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61.
Adam Alemayehu Dominika Zákutná Soňa Kohúteková Václav Tyrpekl 《Journal of the American Ceramic Society》2022,105(7):4621-4631
Ceria, pure or doped, is an important electrolyte material in solid oxide fuel cells, catalysts, and plutonium surrogates. Even though ceria is a widely studied material, its coprecipitation with the most common doping element, gadolinium, remains mostly overlooked. Here, we present a comprehensive study of gadolinium–cerium oxalates prepared by coprecipitation of gadolinium (III) and cerium (III) salts by oxalic acid under different reaction conditions and element ratios. For this purpose, we assessed the effects of basic precipitation conditions on the final oxalate size, shape, and conversion into the corresponding oxides. The results showed that coprecipitation with oxalic acid yields and ideal solid solution, which translates into the oxides. This low-cost and straightforward synthetic route provides then high-quality solid solutions of Ge–Gd in the oxide lattice. Thus, this approach has a high industrialization potential, with significant advantages over hydrolysis or hydrothermal techniques. 相似文献
62.
Nam-Hyung Kim Tae Hyung Lee Joong So Choi 《Korean Journal of Chemical Engineering》2000,17(5):534-540
The superabsorbent poly(AM-SAS-AA)s were synthesized to improve the water absorption capacities in comparison with the poly(AM-SAS)
by an aqueous solution polymerization method from acrylamide (AM), sodium allylsulfonate (SAS), and acrylic acid (AA). The
reaction conditions were controlled by varying the AA concentrations and fixing other agent concentrations to obtain the optimal
superabsorbent poly(AM-SAS-AA). The poly(AM-SAS-AA) showed maximal absorption capacity at 0.3 mol/L among AA concentrations
from 0.053mol/L to 0.4 mol/L. The water absorption capacities of poly(AM-SAS-AA)s prepared at the optimal reaction condition
were measured within the temperature ranges from 298.15K to 318.15K. Those experimental data were used to describe the effect
factors on absorption capacities and swelling equilibria data among those data were correlated with the swelling models to
estimate the interchange energy parameters. Each swelling models combined with group contribution models (UNIFAC, ASOG) was
introduced to calculate the swelling equilibria of water(1)/poly(AM-SAS-AA)(2) systems. The swelling behaviors could be described
by the estimated parameters, and the calculated values agreed well with the experimental data. 相似文献
63.
64.
Dr. Dae-Shik Kim Dr. Atsushi Endo Dr. Francis G. Fang Dr. Kuan-Chun Huang Dr. Xingfeng Bao Dr. Hyeong-wook Choi Dr. Utpal Majumder Dr. Young Y. Shen Steven Mathieu Xiaojie Zhu Kristen Sanders Dr. Thomas Noland Dr. Ming-Hong Hao Dr. Yu Chen Dr. John Y. Wang So Yasui Karen TenDyke Jiayi Wu Christy Ingersoll Kara A. Loiacono Dr. Janna E. Hutz Dr. Nadeem Sarwar 《ChemMedChem》2021,16(11):1741-1744
A strategy for creating potent and pan-genotypic stimulator of interferon genes (STING) agonists is described. Locking a bioactive U-shaped conformation of cyclic dinucleotides by introducing a transannular macrocyclic bridge between the nucleic acid bases leads to a topologically novel macrocycle-bridged STING agonist (MBSA). In addition to substantially enhanced potency, the newly designed MBSAs, exemplified by clinical candidate E7766 , exhibit broad pan-genotypic activity in all major human STING variants. E7766 is shown to have potent antitumor activity with long lasting immune memory response in a mouse liver metastatic tumor model. Two complementary stereoselective synthetic routes to E7766 are also described. 相似文献
65.
66.
Ning-Ping Foo Yu-Fan Liu Ping-Ching Wu Chung-Hsi Hsing Bu-Miin Huang Edmund-Cheung So 《International journal of molecular sciences》2021,22(13)
Midazolam (MDZ) could affect lymphocyte immune functions. However, the influence of MDZ on cell’s K+ currents has never been investigated. Thus, in the present study, the effects of MDZ on Jurkat T lymphocytes were studied using the patch-clamp technique. Results showed that MDZ suppressed the amplitude of delayed-rectifier K+ current (IK(DR)) in concentration-, time-, and state-dependent manners. The IC50 for MDZ-mediated reduction of IK(DR) density was 5.87 μM. Increasing MDZ concentration raised the rate of current-density inactivation and its inhibitory action on IK(DR) density was estimated with a dissociation constant of 5.14 μM. In addition, the inactivation curve of IK(DR) associated with MDZ was shifted to a hyperpolarized potential with no change on the slope factor. MDZ-induced inhibition of IK(DR) was not reversed by flumazenil. In addition, the activity of intermediate-conductance Ca2+-activated K+ (IKCa) channels was suppressed by MDZ. Furthermore, inhibition by MDZ on both IK(DR) and IKCa-channel activity appeared to be independent from GABAA receptors and affected immune-regulating cytokine expression in LPS/PMA-treated human T lymphocytes. In conclusion, MDZ suppressed current density of IK(DR) in concentration-, time-, and state-dependent manners in Jurkat T-lymphocytes and affected immune-regulating cytokine expression in LPS/PMA-treated human T lymphocytes. 相似文献
67.
68.
Soo Cheong Chang Jin Sung Yoo Je Wan Woo Joong So Choi 《Korean Journal of Chemical Engineering》1999,16(5):581-584
Superabsorbent poly(acrylamide-sodiumallylsulfonate) was synthesized from acrylamide (AM) and sodiumallylsulfonate (SAS) by a solution polymerization method. N,N’-methylenebisacrylamide (BIS) was used as the crosslinker; potassium persulfite (PP) and N,N,N’,N’-tetra-methylenediamine (TMEDA) were used as the redox initiator during the synthesis. The absorption capacities of the synthesized superabsorbent poly(AM-SAS) were repeatedly measured to obtain the optimal poly(AM-SAS) according to the variations of monomer concentration at 298.15 K. Its maximal absorption capacity appeared as 811 times at 0.1 mol/L among from 0.01 mol/L to 0.16 mol/L of SAS concentrations. The swelling equilibria at those conditions from 298.15 K to 318.15 K were measured and used to estimate the parameters by correlating with the Flory-Huggins model. The swelling behavior could be described by the parameters and the calculated values agreed satisfactorily with the experimental data. 相似文献
69.
As Asian economies have grown rapidly, Asia has become a new leading market of the luxury goods industry. This paper used conjoint analysis (CA) for the optimal design of a luxury brand outlet mall to maximize the customer lifetime value (CLV). This approach complements a simple CA by considering CLV. The proposed approach is then applied to designing a suburban luxury brand outlet mall in Korea, a new concept to Korea. The results indicate that the optimal design for the outlet mall is the medieval European-style mall, with the linkage to Natural Tourism, which consists of the restaurants with delicious food and the stores with similar ratio between masstige and luxury brands. 相似文献
70.
Transmission delays occur when a virtual environment responds to the hand and head movements of an operator. The effects of hand and head-related delays on discrete manual performance was investigated experimentally and compared. Imposed hand and head-related pure delays equal to or greater than 110 ms and 220 ms, respectively, significantly increased hand Movement Time (MT). The effect of hand-related delays was greater than that of head-related delays of the same magnitude. A regression model describing the combined effects of both delays on MT is reported (R(2) = 0.95). Analyses of the interactions among delays, target width, and distances have shown the need to adopt the traditional classification of delays into (1) control delay, and (2) display delay. The use of this taxonomy and the regression analyses to describe and explain the effects of individual and combined effects of delays on discrete target-reaching task performance in virtual environments are discussed. 相似文献