添加物对ZrO2系快离子导体烧结性能的影响

本文介绍了１３２０℃下，ＣａＯ，Ｙ２Ｏ３等稳定剂，低融物组成及１－６价阳离子化合物对ＺｒＯ２烧结性能的影响并列举出材料的晶型及某些主要性能。     

CO2在全氟羧酸离子交换膜内促进传质特性的研究

本文以全氟羧酸离子交换膜为支撑体、乙二胺(EDA)为活性络合剂、制备促进传质膜。在常用的工业条件下,测定了纯CO_2以及CO_2/N_2二元混合物在该膜内的渗透通量。实测结果表明,此膜对CO_2的促进因子可达13.8,而对CO_2/N_2的分离因子高达316。本文假设促进传质过程的控制步骤为气体在膜相的扩散,据此导出了相应的机理模型,该模型与实测结果吻合良好。     

陶瓷原料中SiO_2的钼酸银沉淀法测定

通过实验,发现络合滴定用的指示剂——偶氮胂—Ⅲ,可用作本测定中的沉淀滴定指示剂。根据标准 AgNO_3溶液同 MoO_4~(2-)的定量反应,计算出以硅钼黄 Hg[Si(Mo_2O_7)_6]形式存在的MoO_4~(2-)量,再据以算出硅酸盐中 SiO_2的含量。     

State space approximation for general fractional order dynamic systems

Approximations for general fractional order dynamic systems are of much theoretical and practical interest. In this paper, a new approximate method for fractional order integrator is proposed. The poles of the approximate model are unrelated to the order of integrator. This feature shows benefits on extending the algorithm to the systems containing various fractional orders. Then a unified approximate method is derived for general fractional order linear or nonlinear dynamic systems via combining the proposed new method with the distributed frequency model approach. Numerical examples are given to show the wide applicability of our method and to illustrate the acceptable accuracy for approximations as well.     

Secure and robust image hashing via compressive sensing

Image hash functions find extensive applications in content authentication, database search. This paper develops a novel algorithm for generating a secure and robust image hash based on compressive sensing and Fourier-Mellin transform. Firstly, we incorporate Fourier-Mellin transform into our method to improve its performance under rotation, scale, transition attacks. Secondly, we exploit the property of dimension reduction inherent in compressive sensing for hash design. The statistic structure and sparse of the wavelet coefficients assure efficient compression in situation of including maximum the image features. The hashing method is computationally secure without additional randomization process. Such a combined approach is capable of tackling all types of attacks and thus can yield a better overall performance in multimedia identification. To demonstrate the superior performance of the proposed schemes, receiver operating characteristics analysis over a large image database is performed. Experimental results show that the proposed image hashing is robust to a wide range of distortions and attacks. When compared with the current state-of-the-art methods, the proposed method yields better identification performances under geometric attacks such as rotation attacks and brightness changes.     

刍议市政道路养护机械优化配置评价指标体系构建

市政府道路是城市道路的主要组成部分。通过对市政府道路养护的必要性、养护机械配置的问题以及如何构建合理的评价指标体系等进行阐释,为市政府道路养护工作提供相应的参考意见。     

壳聚糖固定化脲酶生物传感器选择性测定铜离子

基于重金属对脲酶的抑制作用,研制了用于测定铜离子的生物传感器。该生物传感器的制备以壳聚糖为载体,将脲酶固定于pH电极表面。由于壳聚糖对Cu2+的富集,该生物传感器展现出高灵敏度。在样品溶液中加入5 mmol/L NaI,可以消除Hg2+和Ag+的干扰,从而实现Cu2+的选择性检测。在0.005～0.5μg/mL的浓度范围内,脲酶活性的抑制率与Cu2+浓度的对数呈良好的线性响应关系,其检出限为0.002μg/mL。将使用后的生物传感器浸泡于0.5 mmol/L的EDTA溶液再生5 min,被Cu2+抑制的脲酶的活性可以得到恢复。     

基于移动平台的校园资讯系统设计与实现

为了让高校师生可以快捷方便地获取到校园各类资讯,摆脱时间和空间的限制,设计了一种基于移动平台的校园资讯系统。该系统在PC平台上采用Asp.Net和SQL Server 2005技术,基于B/S的三层网络结构设计,在移动平台上基于C/S模式设计并开发了一个具备相应功能的Android手机客户端应用[1]。该系统具有查询课程、查询教室、查询考试安排、学生交友、发布商品、查询商品等基本功能。该移动平台系统界面友好,操作方便,资讯丰富,极大地方便了高校师生的学习、工作和生活。     

甲缩醛空气氧化制甲醛催化剂的研制和工艺条件探讨

考察了铁钼催化剂对甲缩醛空气氧化制甲醛的催化性能。制备了多种不同钼铁比和第三、第四组分的催化剂,进行了活性评价和筛选,探讨了适宜的工艺条件范围。对于所选定的催化剂(钼铁比为1.82～1.88;铬铁比为0.1～0.38)在适宜的工艺条件(甲缩醛进料浓度4.5～5.5％;甲缩醛和氧气进料比1:2.0±0.2;空速12000～22000h~(-1);热点温度370～390℃)下,甲醛收率可达85％左右。