亲电聚合路线合成聚醚醚酮酮砜的研究

用4,4′-二苯氧基二苯砜(DPODPS)分别与对苯二甲酰氯(TPC)、间苯二甲酰氯(IPC)或2,5-二氯对苯二甲酰氯(DCC)在1,2-二氯乙烷(DCE)中,以无水 AlCl_3为催化剂,在 N-甲基吡咯烷酮(NMP)存在下,通过付-克亲电聚合反应,制得了五种不同结构的聚醚醚酮酮砜(简称PEEKKS)。用红外光谱(IR)、X-射线衍射(XRD)、扫描电镜(SEM)、差示扫描量热(DSC)、热重(TG)及耐溶剂试验,对聚合物进行了表征。结果表明,五种聚合物的对数比浓粘度(η_(inh))均达到0.85以上.具有较低的熔融温度、良好的溶解性能和耐高温性能,PEEKKS 属于非晶态聚合物。     

B—ISDN宽带UNI信令点到多点配置的实现

本文根据ＩＴＵ－Ｔ最新的Ｑ．２９７１协议，以及笔者所从事的实际课题，提出一整套Ｂ－ＩＳＤＮ第三层ＵＮＩ信令的软件实现策略，其特点是能同时满足用户对点到点以及点到多点广播这两种通信方式的要求，而且可以动态配置。     

WAVELET ALGORITHM FOR INTEGRAL OPERATOR EQUATION AND ITS APPLICATIONS TO ELECTROMAGNETIC PROBLEMS

A brief summary of the basic theory of wavelet is proposed. The properties of wavelet function are discussed. The possible applications of wavelet to electromagnetics are given. Examples show that the wavelet method is feasible and effective for solving electromagnetic problems.     

氧化锌压敏陶瓷烧结致密化过程的研究

本文研究了氧化锌压敏陶瓷的致密化过程，结果发现只有当烧结温度升高到一定值时，试样中的ＺｎＯ粉粒产生聚集，致密化过程才开始．致密化是瓷体获得稳定电性能的基础．低熔点添加剂Ｂ２Ｏ３可以降低致密化的起始温度，而致密化过程中的等温烧结对ＺｎＯ压敏陶瓷的最大密度几乎没有影响．     

Locally optimum rank detection of correlated random signals inadditive noise

Nonparametric detection of a zero-mean random signal in additive noise is considered. The locally optimum detector based on signs and ranks of observations is derived, for good weak-signal detection performance under any specified noise probability density function. This detector is shown to have interesting similarities to the locally optimum detector for random signals. It may also be viewed as a generalization of the locally optimum rank detector for known signals. Examples of the test statistic of the detector are given for some specific noise probability density functions. Asymptotic and finite sample-size performance of the locally optimum rank detector is also considered     

Cure reaction for modified diallylbisphenol A/diaminodiphenylsulfone/bismaleimide

The glass‐transition temperature as a function of curing conversion for a modified diallylbisphenol A/diaminodiphenylsulfone/bismaleimide (BMI) resin was investigated at different temperature regimes and modeled using a modified Di Benedetto equation. Although the relationship between the glass‐transition temperature and conversion of the BMI system conforms to the Di Benedetto equation for α < 0.6 and at lower cure temperatures, at higher cure temperatures the results deviated significantly from the equation; thus, it was an inadequate model for the system. Fourier transform IR analysis showed that the major crosslinking reactions did not occur during cure for the modified BMI at and below 150°C. However, as the cure temperature was increased, the crosslinking reactions responsible for 3‐dimensional network structures became more dominant. At 190°C the C? N? C_stretch vibration of the uncured maleimide ring converted into succinimide rings in the curing process. Simultaneously, a decrease was observed for the absorbance bands of ? C? H_bending (maleimide). The higher cure temperatures induced a significantly faster initial crosslinking rate and also resulted in a shorter period of time after which further crosslinking was retarded, because the increase in the crosslinks also physically slowed further crosslinking activity. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 85: 227–235, 2002     

Design aspects of planar and conventional SMPS transformer: a cost benefit analysis

The intent of this paper is to design a high-frequency transformer that is to be incorporated into the DC/DC pulsewidth-modulated switch-mode power supplies by two different technical approaches: a conventional wound-coil magnetic using copper wires, and a planar magnetic with layered copper tracks on laminated printed circuit board. Comparisons will be made between the two approaches in terms of profile: mounting height and surface area, and performance: power losses and efficiency. Other indicators like temperature rise and leakage inductance that causes electromagnetic interference, and cost, materials, and process fluency are also to be looked into. A sandwiched configuration for primary and secondary windings is proposed for the planar type. Issues arising and typical phenomena encountered will be discussed in detail. Primarily, the dominating factor in performance, cost effectiveness, or circuit compactness that restrains the choice of a particular type is to be evaluated.     

汽油辛烷值智能调合系统

采取一种能够在线学习、不断提高、建立一系列模型的策略，提出了一种具有学习功能的汽油辛烷值智能调合系统。该系统可以根据成品汽油辛烷值指标、生产成本和市场价格等因素提供一个较好的油品调合调度方案。实际应用结果表明，利用参数学习的方法计算调合汽油辛烷值是可行的。     

云龙水库大坝表面变形观测资料分析

1工程概况云龙水库是昆明市掌鸠河引水供水工程的水源工程,位于昆明市西北部禄劝县的云龙乡岔河村附近,距昆明市区约86km。大坝坝址选在金沙江水系二级支流掌鸠河上游峡谷河段内,初期规模正常蓄水位2087.97m,校核洪水位2091.98m;终期规模水库正常蓄水位2089.67m,设计洪水位2092.59m,校核洪水位2093.58m。初期规模总库容4.48亿m3,终期规模总库容4.84亿m3,属大(2)型水库工程,工程等别为Ⅱ。水库枢纽建筑物由大坝,泄洪、导流隧洞,引水隧洞,溢洪道等组成。除溢洪道按初期规模兴建外,其余枢纽建筑物均按终期规模兴建。泄洪、导流和引水建筑物布置…     

Inventory routing with continuous moves

The typical inventory routing problem deals with the repeated distribution of a single product from a single facility with an unlimited supply to a set of customers that can all be reached with out-and-back trips. Unfortunately, this is not always the reality. We introduce the inventory routing problem with continuous moves to study two important real-life complexities: limited product availabilities at facilities and customers that cannot be served using out-and-back tours. We need to design delivery tours spanning several days, covering huge geographic areas, and involving product pickups at different facilities. We develop an innovative randomized greedy algorithm, which includes linear programming based postprocessing technology, and we demonstrate its effectiveness in an extensive computational study.