Preparation and Catalytic Performance of Mesostructured Aluminosilicate Nano-particles with Wormhole-Like Framework Structure

A facile two-step sol–gel method has been developed for the preparation of mesostructured aluminosilicate nano-particles (Si/Al = 7.5) with wormhole-like but uniform pore structures and highly catalytic activities towards bulky hydrocarbon cracking. It is desirable that, as this synthesis takes place in the absence of alkali cations, the mesoporous nano-particulate material is directly obtained in the acid form, making a subsequent ion-exchange and calcination treatment superfluous.     

A schema aware ETL workflow generator

Extract, Transform and Load (ETL) processes organized as workflows play an important role in data warehousing. As ETL workflows are usually complex, various ETL facilities have been developed to address their control-flow process modeling and execution control. To evaluate the quality of ETL facilities, Synthetic ETL workflow test cases, consisting of control-flow and data-flow aspects are needed to check ETL facility functionalities at construction time and to validate the correctness and performance of ETL facilities at run time. Although there are some synthetic workflow and data set test case generation approaches existed in literatures, little work is done to consider both aspects at the same time specifically for ETL workflow generators. To address this issue, this paper proposes a schema aware ETL workflow generator with which users can characterize their ETL workflows by various parameters and get ETL workflow test cases with control-flow of ETL activities, complied schemas and associated recordsets. Our generator consists of three steps. First, with type and ratio of individual activities and their connection characteristic parameter specification, the generator will produce ETL activities and form ETL skeleton which determine how generated activities are cooperated with each other. Second, with schema transformation characteristic parameter specification, e.g. ranges of numbers of attributes, the generator will resolve attribute dependencies and refine input/output schemas with complied attributes and their data types. In the last step, recordsets are generated following cardinality specifications. ETL workflows in specific patterns are produced in the experiment in order to show the ability of our generator. Also experiments to generate thousands of ETL workflow test cases in seconds have been done to verify the usability of the generator.     

浅谈皮带定量给料机的机械配置选型

皮带定量给料机是目前水泥生产企业中最为常见的过程计量和配料的设备。作者结合多年来开发、调试和使用皮带定量给料机的实践经验与资料积累，介绍了如何根据实际需要和使用量程，通过对皮带定量给料机的主要机械参数的计算来合理地选用定量给料机的型号和规格。     

Early age microstructure of Portland cement mortar investigated by ultrasonic shear waves and numerical simulation

This paper investigates the ability of a shear wave reflection (WR) method to monitor microstructural changes of Portland cement mortar during hydration. The wave reflection method measures the reflection loss of shear waves at an interface between a steel plate and mortar. Mortars with water/cement ratios of 0.35, 0.5 and 0.6 were tested at isothermal curing conditions of 25 °C. The numerical model HYMOSTRUC3D was used to simulate the evolution of microstructural properties of the cement paste phase of the tested mortars. The parameters obtained from the simulations were the volume fraction of the total and connected solid phase and the specific contact area of the hydrated cement particles. The investigations have shown that the wave reflection measurements are governed primarily by the degree of the inter-particle bonding of the cement particles as calculated from the specific contact area of a simulated microstructure.     

Preparation and characterization of antibacterial silver-dispersed activated carbon aerogels

Silver-dispersed carbon aerogels (CAs) were obtained by direct immersion of organic aerogels prepared by ambient pressure drying technique in AgNO₃ aqueous solution and then carbonization. The effect of preparation conditions such as the resorcinol/catalyst ratio, the feed AgNO₃ concentration, the ratio of aerogel mass/solution volume, immersion time and carbonization temperature on the bulk density and silver content as well as the BET surface area of the dispersed CAs was studied. The dispersion and structure of silver nanoparticles in obtained materials were investigated by means of scanning electron microscopy, transmission electron microscopy and X-ray diffraction. The Ag-dispersed CAs prepared exhibit strong and long-term antibacterial activity.     

硫化镉微晶掺杂玻璃及薄膜的制备与光学性能的研究

用溶胶－凝胶法制备了硫化镉微晶掺杂玻璃和薄膜材料，使用了三种不同的方法引入所需的Ｓ＾２－离子，通过Ｘ射线和透射电镜等实验手段，分析了微晶结构显微相，标定出晶体确为ＣｄＳ，并测得微晶的尺寸。从室温吸收光谱上观察到吸收截止边随着ＣｄＯ掺杂凝胶在１５０℃时通Ｈ２Ｓ气体时间的延长（１－８ｈ）而移向长波方向，从而确定其为量子尺寸效应的实验依据。在Ｎｄ：ＹＡＧ强激光光场的作用下，薄膜样品中观察到二次谐波信号，     

再结晶法制备高纯超细Al2O3粉的研究

本文介绍了用一种再结晶技术制造高炖、超细Al_2O_3粉体的新方法。 将硫酸铝铵溶液(AA)滴入碳酸氢铵溶液(AHC),经过反应合成一种新的含铝化合物,碳酸氢铝铵(AACH),然后在高温下煅烧,生成超细Al_2O_3粉体。另外还采用了X射线,红外光谱,DTA,以及TEM等手段,研究了反应温度、浓度、PH值和老化条件等对生成物AACH和Al_2O_3的影响。     

一种评估LEO卫星通信网络抗毁性的新方法研究

抗毁性是低轨卫星通信网络的重要属性,评估卫星网络抗毁性对卫星网络结构设计具有重要意义.针对低轨卫星网络的特点,在对复杂网络抗毁性的研究基础上,建立以自然连通度为基础的卫星网络抗毁性测度指标,利用STK/Matlab仿真工具分析卫星网络的抗毁性.实验分析表明,仿真结果可以有效评估卫星网络抗毁性大小.     

医疗大数据特征挖掘及重大突发疾病早期预警

通过运用新兴的尖端云计算技术,设计研发了健康云平台。采用分布式云存储技术存储大规模的异构多模态生理信号数据,将数据挖掘模型（L1-逻辑斯蒂）整合至MapReduce框架中,快速挖掘用户的健康信息以及重大疾病高风险因子,让用户能实时地了解自己的身体状况,同时对用户的异常状况给出预警信息,并通知其前往医院就医,实现了对重大突发疾病的早期预警。     

国产SEBS流变性能评价

通过对国产SEBS(氢化苯乙烯-丁二烯-苯乙烯嵌段共聚物)流变性能进行测试．分析不同结构、不同嵌段的S／B质量比值、不同相对分子质量、不同加工温度对SEBS产品流变性能的影响．促进用户对国产SEBS性能的了解。