Formation of texture of Ni48Mn31Ga21 polycrystalline alloy by thermal simulation pack rolling technology

1 Introduction Heusler type Ni2MnGa magnetic shape memoryalloy, which is a new kind of functional material withferromagnetism and thermoelastic martensitictransformation, attracts the interests of many people allover the world in recent years. The alloy …     

Preparation and characterization of TiO2 photoelectrode codoped with aluminum and boron and its application in dye-sensitized solar cell

Nanocrystalline titania films codoped with aluminum and boron were prepared by cathodic vacuum arc deposition. In the process, titanium alloy target was used under an O2/Ar atmosphere, and sensitization of films were carried out by natural dye-sensitized complex in anhydrous ethanol. The structure, surface morphology and UV-vis spectra of titania films codoped were measured by X-ray diffraction analysis, scanning electron microscopy and ultraviolet-visible spectrometer. Theas-deposited films are found to be amorphous. The films annealed were examinedto be of anatase structure with orientation along the (101) planes, the averagecrystal size is in the range between 41 and 45 nm. SEM results show that thereare some pores in the codoped titania films, the optical properties of the dye-sensitized films were also measured which reveals that the spectral responses of films shift to the visible region. Under simulated sunlight illumination, the overall energy conversion efficiency of dye-sensitized nanocrystalline solar cell is 0.9%.     

Experimental and numerical study of warm deep drawing of AZ31 magnesium alloy sheet

Warm forming of magnesium alloy sheet has attracted more and more attention in recent years. The formability of magnesium alloy sheet at elevated temperature depends on appropriate processes, and the fabrication of high-performance sheet. In this research, an AZ31 magnesium alloy sheet with excellent performances is fabricated by the cross-rolling and the uniform annealing treatments. The uniaxial tensile tests are conducted using a Gleeble 3500 thermal–mechanical simulator, and the mechanical properties of AZ31 magnesium alloy sheet are analyzed. Finally, some limiting drawing ratio (LDR) experiments are performed. The experiments show that the LDR can reach 2.0 at the forming temperature of 150 °C and the drawing velocity of 15 mm/s. A warm deep drawing process is also simulated by the finite element method. The influences of drawing temperature and blank holder force on the formability are numerically investigated. The simulation demonstrated that variable blank holder force technology can improve the LDR from 3.0 to 3.5, and decrease the wall thinning ratio from 15.21% to 12.35%.     

155kA预焙槽多组阳极脱落的原因及对策

通过对155kA预焙槽造成多组阳极脱落的原因分析和采取对策的总结，可作为其它容量预焙槽处理类似事故的借鉴，起到预防和杜绝此类事故发生的积极作用。     

离心铸造双金属复合辊筒技术

介绍了采用离心复合铸造方法来生产双金属铸铁辊筒的技术,通过实例阐述了确定离心工艺参数的方法以及复合辊筒内外层的整个浇注工艺过程,并探讨了在双金属复合铸铁辊筒生产中经常出现的裂纹、硬度低、结合不良和工作层厚度不足以及夹杂等铸造缺陷的产生原因,同时,提出了在生产中所应采用的防止措施.     

离心铸造高镍铬铸铁复合辊套的研制

详细介绍了离心铸造高镍铬铸铁复合辊套内外层金属铸造工艺参数及整个铸造生产过程。     

一种新型储能点焊机的研制

介绍一种新型储能点焊机，采用电容恒流充电；电容电压的比较充电控制，有触点无电流换向等项技术，获得了较好的工作效果。     

Einfluß des totvolumens auf die Al2O3-CVD-Abscheidung

The influence of the free gas volume around the substrate on the chemical vapor deposition of Al₂O₃ layers in the AlCl₃/H₂/CO₂ system at different pressures and temperatures has been studied. Through the water gas reaction which occurs homogeneously in the gas phase, the Al₂O₃ growth rate increases with increasing free gas volume until a certain volume is reached, after which it remains constant. For this ‘critical free gas volume’ a theoretical characteristic dimension L_max is introduced. It is defined as the normal distance from a substrate surface, at which the water molecules formed from the CO₂ + H₂ in the gas phase can no longer reach the substrate surface in the time available. The dependencies of L_max on pressure, temperature and gas flow rate deduced through this theoretical consideration show agreement with the experimental results.

Zusammenfassung

Der Einfluß des die Substrate umgebenden Totvolumens auf die Al₂O₃-CVD-Abscheidung im System AlCl₃/H₂/CO₂ wurde systematisch bei verschiedenen Drücken und Temperaturen untersucht. Durch die homogen in der Gasphase ablaufende Wassergasreaktion nimmt in allen Fällen die Abscheidungs-geschwindigkeit mit vergrößerten Totvolumen zuerst zu, bleibt aber ab einer bestimmten Totvolumensgröße konstant. Für diese “kritische Totvolumensgröße” wird die theoretische Kenngröße L_max eingeführt. Diese Größe ist als Normalabstand zur Substratoberfläche definiert, bei dem das in der Gasphase aus CO₂ + H₂ gebildeten Wasser in der zur Verfügung stehenden Zeit die mit AlCl₃ belegte Oberfläche der Substrate nicht mehr erreichen kann. Die aus dieser theoretischen Überlegung abgeleiteten Voraussagen über die Abhängigkeit des L_max von Druck, Temperatur und Gasströmungsgeschwindigkeit zeigten Übereinstimmung mit den Versuchsergebnissen.     

Synergistic Extraction of Rare Earth Ions by 1-phenyl-3-methyl-4-benzoyl-5-pyrazolone and Trioctylphousphine Oxide in Paraffin Wax

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浅议我国无缝钢管生产技术发展方向

介绍了我国无缝钢管生产技术现状及国内外无缝钢管产销概况。根据我国经济建设对无缝钢管的需求情况，提出了发展我国无缝钢管生产技术的设想。