age of curing of matrix and the effect of exposure to degrading environments, like seawater and salt water, on the interfacial bond between the fibers and cementitious matrix were studied. The aim of these experiments was to understand the properties of fiber/matrix interface, which are of primary significance in predicting the overall behavior of fiber-reinforced cement-based composites. Polypropylene fibers have a weak bond with cementitious matrix because of smooth surface of fibers, which does not allow for sufficient friction to develop between the two. In this study a new method to improve the frictional bond by means of mechanical indentations of fibers was also proposed. The bonding performance was characterized by means of pullout tests of the plain and modified fibers from a cementitious matrix. An optimum level of fiber modification for maximization of bond efficiency was determined experimentally. 相似文献
128.
129.
Equivalent conductances of Bu4NBPh4, Bu4NNO3, Bu4NI,KClO4, Kl, NaI, NaBPh4, Ph4PCl, LiCl, AgNO3 and CuClO4. 4AN have been measured at 25°C in binary mixtures of N,N-dimethylformamide (DMF) containing 1 mol % of 1, 1, 3, 3-tetramethylurea (TMU), dimethylsulphoxide (DMSO) and hexamethylphosphotriamide (HMPT). Such measurements for LiCl, NaI, KClO4 and CuClO4. 4AN have also been carried out in DMF and in binary mixtures of DMF containing 1 mol % pyridine (Py), α-picoline (α-Pic), β-picoline (β-Pic), γ-picoline (γ-Pic) and acetonitrile (AN). The conductance data in all the cases have been analyzed by the Shedlovsky equation. Limiting ion conductances have been obtained by the method of Fuoss et al. The actual solvated radii of ions, evaluated using limiting ion conductances show that Ag+ and Cu+ have strong preferential solvation by all solvents which have been used to prepare the binary mixtures with DMF and the preferential solvation for both Ag+ and Cu+ with HMPT, DMSO and TMU is relatively stronger than with AN and is practically of similar magnitude as with the organic bases. 相似文献
130.
Thermal behaviour of starch-graft-polyacrylamide (S-g-PAM) copolymers was evaluated. Grafting of polyacrylamide onto starch lowers the initial decomposition temperature. However, the over-all stability as assessed by the shape of thermogravimetric curve and integral procedural decomposition temperature increased with an increase in % graft-on. 相似文献