Investigation of machining characteristics in rotary ultrasonic machining of alumina ceramic

Alumina ceramic is well documented as a much-demanded advanced ceramic in the present competitive structure of manufacturing and industrial applications owing to its excellent and superior properties. The current article aimed to experimentally investigate the influence of several process variables, namely: spindle speed, feed rate, coolant pressure, and ultrasonic power, on considered machining characteristics of interest, i.e., chipping size and material removal rate in the rotary ultrasonic machining of alumina ceramic. Response surface methodology has been employed in the form of a central composite rotatable design to design the experiments. Variance analysis testing has also been performed with a view to observing the consequence of the considered parameters. The microstructure of machined rod samples was evaluated and analyzed using a scanning electron microscope. This analysis has revealed and confirmed the presence of plastic deformation that caused removal of material along with brittle fractures in rotary ultrasonic machining of alumina ceramic. The validity and competence of the developed mathematical model have been verified with test results. The multi-response optimization of machining responses (material removal rate and chipping size) has also been attempted by employing a desirability approach, and at an optimized parametric setting the obtained experimental values for material removal rate and chipping size were 0.4166?mm³/s and 0.5134?mm, respectively, with a combined desirability index value of 0.849.     

A novel application of micro-EDM process for the generation of nickel nanoparticles with different shapes

This article explains production of nickel nanoparticles through a micro-electrical discharge machining (EDM) process with a combination of different process parameters. The production of nickel nanoparticles was carried out in a dielectric medium (deionized water) with developed micro-EDM while polyvinyl alcohol worked as the stabilizing agent. The characterization of nickel nanoparticle was done by scanning electron microscope (SEM), Energy-dispersive X-ray spectroscopy (EDS), X-ray diffraction (XRD), UV–Vis spectroscopy, and Fourier transform infrared (FTIR) analysis. From this investigation, the mean crystal size of the nickel nanoparticles was found to be in the range of 15–20?mm for a pulse-on time variation of 2–0.3?µs and the crystal size was found to decrease with the decrease of pulse-on time. It was also observed that with this decrease, the shape and size of nickel nanoparticles change from spherical to needle-like. The dispersion stability of nickel nanofluid was determined by viscosity measurements and the dynamic viscosity was noted to decrease by decreasing the pulse duration. From the FTIR spectrum results, it was confirmed that the synthesized nickel nanoparticles in deionized water were pure and monolithic. UV–Vis–NIR spectroscopy depicted that the band gap energy increases with a reduction in the pulse-on time and obtains a higher band gap (5.31?eV) for 0.3?µs pulse-on time.     

Dehazing of remote sensing images using improved restoration model based dark channel prior

Haze degrades visual information of remotely sensed images. Therefore, haze removal is a demanding and significant task for visual multispectral information improvement. The existing haze removal techniques utilize different restrictions and before restoring hazy images in an efficient manner. The review of existing haze removal methods demonstrates that the haze-free images suffer from colour distortion and halo artefacts problems. To solve these issues, an improved restoration model based dark channel prior is proposed in this paper. The proposed technique has redefined transmission map, with the aim to reduce the colour distortion problem. The modified joint trilateral filter is also utilized to improve the coarse estimated atmospheric veil. The experimental results reveal that the proposed approach provides visually significant haze-free images and also preserves the significant detail.     

Development and validation of a Re-Modified Work-Style Short Form Questionnaire for assessment of stress in medical practitioners working in Indian hospitals

Medical practitioners are unduly stressed, leading to ill health, loss of work efficiency, sometimes affecting decision-making capability. The present study was conducted with the aim to quantify the psychosocial factors that affect the medical practitioners working in Indian hospitals. This study constructed and validated Re-Modified Work-Style Short Form Questionnaire, an eight-item instrument based on work style of 108 medical practitioners comprising Indian physicians and surgeons. The re-modified tool had acceptable validity and internal consistency, which the modified one did not. Explorative factor analysis identified and labelled three factors: ‘Working through pain’, ‘Deadlines/pressure’ and ‘Self-imposed workload’. The findings of the study reveal that the mean total work style score exceeded the standardised limits ≥16, which suggests that the work style of medical practitioners working in Indian hospitals are at risk which may precipitate psychosocial stress. Factor weights was derived through Analytic Hierarchy Process to prioritise the relative importance of three potential work-style factors. The study may help to increase the preventive strategies to proactively reduce the effect of risk factors for the precipitation of stress, successfully leading to its attenuation.     

Shear wave propagation in vertically heterogeneous viscoelastic layer over a micropolar elastic half-space

This article deals with the propagation of SH-wave in a vertically heterogeneous viscoelastic layer lying over a micropolar elastic half-space. Dispersion and damping equations are obtained analytically in closed form. Phase and damped velocities are computed numerically and depicted by means of a graph to exhibit the substantial effect of heterogeneity, viscoelasticity (internal friction), and micropolar parameter. As a special case of the problem, it is found that deduced dispersion relation is well in agreement to the classical-Love wave equation and damping equation vanishes identically for the isotropic case. Influence of micropolarity present in the medium of half-space is highlighted through comparative study.     

Effect of undulation on SH-wave propagation in corrugated magneto-elastic transversely isotropic layer

This article delves to study the effect of corrugated boundary surfaces on the propagation of horizontally-polarized shear waves (SH-waves) in a magnetoelastic transversely isotropic layer under a hydrostatic state of stress lying over an elastic half-space under gravity. A dispersion equation has been derived in closed-form and is found to be in good agreement to the classical Love-wave equation. The effect of magnetoelasticity, hydrostatic state of stress, gravity, corrugation, position parameter, and undulation on the phase velocity of the SH-wave has been identified. Numerical computation along with graphical demonstration has been carried out for cadmium, magnesium, and zinc materials of hexagonal symmetry to highlight some significant facts.     

Green synthesis of highly stable carbon nanodots and their photocatalytic performance

The present study reports a novel, facile, biosynthesis route for the synthesis of carbon nanodots (CDs) with an approximate quantum yield of 38.5%, using Musk melon extract as a naturally derived‐precursor material. The synthesis of CDs was established by using ultraviolet–visible (UV–vis) spectroscopy, Dynamic light scattering, photoluminescence spectroscopy, X‐ray diffraction, transmission electron microscopy and Fourier transform infrared (FTIR) spectroscopy. The as‐prepared CDs possess an eminent fluorescence under UV–light (λ _ex  = 365 nm). The size range of CDs was found to be in the range of 5–10 nm. The authors further explored the use of such biosynthesised CDs as a photocatalyst material for removal of industrial dye. Degradation of methylene blue dye was performed in a photocatalytic reactor and monitored using UV–vis spectroscopy. The CDs show excellent dye degradation capability of 37.08% in 60 min and reaction rate of 0.0032 min⁻¹. This study shows that synthesised CDs are highly stable in nature, and possess potential application in wastewater treatment.Inspec keywords: carbon, nanostructured materials, nanofabrication, catalysis, photochemistry, ultraviolet spectra, visible spectra, photoluminescence, X‐ray diffraction, transmission electron microscopy, Fourier transform infrared spectra, fluorescence, dyesOther keywords: green synthesis, highly stable CD, photocatalytic performance, biosynthesis route, carbon nanodots, quantum yield, Musk melon extract, naturally derived‐precursor material, ultraviolet‐visible spectroscopy, dynamic light scattering, photoluminescence spectroscopy, X‐ray diffraction, transmission electron microscopy, Fourier transform infrared spectroscopy, FTIR spectroscopy, fluorescence, biosynthesised CD, photocatalyst material, industrial dye, methylene blue dye degradation, photocatalytic reactor, UV‐vis spectroscopy, wastewater treatment, size 5 nm to 10 nm, time 60 min     

Fatigue crack growth prediction in nuclear piping using Markov chain Monte Carlo simulation

In this paper, we present and demonstrate a methodology to improve probabilistic fatigue crack growth (FCG) predictions by using the concept of Bayesian updating using Markov chain Monte Carlo simulations. The methodology is demonstrated on a cracked pipe undergoing fatigue loading. Initial estimates of the FCG rate are made using the Paris law. The prior probability distributions of the Paris law parameters are taken from the tests on specimen made of the same material as that of pipe. Measured data on crack depth over number of loading cycles are used to update the prior distribution using the Markov chain Monte Carlo. The confidence interval on the predicted FCG rate is also estimated. In actual piping placed in a plant, the measured data can be considered equivalent to the data received from in-service inspection. It is shown that the proposed methodology improves the fatigue life prediction. The number of observations used for updating is found to leave a significant effect on the accuracy of the updated prediction.     

Mechanical and Thermophysical Properties of Cerium Monopnictides

The ultrasonic attenuation due to phonon–phonon interaction, thermoelastic relaxation and dislocation damping mechanisms has been investigated in cerium monopnictides CeX (X: N, P, As, Sb and Bi) for longitudinal and shear waves along \({\langle }100{\rangle }\), \({\langle }110{\rangle }\) and \({\langle }111{\rangle }\) directions. The second- and third-order elastic constants of CeX have also been computed in the temperature range 0 K to 500 K using Coulomb and Born–Mayer potential upto second nearest neighbours. The computed values of these elastic constants have been applied to find out Young’s moduli, bulk moduli, Breazeale’s non-linearity parameters, Zener anisotropy, ultrasonic velocity, ultrasonic Grüneisen parameter, thermal relaxation time, acoustic coupling constants and ultrasonic attenuation. The fracture/toughness ratio is less than 1.75, which shows that the chosen materials are brittle in nature as found for other monopnictides. The drag coefficient acting on the motion of screw and edge dislocations due to shear and compressional phonon viscosities of the lattice have also been evaluated for both the longitudinal and shear waves. The thermoelastic loss and dislocation damping loss are negligible in comparison to loss due to Akhieser damping (phonon–phonon interaction). The obtained results for CeX are in qualitative agreement with other semi-metallic monopnictides.     

Self-nanoemulsifying drug delivery system of docosahexanoic acid: development,in vitro,in vivo characterization

Context: Docosahexanoic acid (DHA) is an essential omega-3 fatty acid for normal brain development and its use has increased considerably in recent years.

Objective: The aim of this study is to develop and evaluate self-nanoemulsifying drug delivery systems (SNEDDS) of DHA for improved palatability, dispersibility and bioavailability.

Methods: The SNEDDS were prepared and evaluated for miscibility, employing different combinations of olive oil and soyabean oil as oil phase, Span 80, Span 20, soya phosphatidylcholine, Labrafil M 1944 CS as surfactants while Tween 80, PEG 400, Cremophor RH40 and propylene glycol as cosurfactants. Thermodynamically stable SNEDDS were characterized for dispersibility, self-emulsification time, droplet size, zeta potential along with sensory analysis. The optimized formulation was subjected to ex vivo and in vivo evaluation such as intestinal permeability, memory performance test, brain concentration and histopathology studies.

Results: The optimized SNEDDS formulation showed emulsification time of 27?±?4.7?s with droplet size of 17.6?±?3.5?nm and zeta potential of??37.6?±?0.5?mV. Intestinal absorption study depicted 18.3%, 21.5%, 41.5%, 98.7% absorption of DHA with SNEDDS-based formulation in comparison to 8.2%, 15.1%, 28.8%, 46.1% absorption of DHA with oil-based marketed formulation after 0.5, 1, 2 and 4?h. DHA concentration in brain homogenate was found to be increased to 2.6-fold in comparison to DHA-marketed formulation. This could be ascribed to enhanced dispersibility and bioavailability of DHA from nanosized formulation.

Conclusion: The developed formulation led to enhanced dispersibility and bioavailability of DHA due to the formation of nanodroplets.