Gr（C）纤维增强镁基复合材料的界面结构

采用真空—压力浸渗工艺制备Ｇｒ（Ｃ）／Ｍｇ复合材料，Ｇｒ／Ｍｇ材料界面上无化学反应迹象，有析出物γ相（Ｍｇ１７Ａｌ１２），该析出物形状、大小与制备工艺条件，主要是纤维预制件温度有关。Ｃ／Ｍｇ复合材料界面Ａｌ含量较基体高出２倍多，文中分析了可能的原因     

The establishment of the statistical-thermodynamic model of D81-structure and its application to α-Nb5Si3

A statistical-thermodynamic model for binary nonstoichiometric A₅B₃ with D8₁-structure has been established on the basis of the grand canonical ensemble. In the model the average chemical potentials according to the composition and a new extra equation as a boundary condition are proposed for more accuracy and free experimental data calculations. The model can be used in any A₅B₃ type compounds with D8₁ structure. The establishment method of the statistical-thermodynamic model can be extended to other complicated structures. We apply the statistical-thermodynamic model to α-Nb₅Si₃ and the parameters used in the model are obtained from the first-principles' calculations. From these parameters the expression for the point defect concentrations as a function of compositions and temperatures is obtained by numeral calculations. The constitutional defects and thermal defects in α-Nb₅Si₃ are discussed.     

T形焊缝未焊透宽度的测定

在制作港口起重机械和森工机械中，采用了制作容易、省工省料的T形焊缝，焊缝中允许存在未焊透，但为保证机械质量和安全性，对未焊透宽度有一定限制，这就要求对焊缝未焊透宽度和位置进行测量。笔者根据未焊透的特点以及普通斜探头和直探头的声场结构，采用未焊透端线定位法和两端线同时回波声程定位法对T形焊缝的内部和根部未焊透进行检测，经超声波和焊缝低倍宏观检验相比较，前者检测方便，准确度高，重复性好。     

STUDY ON THE STABILITY OF T’PHASE IN THE Al-Zn-Cu TERNARY SYSTEM

The phase constitutes and phase compositions in the eight alloys designed with dif-ferent compositions of Al--Zn--Cu system have been determined after the homogenoustreatment and then equilibrium cooling to 20℃ by use of optical microscope, electronprobe microanalysis and X--ray diffraction. It has been found that there existed the T'phase in the seven alloys. Consequently, it was testified that the T' phase was stableat room temperature. At the same time, the phase relationship was not locally rightfor the isothermal section of 20℃ of Al--Zn--Cu system of the ASM published in 1997.     

激光熔覆TiC增强FeAl金属间化合物基复合材料涂层磨损性研究

利用激光熔覆技术在1Cr18Ni9Ti奥氏体不锈钢表面制得了以TiC为增强相、以FeAl 金属间化合物为基体的耐磨复合材料涂层，研究了激光熔覆。FiC／FeAl复合材料涂层在干滑动磨损条件下的耐磨性能及磨损机制。结果表明：随着载荷和滑动速率的增加，TiC／FeAl金属间化合物基复合材料涂层的磨损速率增加，其磨损机制随着载荷的增加逐渐由磨料磨损向粘着磨损转变；激光熔覆层中TiC体积分数的增加，一方面提高了涂层的磨料磨损抗力，另一方面降低了熔覆层表面与对磨材料之间的粘着倾向，提高了TiC／FeAl涂层的滑动磨损性能。激光熔覆TiC/FeAl金属间化合物基复合材料涂层具有优异的耐磨性能并随TiC体积分数的增加而提高。     

Mercury transformation across particulate control devices in six power plants of China: The co-effect of chlorine and ash composition

This paper presents the results of field measurements on mercury speciation in six power plants of China by applying the Ontario hydro method. During the tests, flue gas was sampled simultaneously before and after particulate control devices (electrostatic precipitator and fabric filter baghouse) along with the pulverized coal, bottom ash and fly ash sampling. The amount of oxidized mercury in gas phase before and after ESP/FF suggests that mercury oxidation after combustion is a kinetically controlled process. The comparison of mercury speciation in different power plant indicates a clear relationship with coal type, especially the chlorine concentration and the basic ash compositions in coal. Both of the factors are analyzed quantitatively in this study. A new parameter C (ratio of chlorine in coal to base/acid ratio) has been introduced to evaluate the co-effect of the two factors above on mercury speciation.     

提高自主创新能力促进模具行业快速发展

“十五”期间,中国橡胶工业实现了持续、快速、健康的发展,作为给橡胶配套的模具企业生产形势也是蒸蒸日上,民间投资积极性很高,民营企业的发展非常快。子午胎模具是橡胶模具里技术含量最高、应用领域最广、市场前景最好的模具,规模较大的轮胎模具企业从生产斜交胎、力车胎模具转为生产子午胎模具。同时,为了适应市场的需求,各企业纷纷加大对技术的投入,在制造手段上大力应用高新技术。不仅从国外引进先进的生产技术,还从国外引进五轴以上加工中心,实现了CAD/CAM/CAE(计算机辅助分析)。信息化的广泛应用优化了设计和加工过程,使模具设计…     

β-萘乙醚的合成中催化剂应用进展

β-萘乙醚是一种合成香料,广泛用于生产香皂、化妆品和洗涤剂等行业中,还可以作玫瑰香、柠檬香等香料的定香剂.综述了酸性催化剂、碱性催化剂和相转移催化剂等催化合成β-萘乙醚的方法.并对各催化剂的性能、优缺点进行了分析.通过比较发现与其它催化剂相比,使用固载相转移催化剂来合成β-萘乙醚具有反应条件温和,反应时间短,产率高,操作简单,不污染环境,而且易回收并能够重复使用,具有较好的应用前景.     

RTM工艺中气泡形成及消除研究

总结了关于RTM（树脂压铸）工艺中气泡缺陷的文献报道，对RTM中气泡缺陷的形成机理、影响因素及各研究者提出的消泡方法、理论和模型进行了概述，同时对RTM工艺中气泡缺陷的研究现状给予充分关注，并对RTM缺陷研究的未来方向进行了展望。     

Electron Emission from Barium Strontium Titanate Ceramics

This paper focuses on understanding the influence of materials' properties on the ferroelectric electron emission. Ferroelectric ( x =1.0 and 0.8) and paraelectric ( x =0.67 and 0.5) compositions of barium strontium titanate (Ba _x Sr_{(1− x )}TiO₃) system were chosen for study based on their different ferroelectric and dielectric properties. Similar emission current waveforms were obtained from four compositions with negative triggering voltage applied to the rear electrode of the samples. It was difficult to explain the experimental results using the spontaneous polarization-switching model. The mechanism of electron emission from Ba _x Sr_{(1− x )}TiO₃ ceramics was ascertained to surface plasma emission.