Streptavidin‐Functionalized Three‐Dimensional Ordered Nanoporous Silica Film for Highly Efficient Chemiluminescent Immunosensing

A novel biofunctionalized three‐dimensional ordered nanoporous SiO₂ film is designed for construction of chemiluminescent analytical devices. The nanoporous SiO₂ film is prepared with self‐assembly of polystyrene spheres as a template and 5‐nm SiO₂ nanoparticles on a glass slide followed by a calcination process. Its functionalization with streptavidin is achieved by using 3‐glycidoxypropyltrimethoxysilane as a linker. Based on the high‐selectivity recognition of streptavidin to biotin‐labeled antibody a novel immunosensor is further constructed for highly efficient chemiluminescent immunoassay. The surface morphologies and fabrication processes of both the biofunctionalized film and the immunosensor are characterized using scanning electron microscopy, atomic‐force microscopy, X‐ray photoelectron spectroscopy, and Fourier transform infrared spectroscopy. The three‐dimensional ordered nanopores have high capacity for loading of streptavidin and antibody and promote the mass transport of immunoreagents for immunoreaction, thus the resulting chemiluminescent immunosensor shows wide dynamic range for fast immunoassay, and good reproducibility and stability. Using carbohydrate antigen 125 (CA 125) as a model, the highly efficient chemiluminescent immunosensing shows a linear range of three orders of magnitude, from 0.5 to 400 U mL^?1. This work provides a biofunctionalized porous nanostructure for promising biosensing applications.     

Fabrication,characterization, and analysis of photodetectors metal-porous silicon with different geometry and thickness of the porous silicon layer

Porous silicon photodetectors obtained by electrochemical etching of p-type non-polished crystalline silicon were studied. A metal-porous silicon structure was used to obtain the rectifying behavior. The geometry of the metal layer deposited by thermal evaporation on the porous zone was modified with different masks fabricated using a photolithographic method. The samples obtained under different anodization conditions were characterized by PL. The sample that showed the best intensity in photoluminescence, centered on 675 nm, was selected and five samples obtained under these conditions were prepared to compare the difference in the photoresponse because of the geometry of the evaporated metal layer. The responsivities obtained show us an important difference between the devices and allow us to propose a specific geometrical pattern to obtain a better response in this kind of devices.     

外注入锁定对FP激光器强度噪声的抑制

采用较强的外注入光锁定FP激光器,获得了理想的强度噪声抑制效果.在自由运转的FP激光器的弛豫振荡峰处,最大噪声抑制强度可达9dB.研究了注入光功率和频率失谐对于强度噪声抑制效果的影响.此外,通过实验研究了理想噪声抑制范围与激光器稳定锁定范围之间的关系:它们都随着注入光功率的增加而增大;但在相同的注入光功率下,稳定锁定范围允许更大的频率失谐.     

纤巧型便携式设计中的多媒体信号路径

引言 把语音服务、高分辨率相机模块、MP3或PMP播放器功能整合在单个移动电话设计中,已成为未来中高端电话市场的发展趋势。除了超高的功率（〉700mW）立体声音频功能外,视频输出功能也出现在手机应用中,其输出仍主要是CVBS格式,而某些电话甚至提供S视频或模拟RGB输出。     

CIGS Thin Films for Cd-Free Solar Cells by One-Step Sputtering Process

Cu(In_1?x Ga _x )Se₂ (CIGS) thin films were deposited by a one-step radio frequency (RF) magnetron sputtering process using a quaternary CIGS target. The influence of substrate temperature on the composition, structure, and optical properties of the CIGS films was investigated. All the CIGS films exhibited the chalcopyrite structure with a preferential orientation along the (112) direction. The CIGS film deposited at 623 K showed significant improvement in film crystallinity and surface morphology compared to films deposited at 523 and 573 K. To simplify the manufacturing procedure of solar cells and avoid the use of the toxic element Cd, the properties of ZnS films prepared by RF sputtering were also investigated. The results revealed that the sputtered ZnS film exhibits good lattice matching with the sputtered CIGS film with significantly lower optical absorption loss. Finally, all-sputtered Cd-free CIGS-based heterojunction solar cells with the structure SLG/Mo/CIGS/ZnS/AZO/Al grids were fabricated without post-selenization. Furthermore, the results demonstrated the feasibility of using a full sputtering process for the fabrication of Cd-free CIGS-based solar cell.     

大型客机进近倾斜姿态H∞控制研究

实现快速、精准、抗扰动性强的倾斜姿态控制,是大型客机自动着陆控制系统设计的关键技术之一.以Boeing707飞机在常值侧风扰动下的非线性数学模型为基础,通过配平线性化得到线性方程,综合设计了进近着陆阶段的姿态控制律.由于使用PID控制方法的滚转角响应难以兼顾快速性与稳态性能,设计了基于鲁棒H∞理论的倾斜姿态控制律.分别对两种控制方法跟踪滚转角阶跃指令,以及抗侧风扰动的控制效果进行了比较分析.仿真结果表明,状态反馈H∞控制方法能够实现快速、精准、无超调的倾斜姿态控制,且有侧风扰动存在时具有快速的恢复能力、较好的乘坐品质和较大的抗扰动控制余度.     

Results of test on microprocessor-based voltage and speed regulators carried out on a large physical model complex

Results of experimental tests carried out with microprocessor-based voltage and speed regulators using a digital-analogue-physical model complex of a large power system at the Siberian Power Institute of the USSR Academy of Sciences are described. The physical test facility, and the test objectives and procedures are also outlined. Tests were carried out on a Soviet-built microprocessor AVR and a Canadian-built microprocessor AVR and speed governor. The work described shows that the development of speed and voltage regulators using microprocessors is a feasible and promising proposition.     

表面态型半导体可饱和吸收镜实现Yb∶YAG激光器被动锁模

制作了一种新型的半导体可饱和吸收镜:表面态型半导体可饱和吸收镜.用表面态型半导体可饱和吸收镜作为被动锁模吸收体,实现了半导体端面泵浦Yb∶YAG激光器被动连续锁模.在泵浦功率为1 0 W时,获得了连续锁模脉冲序列,重复频率2 0 0 MHz,锁模脉冲平均输出功率为70 m W.在未加任何色散补偿的情况下,脉冲宽度为4 .35 ps     

塔里木油田酸压返排液重复利用研究

为确定组成复杂、浮油和高价金属离子含量高、酸性强的塔里木油田酸压返排液处理后能否顺利地配制压裂液,通过对返排液水质分析,提出了一套"过滤-化学沉淀-絮凝沉降-压裂液配制"的处理工艺。大量的浮油影响压裂液的溶胀及交联,滤布过滤可去除浮油与块状杂质组成的黏稠物;高价金属离子阻碍稠化剂分子的伸展,影响压裂液的携砂性能,碳酸钠可直接沉淀金属离子并中和残酸;简单处理之后需絮凝剂进一步絮凝处理,除去返排液中的小颗粒杂质。将处理后的水调节至中性或弱酸性直接配制成压裂液使用,可杜绝环境污染,缓解油田水资源匮乏问题。沉淀剂质量浓度为145g/L、絮凝剂质量浓度为1 000mg/L时,返排液中悬浮颗粒杂质的去除率达98%,水质平均粒径2.36μm。利用处理后的酸压返排液配制的压裂液挑挂性能良好,其流变性能和黏弹性能与清水直接配制的压裂液相差不大,均满足SY/T 6376-2008《压裂液通用技术条件》常规压裂液性能标准,适用于塔里木油田超深井高温高剪切要求。研究表明,酸压返排液重复利用配制压裂液的工艺是可行的。     

水包油乳液型复合泥饼清除剂的室内研究

针对裂缝性致密砂岩储层存在的高密度油基钻井液固相颗粒侵入以及泥饼难以清除等问题,开发出一种高效率、抗高温、低成本的水包油型复合泥饼清除剂。复合泥饼清除剂由混合酸、抗高温渗透剂、清洗剂、乳化剂等组成。通过对复合泥饼清除剂——水包油型乳液体系以及新型泥饼清除剂——纳米乳液体系的对比研究分析表明,在洗油方面以及溶蚀泥饼结构方面,复合泥饼清除剂效果优于纳米乳液。该复合泥饼清除剂的稳定性能强,抗温可达120℃;在静态条件下泥饼清除率可以达到90%以上,在动态条件下清除后岩心渗透率恢复值可以达到89%,最佳作业时间为8 h。在目前求降本增效的形势下,该复合泥饼清除剂剂配方简单,性能优良,解堵时间较短,能够有效改善和提高岩心渗透率恢复值。