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31.
32.
The total syntheses of 9(Z),12(E)- and 9(E),12(Z)-octadecadienoic acids have been carried out. A useful intermediate in both
syntheses, 8-bromo-octanoic acid, recently has become available from commercial sources. This compound has been used to expedite
the preparation of these isomers. The remaining carbon atoms were derived from propargyl alcohol along with either 1-heptyne
or acetylene and 1-bromopentane. Because the overall yield for each sequence was roughly 15% and there were no extraordinary
reaction conditions in any of the synthetic steps, the compounds could be prepared readily in multiple gram quantities. The
syntheses of the two compounds were supported by data from a variety of spectroscopic techniques. 相似文献
33.
Alkali-metal carbonate salts meet the requirements for high-temperature solar central receiver systems, but because of their corrosiveness they present special problems in the design of storage tanks. In order to reduce corrosion and temperature sufficiently to retain strength in the storage containing wall, internal and thermal insulation is required. We present design options and operation criteria for sensible-heat, molten-salt storage with internal insulation. 相似文献
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Claudia Stewart Nicole Lum Robert Hill Robert Stephens Paul Rudnick Lynn Rassmussen 《Journal of The Association for Laboratory Automation》2003,8(2):64-65
Primer walking of cloned DNA is a standard research tool. It has been used in the past to determine the sequence of individual clones of interest. With the expansion of DNA sequencing capacity the need to be able to walk larger numbers of clones has become necessary. Our laboratory is a mid-sized genomics facility. In conjunction with the Advanced Biomedical Computing Center (ABCC) we have developed methods for automating the primer selection, DNA sequencing, contig assembly and sequence analysis for clones arrayed in microtiter format. This approach has allowed us to walk 475 clones (five microtiter plates) selected from a cDNA library. 相似文献
36.
Defends the practice of modifying reprints of journal articles to amend typographical and other errors that can affect meaning. A standard should be developed for dealing with such errors by hand writing corrections, including a list of errata, or issuing professionally corrected reprints with the notation that corrections have been made. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
37.
Cuddihy P. Hinman R.T. Avestruz A. Lupton E.C. Livshin G. Rodriguez J.I. Leeb S.B. Clark C.M. Horvath K.J. Volicer L. Landfeldt B. Kay J. Kummerfeld R. Quigley A. West D. Apted T. Sinclair G. Haniff D.J. Kalawsky R. Atkins D. Lewin M. Brown S.J. Shahmehri N. Aberg J. Maciuszek D. Chisalita I. 《Pervasive Computing, IEEE》2004,3(2):48-50
This issue's Works in Progress department presents six abstracts for projects that are developing interesting solutions to the elderly's quality of life challenges. The first two abstracts discuss projects that will help provide the elderly with freedom and independence by instrumenting their environments with supportive technology. The next two abstracts discuss projects building specialized user interfaces for addressing some of the challenges associated with aging, such as vision impairment. The final two abstracts present projects that will aid independence for the elderly by providing remote monitoring and assistance. 相似文献
38.
Almond preferences were produced by giving rats a mixture of almond and sucrose (Experiments 1-4) or saccharin (Experiment 4). A subsequent extinction procedure consisted of either repeated 2-bottle almond versus water tests (Experiment 1) or repeated exposure to almond alone (Experiments 2-4). The main independent variable was whether access to food following a session was given immediately, 30 min later, or 120 min later. No effect of extinction was found in any experiment. An important finding was that varying the delay until food access had no detectable effect. It was concluded that inadvertent flavor-food associations do not maintain preference for the flavor under extinction conditions. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
39.
The Republicans took control of both houses of Congress in November of 1994 for the 1st time in 42 yrs. Although the magnitude of the Clinton Administration's proposed Health Security Act may well have triggered fears of overcontrol, it is clear that the delivery of psychological care will be changed dramatically by the combined forces of federal and state health reform. R. J. Resnick, President of the American Psychological Association, has appointed the Task Force on Education and Training for Work in Organized Delivery Systems to look at how psychological health care is provided in the new and evolving systems, and to examine how current training programs prepare new psychologists to practice in and around organized health care systems. Dr. Resnick is similarly concerned about standardization of training, training in nontraditional areas of competence, and increased federal recognition and funding of training in psychology. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
40.