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931.
V. Kevorkijan 《Metallurgical and Materials Transactions A》2004,35(2):707-715
Semi-industrial samples of Mg AZ80/SiC/50p composites (machined bars with o.d.=80 mm and length=150 mm, having a maximum 2 vol pct of retained porosity) were successfully
fabricated by pressureless, low-pressure (under overpressure of about 0.3 MPa) and moderate-pressure (under overpressure of
about 0.8 MPa) infiltration. Pressureless infiltration was completed in 24 hours under the flowing atmosphere of nitrogen,
whereas the moderate and low-pressure infiltrations were performed under a static atmosphere of pressurized nitrogen for 7
and 0.5 hours, respectively. The composite samples obtained by all applied infiltration paths posessed a homogeneous microstructure
and superior mechanical properties as compared to the nonreinforced matrix. Due to the improved productivity of composite
fabrication in comparison with the other two infiltration paths investigated in this work, the moderate-pressure infiltration
process was recognized as the most competitive. 相似文献
932.
A. Phillion H. W. Zurob C. R. Hutchinson H. Guo D. V. Malakhov J. Nakano G. R. Purdy 《Metallurgical and Materials Transactions A》2004,35(4):1237-1242
We have evaluated controlled decarburization as a method for probing the effect of alloying elements on ferrite growth from
austenite. The technique permits the exploration of longer-time ferrite layer growth; it minimizes the effects of interface
structure on ferrite growth; and it permits the isolation of the effects of temperature and alloying element concentration
on ferrite/austenite interface motion. The study of the decarburization of initially homogeneous Fe-C-Ni alloys was complemented
by experiments using specimens with a controlled nickel concentration gradient. Although the decarburization method yields
consistent results at longer times, it is found to be less appropriate for the study of initial ferrite growth. Nucleation
in the gas/solid interface region, coupled with uncertainties about the precise time of decarburization, leads to large relative
errors at the earliest times. For these reasons, the method is considered a valuable complement to studies based on precipitation
boundary conditions.
This article is based on a presentation given in the symposium “The Effects of Alloying Elements on the Gamma to Alpha Transformation
in Steels,” October 6, 2002, at the TMS Fall Meeting in Columbus, Ohio, under the auspices of the McMaster Centre for Steel
Research and the TMS-ASM Phase Transformations Committee. 相似文献
933.
Mixtures of Cr and Mo elemental powders, with the nominal compositions Cr25Mo75, Cr50Mo50, and Cr75Mo25, are processed by high-energy ball milling at ambient temperature. Milling is observed to force the mixing of the immiscible
bcc elements Cr and Mo into solid solutions. The lattice parameter of these solid solutions, measured by X-ray diffraction
(XRD), displays the expected positive deviation from Vegard’s law. These deviations are compared to the ones predicted by
Eshelby’s inclusion model for dilute alloys. The conventional Williamson-Hall approach is shown to fail to determine the grain
size in as-milled samples, probably due to the high density of dislocations. Annealing at 700 °C for 10 hours under argon
leads to a large reduction in structural defect density, without inducing any significant decomposition. The mixing measured
in Cr-Mo is discussed in the broader context of the mechanical mixing forced by ball milling in moderately immiscible systems. 相似文献
934.
Yaojun Lin Yizhang Zhou Enrique J. Lavernia Kevin M. McHugh 《Metallurgical and Materials Transactions A》2004,35(11):3633-3635
From the geometrical standpoint, this article presents a qualitative theoretical analysis and prediction of the transient
to steady-state transition during the spray-rolling process, a novel manufacturing technique for aluminum strips. The analytical
results indicate that, when the deposited materials at the specific points on one roll surface overlap their counterparts
on the other roll surface, spray rolling transits from the transient state to the steady state. The specific points are the
limiting deposition positions of the atomized droplets on the roll surface initially. 相似文献
935.
Theoretical and experimetal methods have been developed to characterize the effect of mechanical loading on the mesoscopic
and macroscopic mechanical state of polycrystalline materials. Ferritic and austenitic single-phase materials were first analyzed,
then phase interaction was studied in a multiductile phase material (austeno-ferritic duplex steel) and a natural reinforced
composite (pearlitic steel). The theoretical method is based on the self-consistent approach in which elastic and plastic
characteristics of the phases have been applied through the micromechanical behavior of single-crystal-using slip systems
and microscopic hardening. The effects of a crystallographic texture and phase interaction during loading and after unloading
were studied. The elastic and plastic anisotropy of the grains having the same crystallographic orientation were assessed
by diffraction strain analysis. The simulation was compared with the experiments performed using the X-ray diffraction technique.
In the considered duplex and pearlitic steels, it was observed that the ferrite stress state is much lower than the austenite
and cementite ones. The results of diffraction strain distribution have showed the pertinence of the models and give valuable
information, for example, for the yield stress and the hardening parameters of each phase in a two-phase material. 相似文献
936.
T. Connolley M. J. Starink P. A. S. Reed 《Metallurgical and Materials Transactions A》2004,35(3):771-783
Notches were machined in specimens of INCONEL 718 by a broaching process, where differing broaching runs led to differing
extents of subsurface deformation and surface roughness. Fatigue tests were carried out at 600 °C with a trapezoidal loading
waveform at 0.25 Hz. The broaching process that led to the more severe subsurface deformation (but lower surface roughness)
showed the worst fatigue performance. Analysis of total strain amplitude in the notch root with the aid of an elastoplastic
finite-element (FE) model showed that the work hardening related to the subsurface deformation caused by the different broaching
can account for the difference in fatigue lives. Differences in initiation and growth behavior were seen for the two broached
finishes as well as for broached and subsequently polished samples. These differences are discussed in terms of a change in
crack growth initiation and growth mechanisms due to the presence of the work-hardened layer. 相似文献
937.
Cyclic oxidation response of multiphase niobium-based alloys 总被引:4,自引:0,他引:4
Kwai S. Chan 《Metallurgical and Materials Transactions A》2004,35(2):589-597
Cyclic oxidation tests were performed on multiphase Nb-based alloys containing silicide, Laves, and Nb solid solution phases.
In particular, the oxidation resistance of six alloys with various compositions (Nb, Ti, Hf, Cr, Ge, and Si) and microstructures
was characterized by thermal cycling from ambient temperature to a peak temperature that ranges from 900 °C to 1400 °C. Weight
change data were obtained and the corresponding spalled oxides were collected and identified by X-ray diffraction. The results
indicated that Nb-based alloys formed a mixture of CrNbO4, Nb2O5, and Nb2O5 · TiO2, with possibly small amounts of SiO2 or GeO2. The oxidation resistance was improved when CrNbO4 formed instead of Nb2O5 and Nb2O5 · TiO2. These results were used to assess the influence of microstructure and composition on the oxidation resistance of multiphase
Nb-based alloys. 相似文献
938.
Charuhas V. Thakar Orfeas Liangos JeanPierre Yared David A. Nelson Srinivas Hariachar Emil P. Paganini 《Hemodialysis international. International Symposium on Home Hemodialysis》2003,7(2):143-147
Background: Acute renal failure (ARF) after cardiac surgery is associated with significant morbidity and mortality, irrespective of the need for dialysis. Previous studies have attempted to identify predictors of ARF and develop risk stratification algorithms. This study aims to validate the algorithm in an independent cohort of patients that includes a significant proportion of female and black patients and compares two different definitions of renal outcome.
Methods: A large single center cardiac surgery database was examined (n, 24,660; 1993–2000) which included 29.9% females and 3.7% black patients. Post‐operative ARF was defined as: a) ARF requiring dialysis, b) > 50% reduction in creatinine clearance relative to baseline or requiring dialysis. Clinical variables related to baseline renal function and cardiovascular disease were used in recursive partitioning analysis for both outcome definitions. Chi‐square goodness of fit analysis was performed to validate the algorithm.
Results: The frequency of post‐operative ARF requiring dialysis ranged between 0.5 and 15.5% based on the risk categories with the area under the receiver operating characteristic (ROC) curve of 0.78. Using the more inclusive definition of ARF, the frequency was significantly higher ranging from 2.6 to 25%(P < 0.001) with an area under ROC curve of 0.65.
Conclusions: The renal risk stratification algorithm is valid in predicting post‐operative ARF in an independent cohort of patients, well represented by differences in gender and race. Since the need for dialysis remains subjective, a more objective and inclusive definition of ARF may help in identifying a larger number of patients 'at‐risk'. 相似文献
Methods: A large single center cardiac surgery database was examined (n, 24,660; 1993–2000) which included 29.9% females and 3.7% black patients. Post‐operative ARF was defined as: a) ARF requiring dialysis, b) > 50% reduction in creatinine clearance relative to baseline or requiring dialysis. Clinical variables related to baseline renal function and cardiovascular disease were used in recursive partitioning analysis for both outcome definitions. Chi‐square goodness of fit analysis was performed to validate the algorithm.
Results: The frequency of post‐operative ARF requiring dialysis ranged between 0.5 and 15.5% based on the risk categories with the area under the receiver operating characteristic (ROC) curve of 0.78. Using the more inclusive definition of ARF, the frequency was significantly higher ranging from 2.6 to 25%(P < 0.001) with an area under ROC curve of 0.65.
Conclusions: The renal risk stratification algorithm is valid in predicting post‐operative ARF in an independent cohort of patients, well represented by differences in gender and race. Since the need for dialysis remains subjective, a more objective and inclusive definition of ARF may help in identifying a larger number of patients 'at‐risk'. 相似文献
939.
The purpose of this study is to apply continuum damage mechanics – introduced through the concept of fabric tensors – to composite materials within the framework of the theory of elasticity. A directional data model of damage mechanics for composite materials will be developed using fabric tensors. The introduction of fabric tensors into the analysis of damage of composite materials will allow for an enhanced and better understood physical meaning of damage. The micromechanical approach will be used here to relate the damage effect through fabric tensors to the behavior of composite materials. In this approach, damage mechanics is introduced separately to the constituents of the composite material through different constituents’ damage effect tensors. The damaged properties of the composite system as a whole can then be obtained by proper homogenization of the damaged properties of the constituents.
The derivation of a generalized formulation of damage evolution will be shown here in a mathematically consistent manner that is based on sound thermodynamic principles. Numerical examples will be presented to show applicability. In addition, damage evolution for the one-dimensional tension case is also illustrated. 相似文献
940.
Eaton P. Ragusa A. Clavel C. Rojas C.T. Graham P. Duran R.V. Penades S. 《IEEE transactions on nanobioscience》2007,6(4):309-318
Glyconanoparticles which present carbohydrate and amino groups motifs at their surface were produced. These particles were highly stable and soluble in aqueous solutions. The presence of the carbohydrate groups also allowed the inclusion of more strongly binding groups, without affecting solubility. The binding of a model DNA, plasmid by these nanoparticles was studied by atomic force microscopy, transmission electron microscopy, and gel electrophoresis. Significant differences between the nanoparticles based on their affinities for the DNA were found, with implications for their potential use as nonviral gene delivery agents. 相似文献