邻硝基苯甲醚液相加氢制邻氨基苯甲醚的研究

对邻硝基苯甲醚液相加氢还原制邻氨基苯甲醚的工艺进行了研究。试验结果表明,加氢还原工艺在产品质量、收率及经济效益方面都优于传统还原工艺。     

刍议酒-湖特高压跨线施工期间水布垭电厂保供电措施

根据酒湖线特高压跨线施工对水布垭电厂运行造成的影响和要求,结合恩施地区及周边的电网结构、特点,电厂从组织管理、技术等多方面采取了种种措施,保证了厂网的安稳运行,并对进一步提升电厂的保供电能力提出了建议。     

降压新药西尼地平杂质Ⅰ的制备

以西尼地平为起始原料,活化MnO2为氧化剂,一步法制备了2,6-二甲基-4-(3-硝基苯基)吡啶-3,5-二甲酸3-(2-甲氧基)乙酯5-(3-苯基)-2(E)-丙烯酯(记为西尼地平杂质Ⅰ).经实验优化,制备西尼地平杂质Ⅰ的最适宜条件为:m(西尼地平):m(MnO2)=1.00:1.24,甲苯为溶剂,105℃下反应1 h.反应得到西尼地平杂质Ⅰ收率为92.3％,经高效液相色谱面积归一化法检测后,纯度达到99.2％.产物结构经HRMS,1HNMR、13CNMR以及FTIR进行确认.该反应实现了西尼地平绿色高效直接转化西尼地平杂质Ⅰ.     

HEGM: A hierarchical elastic graph matching for hand gesture recognition

A hierarchical scheme for elastic graph matching applied to hand gesture recognition is proposed. The proposed algorithm exploits the relative discriminatory capabilities of visual features scattered on the images, assigning the corresponding weights to each feature. A boosting algorithm is used to determine the structure of the hierarchy of a given graph. The graph is expressed by annotating the nodes of interest over the target object to form a bunch graph. Three annotation techniques, manual, semi-automatic, and automatic annotation are used to determine the position of the nodes. The scheme and the annotation approaches are applied to explore the hand gesture recognition performance. A number of filter banks are applied to hand gestures images to investigate the effect of using different feature representation approaches. Experimental results show that the hierarchical elastic graph matching (HEGM) approach classified the hand posture with a gesture recognition accuracy of 99.85% when visual features were extracted by utilizing the Histogram of Oriented Gradient (HOG) representation. The results also provide the performance measures from the aspect of recognition accuracy to matching benefits, node positions correlation and consistency on three annotation approaches, showing that the semi-automatic annotation method is more efficient and accurate than the other two methods.     

聚1-丁烯热塑性弹性体的老化与防护

以拉伸性能为主要检测指标，考察了聚1-丁烯[P(1-Bt)]热塑性弹性体的热氧老化、紫外光老化和耐酸碱老化性能，制备了P(1-Bt)和三元乙丙胶(EPDM)防水卷材试样并进行对比：结果表明：单独使用抗氧剂1010，其用量在0．1～0．2质量份时具有较好的防热氧效果；1010与DLTP配合使用效果更佳，最佳配比为m(1010)：n(DLTP)=1：3(1010为0．2份)。热氧防老剂与紫外光吸收剂并用明显优于热氧防老剂或紫外光吸收剂单用时的防紫外光效果；ZnO对热氧老化和紫外光老化也具有很好的防护作用。P(1-Bt)制备的防水卷材的耐紫外光老化性能接近EPDM防水卷材，耐酸碱性能优于后者。     

利用DD混剂合成丙烯酸-3-氯-2-丙烯酯

为了综合利用DD混剂(1,3-二氯丙烯和1,2-二氯丙烷的混合物),以工业副产品DD混剂为主要原料,使1,3-二氯丙烯与丙烯酸、氢氧化钠反应,合成了丙烯酸-3-氯-2-丙烯酯并分离出1,2-二氯丙烷,并确定了适宜的工艺条件。     

鞋用水性聚氨酯胶粘剂的研究进展

介绍了水性聚氨酯鞋用胶粘剂制备方法、性能,以及用于提高水性聚氨酯耐水性、耐溶剂性和耐热性能的交联改性技术,综述了水性聚氨酯的国内外研究进展及其在制鞋领域中的应用情况。     

Telerobot-enabled HUB-CI model for collaborative lifecycle management of design and prototyping

The HUB-CI model is investigated in a telerobotic system in a client/server network to manage the lifecycle of engineering design and prototyping. The purpose of this platform is to support collaborative engineering design and proof of concept to enhance distributed team collaboration and resource utilization. The suggested platform is exemplified in two collaboration support tools and a physical prototyping platform. Structured Co-Insight Management is developed to support innovative idea exchanges and the consensus decision-making during the design process. Conflict/error detection management helps preventing conflicts and errors during the lifecycle of design and development. Physical collaboration over the network occurs when a team controls the telerobot operation during prototyping and testing in design cycles. A pilot system is implemented with a group project for the design of an electronic circuit (including both hardware and software designs). The functional assessment method is used to compare this platform to other collaborative design tools. The system presented offers unique qualitative advantages as an integrated collaboration support system.     

方坯连铸高效化二冷技术

建立了方坯高效连铸二冷数学模型,提出了喷嘴有效喷淋系数和二冷有效比水量的概念.依据二冷均匀冷却的思想,重新设计并优化了二冷喷淋结构和喷嘴的布置,增加了一个二冷喷淋段.提出了新的二冷水模型,即Qi=a bv cv2=d(△T-30) F;二冷各段的喷水量与拉速、浇铸温度、钢水成分和二冷水温相关.实践证明,经优化后的二冷结构和二冷水模型合理,拉速大幅度提高,150×150 mm2断面的最高拉速达3.8～4.0 m/min;铸坯质量明显改善,产量显著提高,经济效益显著.     

显像管屏玻璃池炉耐火材料侵蚀机理

显像管玻璃池炉耐火材料侵蚀是引发其缺陷的主要原因之一,本文主要论述了彩色显像管屏玻璃池炉耐火材料侵蚀机理,并简要讨论了它们所形成的玻璃缺陷.