High-pressure dc sputtering of High-Tc BPSCCO thin films withTc(0) above 100 K

High-T _c Bi(Pb)-Sr-Ca-Cu-O thin films have been made on single-crystal MgO substrates using high-pressure dc sputtering technique. X-ray studies confirm the crystallinity and highly oriented structure withc-axis perpendicular to the substrate. By optimizing the annealing schedule the formation of the high-T _c phase is stabilized. The best film exhibited superconducting transition temperature with zero-resistance temperature,T _c(0), as high as 101 K. Temperature dependence ofJ _c indicates the presence of Josephson-type weak links.     

Self-co-operative ternary pulse-compression sequences

An algorithm called a Hamming scan was developed recently for obtaining sequences with large merit factors and is adopted here to obtain such sequences within which there are nontrivial segments of large merit factors. Correlative detection of the return signal can be based simultaneously on the entire sequence and its segments with large merit factors. Such a coincidence detection scheme can be characterized by a Schur merit factor of the sequence. Sequences with large Schur merit factors are listed.     

Accessing files in an Internet: the Jade file system

The Jade file system, which provides a uniform way to name and access files in an Internet environment, is introduced. Jade is a logical system that integrates a heterogeneous collection of existing file systems in which underlying file systems support different file access protocols. Because of autonomy, Jade is designed under the restriction that the underlying file systems may not be modified. In order to avoid the complexity of maintaining an Internet-wide, global name space, Jade permits each user to define a private name space. Jade's name space supports two features: it allows multiple file systems to be mounted under one directory, and it permits one logical name space to mount other logical name spaces. A prototype of Jade has been implemented to examine and validate its design. The prototype consists of interfaces to the Unix File System, the Sun Network File System, and the File Transfer Protocol. An overview of Jade's design is reported, and the authors' experiences in designing and implementing a large scale file system are reviewed     

Hyaluronic acid induced hyaluronic acid binding protein phosphorylation and inositol triphosphate formation in lymphocytes

In this report, the role of 34 kDa HA-binding protein in hyaluronic acid-induced cellular signalling in lymphocytes has been examined. The binding of 125I-HA to lymphocytes in vivo was found to be inhibited by pre-incubation of the cells with anti-34 kDa HA-binding protein antibodies, thus confirming 34 kDa HA-binding protein as the specific HA-receptor in lymphocytes. This observation was substantiated by anti-34 kDa HA-binding protein antibodies immunoblotting and 125I-HA ligand blotting of lymphocytes cell lysate. The HA-induced cell aggregation, tyrosine phosphorylation and cytoskeletal protein phosphorylation demonstrate the HA-induced early cellular signalling events in lymphocytes. Further, to study the involvement of 34 kDa HA-binding protein in mitogen induced lymphocyte signalling, we studied in vivo phosphorylation and secondary messenger formation. The enhanced 34 kDa HA-binding protein phosphorylation by HA and the inhibition of cellular aggregation and IP3 formation by anti-HA-binding protein antibodies revealed that 34 kDa HA-binding protein is one of the potential mediators in HA-induced signal transduction.     

Dynamics Modelling of Hexaslides using the Decoupled Natural Orthogonal Complement Matrices

In this paper, dynamic model of a class of parallel systems, namely, the hexaslides, is proposed. The model developed is based on the concept the decoupled natural orthogonal complement (DeNOC) matrices, introduced elsewhere. The dynamic model of hexslides, though complex due to the existence of multi-loop kinematic chains, is required for actuator power estimation, computed-torque control, optimum tool trajectory generation, etc. The use of DeNOC offers many physical interpretations, recursive algorithms, and parallel computations. Using the proposed dynamic model, a parallel inverse dynamics algorithm has been presented to compute the actuator forces. This is useful to choose suitable motors for an application. An illustration is provided using an existing machine tool based on hexaslides, namely, the HexaM, while it is carrying out a circular contouring. Secondly, the effect of leg and slider inertias is also studied, which clearly suggests that neither of these can be neglected while finding the actuator forces.     

Oxygen-enrichment of YBa2Cu3 YBa2Cu3O7-δ using the fluidization techniqueusing the fluidization technique

The oxygen-deficient phase of the highT _c superconductor, YBa₂Cu₃O₇, was oxygen-enriched using the fluidization technique to give good superconducting properties. The normal method of oxygen treatment at 900°C for 24 h and at 600°C for 24 h has been reduced to just one treatment at 600°C for 12 h by the fluidization technique to achieve almost the same strength of superconducting signal for the YBa₂Cu₃O₇ powder, which establishes the attractiveness of the latter route for the large-scale preparation of superconducting material. The particle sizes were in the range 0–90, 90–180 and 180–420 μm. The fluidized particles were crystalline with orthorhombic distortion.T _c ^onset , estimated using the a.c. magnetic susceptibility method, was 91·3 K. The volume fraction of superconducting material in the product was 83·7–85·3%, one of the highest values reported so far for YBa₂Cu₃O₇.     

Spectrophotometric determination of some antioxidants with potassium permanganate and metol

New spectrophotometric methods for the assay of some antioxidants have been developed using potassium permanganate and metol (p-N-methyl amino phenol). Metol is oxidised at pH 3.0 with potassium permanganate and coupled with antioxidants to give λ_max at 560 nm for propyl gallate and gallic acid and 510nm for butylated hydroxy anisole. The method is simple, sensitive, reproducible and accurate within ±1% and applicable to the assay of antioxidants (gallic acid, propyl gallate and butylated hydroxy anisole) in oils and fats.