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81.
Abstract. This paper derives expressions for the exact bias and variance of a general class of spectral density estimators at the zero frequency, building on the work of Neave (The exact error in spectrum estimates. Ann. Math. Statist. 42 (1971), 961–75) who studied the case where the mean of the series is assumed known. These expressions are evaluated for 15 different windows and for a wide variety of stationary time series. The exact error of the estimators is found to depend on whether the sample mean has to be estimated, and some windows are noticeably inferior at certain values of the bandwidth. A response surface analysis reveals that the finite sample relationships between the bandwidth and the exact error are quite different from the ones suggested by asymptotic theory. 相似文献
82.
83.
Serge Beaupré Pierre‐Luc T. Boudreault Mario Leclerc 《Advanced materials (Deerfield Beach, Fla.)》2010,22(8):E6-E27
World energy needs grow each year. To address global warming and climate changes the search for renewable energy sources with limited greenhouse gas emissions and the development of energy‐efficient lighting devices are underway. This Review reports recent progress made in the synthesis and characterization of conjugated polymers based on bridged phenylenes, namely, poly(2,7‐fluorene)s, poly(2,7‐carbazole)s, and poly(2,7‐dibenzosilole)s, for applications in solar cells and white‐light‐emitting diodes. The main strategies and remaining challenges in the development of reliable and low‐cost renewable sources of energy and energy‐saving lighting devices are discussed. 相似文献
84.
85.
Bomatí-Miguel O Tartaj P Morales MP Bonville P Golla-Schindler U Zhao XQ Veintemillas-Verdaguer S 《Small (Weinheim an der Bergstrasse, Germany)》2006,2(12):1476-1483
Passivated iron nanoparticles (10-30 nm) have been synthesized by laser pyrolysis of a mixture of iron pentacarbonyl and ethylene vapors followed by controlled oxidation. The nanoparticles show a well-constructed iron-iron oxide core-shell structure, in which the thickness and nature (structure similar to maghemite, gamma-Fe2O3) of the shell is found to be independent of the initial conditions. On the other hand, the composition of the core is found to change with the particle size from the alpha-Fe structure to a highly disordered Fe phase (probably containing C atoms in its structure). The dependence of the magnetic properties on the particle size, iron oxide fraction, and temperature was also investigated. In the case of smaller particles, the magnetic data indicate the existence at low temperature of a large exchange anisotropy field, the magnitude of which increases with decreasing temperature in correspondence with the freezing of magnetic moments in the oxide shell. 相似文献
86.
Jean‐Pierre Coyette Karl Meerbergen Mickaël Robb 《International journal for numerical methods in engineering》2005,64(13):1752-1768
In this paper, we analyse the numerical time integration of models of exterior acoustics. The major challenge lies in the instabilities that may arise from the infinite elements. In this paper we consider the special case of spherical infinite elements formulations, which have shown their relevance for industrial applications. We propose a method that combines Crank–Nicholson's method with a filtering step by the backward Euler method. The paper is illustrated with an example relevant to industry. Copyright © 2005 John Wiley & Sons, Ltd. 相似文献
87.
88.
den Hertog MI Rouviere JL Dhalluin F Desré PJ Gentile P Ferret P Oehler F Baron T 《Nano letters》2008,8(5):1544-1550
Silicon nanowires (NW) were grown by the vapor-liquid-solid mechanism using gold as the catalyst and silane as the precursor. Gold from the catalyst particle can diffuse over the wire sidewalls, resulting in gold clusters decorating the wire sidewalls. The presence or absence of gold clusters was observed either by high angle annular darkfield scanning transmission electron microscopy images or by scanning electron microscopy. We find that the gold surface diffusion can be controlled by two growth parameters, the silane partial pressure and the growth temperature, and that the wire diameter also affects gold diffusion. Gold clusters are not present on the NW side walls for high silane partial pressure, low temperature, and small NW diameters. The absence or presence of gold on the NW sidewall has an effect on the sidewall morphology. Different models are qualitatively discussed. The main physical effect governing gold diffusion seems to be the adsorption of silane on the NW sidewalls. 相似文献
89.
Charuhas V. Thakar Orfeas Liangos Jean&#;Pierre Yared David A. Nelson Srinivas Hariachar Emil P. Paganini 《Hemodialysis international. International Symposium on Home Hemodialysis》2003,7(2):143-147
Background: Acute renal failure (ARF) after cardiac surgery is associated with significant morbidity and mortality, irrespective of the need for dialysis. Previous studies have attempted to identify predictors of ARF and develop risk stratification algorithms. This study aims to validate the algorithm in an independent cohort of patients that includes a significant proportion of female and black patients and compares two different definitions of renal outcome.
Methods: A large single center cardiac surgery database was examined (n, 24,660; 1993–2000) which included 29.9% females and 3.7% black patients. Post‐operative ARF was defined as: a) ARF requiring dialysis, b) > 50% reduction in creatinine clearance relative to baseline or requiring dialysis. Clinical variables related to baseline renal function and cardiovascular disease were used in recursive partitioning analysis for both outcome definitions. Chi‐square goodness of fit analysis was performed to validate the algorithm.
Results: The frequency of post‐operative ARF requiring dialysis ranged between 0.5 and 15.5% based on the risk categories with the area under the receiver operating characteristic (ROC) curve of 0.78. Using the more inclusive definition of ARF, the frequency was significantly higher ranging from 2.6 to 25%(P < 0.001) with an area under ROC curve of 0.65.
Conclusions: The renal risk stratification algorithm is valid in predicting post‐operative ARF in an independent cohort of patients, well represented by differences in gender and race. Since the need for dialysis remains subjective, a more objective and inclusive definition of ARF may help in identifying a larger number of patients 'at‐risk'. 相似文献
Methods: A large single center cardiac surgery database was examined (n, 24,660; 1993–2000) which included 29.9% females and 3.7% black patients. Post‐operative ARF was defined as: a) ARF requiring dialysis, b) > 50% reduction in creatinine clearance relative to baseline or requiring dialysis. Clinical variables related to baseline renal function and cardiovascular disease were used in recursive partitioning analysis for both outcome definitions. Chi‐square goodness of fit analysis was performed to validate the algorithm.
Results: The frequency of post‐operative ARF requiring dialysis ranged between 0.5 and 15.5% based on the risk categories with the area under the receiver operating characteristic (ROC) curve of 0.78. Using the more inclusive definition of ARF, the frequency was significantly higher ranging from 2.6 to 25%(P < 0.001) with an area under ROC curve of 0.65.
Conclusions: The renal risk stratification algorithm is valid in predicting post‐operative ARF in an independent cohort of patients, well represented by differences in gender and race. Since the need for dialysis remains subjective, a more objective and inclusive definition of ARF may help in identifying a larger number of patients 'at‐risk'. 相似文献
90.
Stefan Drawin Denis Boivin Pierre Petit 《Metallurgical and Materials Transactions A》2005,36(3):497-505
Texture and crystallographic orientation relationships in arc-melted hypoeutectic and hypereutectic binary Nb-Si alloys are investigated. Electron backscattered diffraction (EBSD) is used here in conventional conditions, i.e., at relatively high spatial resolution (<1 μm) for ∼400×400 μm fields, as well as on very large fields (1.1×1.1 mm), at lower resolution, to get a statistical overview of the microstructure. In as-cast Nb-16Si and Nb-22Si alloys (compositions are in at. pct), [001]Nb3Si is found parallel to the local thermal gradient, with Nb3Si + Nb eutectic cells, giving rise to a microstructure similar to that obtained by directional solidification. In Nb-22Si alloy, the following orientation relationships between poles of metallic and silicide phases have been found: (111)Nb//(111)Nb3Si (as cast), (011)Nb//(011) α-Nb5Si3, and (111)Nb//(100) α-Nb5Si3 (heat treated at 1500 °C, 75 hours). This article is based on a presentation made in the symposium entitled “Beyond Nickel-Base Superalloys,” which took place March 14–18, 2004, at the TMS Spring meeting in Charlotte, NC, under the auspices of the SMD-Corrosion and Environmental Effects Committee, the SMD-High Temperature Alloys Committee, the SMD-Mechanical Behavior of Materials Committee, and the SMD-Refractory Metals Committee. 相似文献