Design Guideline for New Generation of High-Temperature Guarded Hot Plate

This paper complements the existing measurement standards and literature for high-temperature guarded hot plates (HTGHPs) by addressing specific issues relating to thermal conductivity measurement of technical insulation at high temperatures. The examples given are focused on the designs of HTGHPs for measuring thin thermal insulation. The sensitivity studies have been carried out on major influencing factors that affect the thermal conductivity measurements using HTGHPs, e.g., the uncertainty of temperature measurements, plate flatness and center-guard gap design and imbalance. A new configuration of center-guard gap with triangular shape cross section has been optimized to obtain the same thermal resistance as a 2 mm wide gap with rectangular shape cross section that has been used in the HTGHPs at NPL and LNE. Recommendations have been made on the selections of heater plate materials, high-temperature high-emissivity coatings and miniature temperature sensors. For the first time, thermal stress analysis method has been applied to the field of HTGHPs, in order to estimate the effect of differential thermal expansion on the flatness of thin rigid specimens during thermal conductivity tests in a GHP.     

Controlled Creating of Cracks in Concrete for Non-destructive Testing

The non-destructive assessment of cracks in concrete is a common task for which non-destructive evaluation solutions have been published. Primarily, these tests have been carried out on artificial cracks that have been created by using notches instead of natural cracks. This study evaluates a procedure designed to create reproducible and controlled cracks in concrete. The procedure is based on using expanding mortar in a series of blind holes. This is done in combination with carefully aligned reinforcement to guide the direction of the crack development. The depth of the crack is also controlled by reinforcement. Crack depth varies statistically in the range of the maximum aggregate size (16 mm) used for concrete.     

Development of cerium and silicon co-doped hydroxyapatite nanopowder and its in vitro biological studies for bone regeneration applications

Multi-ion, co-substituted bioactive glass ceramics play a significant role in the stimulation of physical and biological properties for outstanding effects in biomedical application. The following work attempts to develop HAP as a parent material doped with a combination of cerium (Ce⁴⁺ @1.25?wt%) and silicon (Si⁴⁺ @1, 3 and 5?wt%) by refluxing based sol-gel technique. The anti-bacterial tests exhibit E. coli showing higher inhibition efficiency, in vitro hemolytic test exhibit good compatible nature of dual doped HAP with erythrocytes (<5% of hemolytic). In vitro bioactivity assay confirms that the developed dual doped HAP possesses excellent bone-like apatite layer formation on their surfaces. In vitro cellular study was performed for Ce/Si-HAP@5% powder against MG-63 cells, which demonstrated the good cell viability at higher concentrations (up to 800?µg/ml). Further, dual doped HAP powders were characterized by various analytical techniques such as ATR-FTIR, Powder-XRD, TGA-DTA, SEM-EDS, TEM and XPS analysis. The studies confirm that the synthesized dual doped HAP will act as better bioactive glass ceramics for potential orthopedic and dentistry applications.     

Archaeological Arsenical Bronzes and Equilibrium in the As-Cu System

Metallurgical and Materials Transactions B - Understanding the effects of impurities, segregation, undercooling, and solidification velocity is necessary to reconstruct prehistoric As-Cu alloy...     

Assessment of intradialysis calcium mass balance by a single pool variable‐volume calcium kinetic model

Introduction: A reliable method of intradialysis calcium mass balance quantification is far from been established. We herein investigated the use of a single‐pool variable‐volume Calcium kinetic model to assess calcium mass balance in chronic and stable dialysis patients. Methods: Thirty‐four patients on thrice‐weekly HD were studied during 240 dialysis sessions. All patients were dialyzed with a nominal total calcium concentration of 1.50 mmol/L. The main assumption of the model is that the calcium distribution volume is equal to the extracellular volume during dialysis. This hypothesis is assumed valid if measured and predicted end dialysis plasma water ionized calcium concentrations are equal. A difference between predicted and measured end‐dialysis ionized plasma water calcium concentration is a deviation on our main hypothesis, meaning that a substantial amount of calcium is exchanged between the extracellular volume and a nonmodeled compartment. Findings: The difference between predicted and measured values was 0.02 mmol/L (range ?0.08:0.16 mmol/L). With a mean ionized dialysate calcium concentration of 1.25 mmol/L, calcium mass balance was on average negative (mean ± SD ?0.84 ± 1.33 mmol, range ?5.42:2.75). Predialysis ionized plasma water concentration and total ultrafiltrate were the most important predictors of calcium mass balance. A significant mobilization of calcium from the extracellular pool to a nonmodeled pool was calculated in a group of patients. Discussion: The proposed single pool variable‐volume Calcium kinetic model is adequate for prediction and quantification of intradialysis calcium mass balance, it can evaluate the eventual calcium transfer outside the extracellular pool in clinical practice.     

An experimental investigation on the durability of railway ballast material by magnesium sulfate soundness

In this study, the durability of railway ballast material is investigated by magnesium sulfate soundness tests. Two types of ballast aggregates, which are produced from basaltic rocks and currently used as railway ballast in such high speed railway routes in Turkey, are investigated regarding their resistance against freezing–thawing (FT) and traffic loads. Firstly, the mineralogical and physico-mechanical properties of rocks are determined. Then the degradation of investigated ballast aggregates is determined by magnesium sulfate soundness and Los Angeles abrasion (LAA) tests. The natural FT effects are simulated by magnesium sulfate soundness tests up to 40 cycles, whereas the traffic loads are represented by LAA tests up to 3000 revolutions. The ballast fouling that leads to such problems are also investigated within the scope in the present study. The degree of ballast fouling is quantified as fouling index (FI) which is determined using the crushed particles generated after LAA tests. It is concluded from laboratory studies that rock properties considered are considerably influenced by simulated FT cycles. It is also achieved from the laboratory studies that magnesium sulfate soundness and Los Angeles abrasion tests are good indicators to clarify the fragmentation mechanism of the ballast aggregate in laboratory scale. In conclusion several empirical formulas are developed to predict LAA and FI for each rock type. The proposed empirical formulas could be utilized as a pre-design tool for new railway routes in design stage provided that the investigated ballast aggregates are considered.     

Optimal packing of material flow on conveyor belts

We are interested in an optimal packing density problem for material flows on conveyor belts in two spatial dimensions. The control problem is concerned with the initial configuration of parts on the belt to ensure a high overall flow rate and to further reduce congestion. An adjoint approach is used to compare the optimization results from the microscopic model based on a system of ordinary differential equations with the corresponding macroscopic model relying on a hyperbolic conservation law. Computational results highlight similarities and differences of both optimization models and emphasize the benefits of the macroscopic approach.