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21.
Analysis of characteristic odors from human male axillae 总被引:7,自引:0,他引:7
Xiao -nong Zeng James J. Leyden Henry J. Lawley Kiyohito Sawano Isao Nohara George Preti 《Journal of chemical ecology》1991,17(7):1469-1492
A number of studies concerning the analysis of axillary odors have assumed that the characteristic odor produced in the axillae is due to volatile steroids and isovaleric acid. Organoleptic evaluation of Chromatographic eluants from axillary extracts was employed to isolate the region in the chromatogram where the characteristic odor eluted. The odor of the dissolved eluant was eliminated when it was treated with base, suggesting that acids make up the characteristic axillary odor. Subsequent extraction of the pH-adjusted axillary extract in conjunction with organoleptic evaluation of the Chromatographic eluant, preparative gas chromatography, and analysis by GC-MS as well as GC-FTIR showed the presence of a number of C6 to C11 straight-chain, branched, and unsaturated acids as important contributors to the axillary odor. The major odor component is (E)-3-methyl-2-hexenoic acid. Three homologous series of minor components are also important odor contributors; these consist of the terminally unsaturated acids, the 2-methyl-C6 to -C10 acids and the 4-ethyl-C5 to -C11 acids. These types of acids have not been reported previously as components of the human axillary secretions and have not been proposed previously as part of the principal odor components in this area. 相似文献
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In order to investigate the galvanic anodic protection (GAP) of ferrous metals (such as 410, 304 and 316 stainless steels) in acid solutions by doped polyaniline (PANi), separate doped PANi powder-pressed electrodes with different surface areas (the area ratio of the PANi electrode to stainless steel is between 1:1 and 1:2) have been prepared. These were coupled with ferrous metal in the following solutions: 5 M sulphuric acid, 5 M phosphoric acid and industrial phosphoric acid (containing 5 M phosphoric acid and 0.05% chloride ion) to construct a galvanic cell, in which PANi is cathode while ferrous metal is anode. The results indicate that a PANi electrode with sufficient area can provide corrosion protection to stainless steel in these acidic solutions. A pilot scale coupling experiment was carried out. The results indicate that PANi is a promising material as an electrode for the anodic protection of ferrous metals in acidic solutions in industrial situations. 相似文献
24.
本文介绍单光子时间分辨在线谱仪系统中的多道分析器与IBM PC/XT微型计算机接口的工作原理及控制程序。 相似文献
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“为网络注人文化的灵魂,为文化插上网络的翅膀”这句在2003中国首届国际网络文化博览会上四处飘扬的标语清楚地表明,当代信息革命在经历了从硬件为王到软件为王的转型过程后。正从网络为王时代走向内容为王时代;文化的本体形态、经济形态、技术形态伴随着信息技术的飞速发展正在 相似文献
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Constrained Drying of Aqueous Yttria-Stabilized Zirconia Slurry on a Substrate. I: Drying Mechanism 总被引:1,自引:0,他引:1
Aqueous yttria-stabilized zirconia slurry was cast on a substrate to form wet coatings. Both weight loss and thickness reduction were measured, during the drying process. Lateral drying was observed by in situ monitoring of the coating surface. The drying kinetics were classified as an initial constant rate period (CRP), followed by a falling rate period (FRP). Thickness reduction occurred in the CRP stage, and was uneven across the coating because of lateral flow. As tensile stresses developed within the coating because of the constrained volume shrinkage, crack formation and propagation occurred in the FRP stage and affected the drying rate. 相似文献
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Distributed Denial-of-Service (DDoS) attacks pose a serious threat to Internet security. Most current research focuses on
detection and prevention methods on the victim server or source side. To date, there has been no work on defenses using valuable
information from the innocent client whose IP has been used in attacking packets. In this paper, we propose a novel cooperative
system for producing warning of a DDoS attack. The system consists of a client detector and a server detector. The client
detector is placed on the innocent client side and uses a Bloom filter-based detection scheme to generate accurate detection
results yet consumes minimal storage and computational resources. The server detector can actively assist the warning process
by sending requests to innocent hosts. Simulation results show that the cooperative technique presented in this paper can
yield accurate DDoS alarms at an early stage. We theoretically show the false alarm probability of the detection scheme, which
is insensitive to false alarms when using specially designed evaluation functions.
This work is partially supported by HK Polyu ICRG A-PF86 and CERG Polyu 5196/04E, and by the National Natural Science Foundation
of China under Grant No. 90104005. 相似文献