Ultralow feeding gas flow guiding growth of large-scale horizontally aligned single-walled carbon nanotube arrays

On the basis of the rational analysis about the fluidic property of the system, an ultralow gas flow chemical vapor deposition (CVD) strategy was designed to prepare large-scale horizontally aligned ultralong single-walled carbon nanotube (SWNT) arrays. SWNT arrays could be well obtained under extremely low feeding flow of 1.5 sccm in a 1 in. quartz tube reactor. It was confirmed that the tubes grew floatingly and could cross microtrenches or climb over micro-obstacles in ultraslow gas flow. SWNTs arrays also could be formed no matter the substrate was placed vertically or upside down. The growth mechanism was discussed. Both the buoyancy effect induced by gas temperature/density difference and gas flow stability played dominant roles. More attractively, simultaneous batch-scale preparation of SWNT arrays was realized by the ultralow gas flow strategy. This new strategy turns to be more abstemious, efficient, promising, and flexible compared with the high gas flow rate fast-heating CVD processes.     

利用多米诺效应控制爆破拆除长渡槽

某渡槽为34跨,每跨23.5 m,最大架高17 m,全长799 m.出于对人身安全和设施不受损失考虑,围绕人工机械与爆破拆除两种方案进行论证后,决定用控制爆破拆除渡槽.文章论述了此工程爆破方案设计、技术参数及安全措施,最后取得圆满的爆破效果.     

云南滇黄精药渣中多糖含量的测定

以测定云南滇黄精药渣中多糖的含量为目的,采用热回流法提取总多糖,以葡萄糖为对照品制作标准曲线,采用苯酚-硫酸法和可见分光光度法测定多糖含量。研究结果表明该方法的线性关系良好,线性相关系数≥0.999,精密度良好,相对标准偏差≤3%,准确性良好,平均回收率为99.40%,测得6批滇黄精药渣中多糖的平均含量为4.47%,实验结果可为滇黄精的综合利用提供一定的参考。     

Rapid growth of angle-confined large-domain graphene bicrystals

In the chemical vapor deposition growth of large-area graphene polycrystalline thin films,the coalescence of randomly oriented graphene domains results in a high density of uncertain grain boundaries (GBs).The structures and properties of various GBs are highly dependent on the misorientation angles between the graphene domains,which can significantly affect the performance of the graphene films and impede their industrial applications.Graphene bicrystals with a specific type of GB can be synthesized via the controllable growth of graphene domains with a predefined lattice orientation.Although the bicrystal has been widely investigated for traditional bulk materials,no successful synthesis strategy has been presented for growing two-dimensional graphene bicrystals.In this study, we demonstrate a simple approach for growing well-aligned large-domain graphene bicrystals with a confined tilt angle of 30° on a facilely recrystallized single-crystal Cu (100) substrate.Control of the density of the GBs with a misorientation angle of 30° was realized via the controllable rapid growth of subcentimeter graphene domains with the assistance of a cooperative catalytic surface-passivation treatment.The large-area production of graphene bicrystals consisting of the sole specific GBs with a tunable density provides a new material platform for fundamental studies and practical applications.     

连续混炼过程比能耗分析

将连续混炼过程的有效比能耗分为升温、混炼、脱挥和建压比能耗,并提出了计算各项的一种方法。用该方法对不同机型、不同规格、不同加工对象的连续混炼机的比能耗进行了分析。结果表明,在多数连续混炼过程中,升温比能耗在总有效比能耗中所占比例都较大,建压比能耗所占比例都很小;原料热物性是影响有效比能耗及其构成的根本因素;当原料和混炼产物质量确定时,连续混炼机的螺杆与机筒结构、螺杆直径、产量、混炼工艺等都会影响有效比能耗及其构成。     

Growth and characterization of Pb0.97La0.02(Zr0.66Sn0.27Ti0.07)O3 antiferroelectric single crystals

Single crystals of Pb_0.97La_0.02(Zr_0.66Sn_0.27Ti_0.07)O₃ (PLZST) with the composition near the morphotropic phase boundary were grown by the flux method. The PbO–PbF₂–B₂O₃ system was used as a solvent. PLZST single crystals with the size of 4–6 mm are obtained and these crystals are slightly translucent after polishing. The splitting of (200) reflection peak indicates that the obtained crystals are of a single phase with tetragonal perovskite structure. The element contents of the grown crystals were measured by inductively coupled plasma atomic emission spectrometry. The chemical composition of the crystals is Pb_0.979La_0.014(Zr_0.666Sn_0.285Ti_0.049)O₃. Thermal properties and dielectric properties of PLZST single crystals were studied. The results show that flux-grown PLZST single crystals exhibit obvious endothermic processes and relaxor behaviors near the phase transition temperatures.     

关于细胞神经网络无性模板的设计

本文以连通片检测器无性模板的设计为例，给出了细胞神经网络中无性模板的设计方法及连通片检测器无性模板中各元素的数值范围。     

浅谈微生物实验室培养基制备

培养基的质量是微生物实验室检测工作的基础,事关检测工作的准确性、可靠性。因此,培养基的制备和使用是微生物实验室检测工作中的重要环节。本文针对培养基的储存、制备、灭菌后保存及灭菌效果检验进行分析,以便于保证检测结果的科学有效。     

A novel de-rusting method with molten salt precleaning and laser cleaning for the recycling of steel parts

Clean Technologies and Environmental Policy - Steel parts are a kind of high recovery value product for which de-rusting is the primary step in the recycling process. Laser cleaning is a popular...