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61.
Omnia M. El-Ahwany Ateyya A. Aboul-Enein Samira M. Abdel-Azim Noha A.K. Aboul-Gheit Salah A. Abo-EL-Enein 《Fullerenes, Nanotubes and Carbon Nanostructures》2020,28(6):435-445
AbstractIn this study, Fe–MgO catalyst substrates with various Fe and MgO combinations were evaluated for the growth of different types of carbon nanostructure materials (CNMs), particularly graphene nanoplatelets (GNPs) and carbon nanotubes (CNTs) via chemical vapor deposition using methane as a carbon source. The hydrogen yield was also determined as a valuable by-product in this process. Therefore, a set of Fe–MgO catalysts with different iron loadings (30, 80, 85, 90 and 100?wt %) were prepared by the combustion method to realize this target. The physicochemical properties of freshly calcined Fe–MgO catalysts were investigated by XRD, TPR and BET, while the as-grown CNMs were studied by HR-TEM, XRD and Raman spectroscopy. The results verified that the morphology of as-grown CNMs as well as the H2 yield was directly correlated to the iron content in the catalyst composition. The XRD and TPR results showed that various FeMgOx species with deferent levels of interactions were produced with the gradual incorporation of MgO content. TEM images indicated that GNPs were individually grown on the surface of high loaded iron-containing catalysts (90–100?wt %) due to the presence of highly aggregated iron particles. While multi-walled carbon nanotubes (MWCNTs) with uniform diameters were grown on the low iron-loaded catalyst (30%Fe/MgO) due to the formation of highly dispersed FeMgOx particles. On the other hand, GNPs/MWCNTs hybrid materials were grown on the surface of 80%Fe and 85%Fe/MgO catalysts. This behavior can be interpreted by the co-existence of highly aggregated and highly dispersed Fe2O3 particles in the catalyst matrix. The results demonstrated that the catalyst composition has a notable effect on the nature of CNMs products and H2 yield. 相似文献
62.
Reza Tavakkoli-Moghaddam Samira Vazifeh-Noshafagh Ata Allah Taleizadeh Vahid Hajipour Amin Mahmoudi 《工程优选》2017,49(1):136-160
This article presents a new multi-objective model for a facility location problem with congestion and pricing policies. This model considers situations in which immobile service facilities are congested by a stochastic demand following M/M/m/k queues. The presented model belongs to the class of mixed-integer nonlinear programming models and NP-hard problems. To solve such a hard model, a new multi-objective optimization algorithm based on a vibration theory, namely multi-objective vibration damping optimization (MOVDO), is developed. In order to tune the algorithms parameters, the Taguchi approach using a response metric is implemented. The computational results are compared with those of the non-dominated ranking genetic algorithm and non-dominated sorting genetic algorithm. The outputs demonstrate the robustness of the proposed MOVDO in large-sized problems. 相似文献
63.
The present work reports the synthesis of ZnFe2O4 and ZnO-Zn1-xMxFe2O4+δ (Ln?=?Sm, Eu and Ho) nanomaterials by conventional solid state reactions between Ln2O3, Zn(NO3)2, Fe(NO3)3·9H2O and/or FeCl3·6H2O raw materials at 800?°C for 10?h and 15?h. Stoichiometric and nonstoichiometric reactions were explored for the synthesis of ZnFe2O4. The two Fe sources (Fe(NO3)3 and FeCl3) were used to study the proper raw material type for the synthesis of the ZnFe2O4. The synthesized nanomaterials were characterized by powder X-ray diffraction (PXRD) technique. Rietveld analysis showed that the obtained materials were crystallized well in cubic crystal system with the space group Fd3m and lattice parameters a?=?b?=?c?=?8.4?Å. The rietveld data showed that the purity of ZnFe2O4 was increased from 14% to 88% when the Fe source was changed from FeCl3 to Fe(NO3)3 meanwhile the reaction time was changed from 10 to 15?h. However, the purity was increased to 96% when the stoichiometry of Zn:Fe was changed from 1:2 to 0.8:2 at 800?°C for 15?h. The PXRD data revealed that dopant ion type had a considerable influence on the crystal phase purity of the obtained materials. It was found that Yb2O3 decreased more the purity of the obtained target compared to the other dopant ions. Ultraviolet-visible spectra showed that the synthesized nanomaterials had strong light absorption in the visible light region. Photocatalytic performance of the as-synthesized ZnFe2O4 was investigated for the degradation of pollutant Malachite Green (MG) in aqueous solution under direct visible light irradiation. The degradation yield at the optimized condition (0.09?mL H2O2, 30?mg catalyst and 60?min) was 98%. 相似文献
64.
Ehteram Mohammad Ghotbi Samira Kisi Ozgur EL-Shafie Ahmed 《Water Resources Management》2019,33(15):5207-5230
Water Resources Management - Water allocation is an important issue for systems with multiple stakeholders. Individual and collective decisions are very important for such systems. Thus, a new... 相似文献
65.
Complementary proteomic approaches reveal mitochondrial dysfunction,immune and inflammatory dysregulation in a mouse model of Gulf War Illness 下载免费PDF全文
66.
Saleheh?Abbaspoor Samira?Agbolaghi Farhang?AbbasiEmail author 《Polymer Bulletin》2017,74(4):1103-1119
Nano-channel single crystals were developed via consecutive growth of various polymer single-crystal channels comprising homo and block copolymers by self-seeding method. Poly(ethylene glycol)-b-polystyrene (PEG-b-PS) and poly(ethylene glycol)-b-poly(methyl methacrylate) (PEG-b-PMMA) block copolymers were synthesized by atom transfer radical polymerization. Self-seeding temperature, concentration, and crystallization time affected the width of the channels. This might provide a new way to investigate directional absorption, diffusion, and immobilization of biomacromolecules on the surface. The crystalline blocks of PEG-b-PS and PEG-b-PMMA diblock copolymers were similar, therefore, the continuity of channel-wire growth was guaranteed. Development of complete square channels next to the channels covered with high molecular weight brushes was infeasible. It was ascribed to a higher hindrance of primarily existing tethered chains on the single-crystal channel. Finally, the consecutive channel-wire single crystals were compared with single-step-grown pyramidal and conic structures. These multilayer crystals grew spirally and formed non-flat channels. The structure and morphology of different crystalline channels were detected by atomic force microscopy (AFM) and small angle X-ray scattering (SAXS). In this work, for the first time, the SAXS data of channel-wire single crystals were reported and they were compared by non-flat channel-like crystals. A profound investigation of PEG-b-PS, PEG-b-PMMA copolymers and PEG homopolymer channel-wire single crystals by SAXS and their comparison with AFM data was a novel work in the field of single-crystal engineering. 相似文献
67.
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69.
Samira Mohseni Bababdani Farhad Shahriari Nogorani 《Metallurgical and Materials Transactions A》2014,45(4):2116-2122
Overaluminizing is a commercially accepted treatment to enhance high temperature oxidation resistance of MCrAlY overlay coatings. In the current investigation, a low pressure plasma-sprayed CoNiCrAlY coating was aluminized by two different growth modes: outward growth and inward growth. The resultant microstructures were characterized by means of scanning electron microscopy, energy dispersive spectroscopy, and X-ray diffraction analysis. The results showed that the final microstructure of both types of overaluminized coatings was similar and included Al-rich NiAl and Ni-rich NiAl zones from the top to the bottom. The details of the microstructures are discussed and compared with the results of simple aluminizing of the nickel-based substrate. 相似文献
70.
Yasmine Boudida Mohammed Gagaoua Samira Becila Brigitte Picard Abdelghani Boudjellal Carlos H. Herrera-Mendez 《Critical reviews in food science and nutrition》2016,56(6):957-972
Since years, serine proteases and their inhibitors were an enigma to meat scientists. They were indeed considered to be extracellular and to play no role in postmortem muscle proteolysis. In the 1990's, we observed that protease inhibitors levels in muscles are a better predictor of meat tenderness than their target enzymes. From a practical point of view, we therefore choose to look for serine protease inhibitors rather than their target enzymes, i.e. serine proteases and the purpose of this report was to overview the findings obtained. Fractionation of a muscle crude extract by gel filtration revealed three major trypsin inhibitory fractions designed as F1 (Mr:50–70 kDa), F2 (Mr:40–60 kDa) and F3 (Mr:10–15kD) which were analyzed separately. Besides antithrombin III, an heparin dependent thrombin inhibitor, F1 and F2 comprised a large set of closely related trypsin inhibitors encoded by at least 8 genes bovSERPINA3-1 to A3-8 and able to inhibit also strongly initiator and effector caspases. They all belong to the serpin superfamily, known to form covalent complexes with their target enzymes, were located within muscle cells and found in all tissues and fluids examined irrespective of the animal species. Potential biological functions in living and postmortem muscle were proposed for all of them. In contrast to F1 and F2 which have been more extensively investigated only preliminary findings were provided for F3. Taken together, these results tend to ascertain the onset of apoptosis in postmortem muscle. However, the exact mechanisms driving the cell towards apoptosis and how apoptosis, an energy dependent process, can be completed postmortem remain still unclear. 相似文献