Ozonation of CI Reactive Black 5 using rotating packed bed and stirred tank reactor

This study investigates the ozonation of CI Reactive Black 5 (RB5) by using the rotating packed bed (RPB) and completely stirred tank reactor (CSTR) as ozone contactors. The RPB, which provides high gravitational force by adjusting the rotational speed, was employed as a novel ozone contactor. The same ozone dosage was separately introduced into either the RPB or the CSTR for the investigation, while the experimental solution was continuously circulated within the apparatus consisting of the RPB and CSTR. The decolorization and mineralization efficiencies of RB5 in the course of ozonation are compared for these two methods. Moreover, the dissolved and off‐gas ozone concentrations were simultaneously monitored for the further analysis. As a result, the ozone mass transfer rate per unit volume of the RPB was significantly higher because of its higher mass transfer coefficient and gas–liquid concentration driving force. Furthermore, ozonation kinetics was found to be independent of the gravitational magnitude of an ozone gas–liquid contactor. Therefore, the results suggest employing RPBs as ozone‐contacting devices with the advantage of volume reduction. The experimental results, which can be used for further modeling of the ozonation process in the RPB, also show the requirement of correct design for the RPB. Consequently, the present study is useful for the understanding of practical application of RPBs. Copyright © 2004 Society of Chemical Industry     

国外钻井液和完井液用聚合物

９０年代以来，国外钻井液和完井液用聚合物添加剂的发展取得长足进步。本文介绍了国外目前用于钻井液和完井液的聚合物添加剂的类型及作用。     

布里奇曼法生长碲镉汞晶体的固液界面形态研究

文中综述了布里奇曼法及加速坩埚旋转技术的布里奇曼法生工碲镉汞晶体过程中固液界面形态的研究结果，简单讨论了固液界面形态对组分分布的影响，并将两种技术所得的组分分布结果进行了比较，在分析影响固液界面形态因素的基础上，认为加速坩埚旋转技术是目前改善固液界面形态的有效方法。     

输入——输出迭代算法中松弛因子的确定

本文利用变分的手段提示了输入—输出迭代算法中松弛因子的取值规律。     

结构陶瓷的高温疲劳强度衰减理论

提出了陶瓷材料疲劳强度衰减理论并由此导出了各种疲劳关系式。建立了疲劳基本方程ｄσ＿ｒ／ｄ＿ｉ＝一Ａσ（ｔ）￣ｎｔ￣（－ｍ），得出了疲劳寿命公式Ｔ＝Ｍ（σ＿０－σ）／Ａσ￣ｎ（静疲劳时Ｍ＝１，连续增载疲劳时Ｍ＝ｎ＋１，循环疲劳时Ｍ＝（ｎ＋１）／（１＋Ｒ＋Ｒ￣２＋……＋Ｒ￣ｎ），逐级加载时，并导出不同疲劳方式下疲劳寿命间的关系。同时，用多种Ｓｉ＿３Ｎ＿４材料在高温中作了论证试验，结果与理论一致。     

通过室内实验及同位素测井技术评价高分子聚合物驱油效果

2500万超高分聚合物室内驱油实验研究了聚合物分子量、浓度、粘度、聚用量、段塞组合等各项性能指标对驱油效果的影响。本文根据室内实验结果,在北一区断西注聚后期开展矿场试验,取得了较好的开发效果。试验前后对比,注入粘度明显增大,月含水上升速度得到有效控制,吸入剖面有了新的动用,有63.1%的油井出现了明显的二次受效特征,取得了显著的经济效益。同时对驱油效果进行系统分析。驱油效果表明:应用2500万超高分聚合物是进一步提高聚驱采收率的有效途径。     

尿素醇解合成碳酸酯类化合物技术进展

综述了用尿素醇解合成碳酸酯类化合物的技术进展 ,重点介绍尿素醇解合成碳酸二甲酯研究现状以及与其它工艺路线的比较 ,另外也介绍了尿素醇解合成长碳链脂肪族和芳香族类碳酸酯的研究进展。     

省煤器管开裂原因分析

对省煤器开裂管进行了化学成分及宏、微观分析。分析结果表明，在高温高压条件下，在其焊缝溶合区出现粗大的魏氏组织，管材中的珠光体组织产生了不同程度的球化，而母材组织又存在严重的带状组织。在过热条件下熔合区极易出现裂纹，并由此快速扩展，造成省煤器管开裂。     

An Inductively Coupled Lamb Wave Transducer

Wafer-type piezoelectric transducers are effective transducers for the excitation and detection of ultrasonic Lamb waves in plate-like structures. Such transducers are, however, vulnerable to corrosion and physical damage when mounted in exposed locations. In this paper we describe an inductively coupled Lamb wave transducer that eliminates the need for direct electrical connections. Signals are coupled into and out of the transducer using two probe coils. In this paper we explore the operation of inductively coupled transducers both analytically and experimentally. Finite-element analysis is used to determine inductances and the coupling constant, and electrical circuit analysis to determine the transfer function and its dependence on the gap between the probe coils and the transducer. Experiments show that return signals of millivolt amplitude are obtained when the transducer is excited with 10-V amplitude pulses. These transducers are suitable for permanent mounting on structures to be monitored for cracks or flaws     

电信服务营销渠道转型的必要性

分析了电信企业服务营销渠道的特点、旧有的服务营销渠道模式和存在的问题以及今后电信业和市场等方面发展的新需求，对电信服务营销渠道转型的必要性进行了探讨和研究,同时提供了一个可供参考的服务营销渠道价值评估体系架构,从量化服务营销渠道对电信企业贡献价值的角度论述了服务营销渠道转型的必要性。