Preparation of phenolic resin derived 3-D ordered macroporous carbon

Three-dimensionally ordered long-range macroporous carbon structures were prepared using commercially available phenolic resin by utilizing sacrificial colloidal silica crystalline arrays as templates that were subsequently removed by HF etching after pyrolysis in an argon atmosphere. SEM, TEM, and BET were employed to characterize the morphology and the surface area of the porous carbon structures. The pore size (150–1000 nm) and BET surface area, which reflect pore volume (298.6 m²/g (1.32 cm³/g) ∼ 93.7 m²/g (0.12 cm³/g)), of the macroporous carbon structures produced were approximately proportional to the size (150–1000 nm) of the sacrificial silica sphere templates used (annealing temp. 550°C). The achieved 550 nm porous carbon structures were examined to function as potential catalyst carriers and were successfully impregnated with Ag or Pt-Ru on their inner walls after borohydride reduction at room temperature. In addition, porous carbon patterns were fabricated using the ‘micromolding in capillary’ technique, which has potential applications in the microreaction technology.     

基于PXI总线的LVDS数据采集存储模块的设计

鉴于SAR原始数据量大以及数据传输速率限制的问题,设计了基于PXI的雷达回波和图像数据实时记录模块。大容量数据采集记录系统基于通用的商业PC平台设计,选用FPGA作为主控芯片对电路整体逻辑进行控制;利用LVDS作为数据传输接口对数据进行接收,实现了数据采集、缓存以及通过PXI总线上传至上位机硬盘,以便后续处理。文中介绍了系统方案的总体设计,以及采集存储硬件电路的设计,并对电路的关键技术给以详细的分析。     

脂肪酸系列表面活性剂的研究进展

概括和综述了4大类10余个脂肪酸系列表面活性剂的合成、性能和应用现状，重点评述了烷醇酰胺及其衍生物、乙氧基化脂肪酸甲酯、脂肪酸甲酯磺酸盐、N-酰基ED3A、氨基酸、咪唑啉、甜菜碱、双子表面活性剂等脂肪酸系列表面活性剂的研究进展。此系列表面活性剂易生物降解、安全、多功能和高效能。     

Preparation and morphology of electrically conductive and transparent poly(vinylchloride)-polypyrrole composite films

Summary The chemical process of preparing poly(vinylchloride)-polypyrrole composite films with high electrical conductivity and transparency has been studied. Pyrrole has been diffused into the poly(vinylchloride) matrix in the swelling medium of n-hexane and acetone mixture. The oxidative polymerization of the diffused pyrrole in the binary solvent system of acetonitrile and methanol gives high conductivity of the polypyrrole as well as the good penetration of the oxidant into the PVC polymer matrix. The analytical testing of the composite film shows the formation of homogeneous mixture of polypyrrole and poly(vinylchloride) conductive layer within the 1.0m of thickness on the film surface. The transparency of the composite film showed about 50–60% at 500 nm. The electrical conductivity of the composite was about 20 s/cm.     

Rheology-processing-property relationships in tubular blown film extrusion. I. High-pressure low-density polyethylene

Three different grades of high-pressure low-density polyethylene resin were used to establish relationships between tubular film blowability and the molecular parameters, namely, the molecular weight distribution (MWD) and the degree of long-chain branching (LCB), and also between the processing conditions and the mechanical properties of the tubular blown films produced. For the study, both the shearing and elongational flow properties of the resins were determined. During the tubular film blowing experiment we measured the freeze-line position, the tubular bubble diameter, the takeup speed, the axial tension, the pressure inside the tubular bubble, and the mass flow rate of the resin. The thickness of the tubular blown films was measured from the samples collected. In order to determine the tubular film blowability, we measured the maximum takeup speed at which the tubular blown bubble broke, for various blowup ratios. The measurements described above permitted us to calculate the tensile stresses at the freeze line, in both the machine and transverse directions, and they were found to be correlatable to the processing conditions employed. It has been found that the tubular film blowability is increased as the resin's MWD becomes narrower and the degree of LCB is less. It has been found further that a resin having lower elongational viscosity tends to give a greater draw-down ratio, indicating a better tubular film blowability. Finally, the tensile properties of the tubular blown films were found correlatable to the processing variables, namely, blowup and takeup ratios.     

"再听证"条款考疑

介绍了日本、韩国及我国台湾地区的行政程序法关于再次举行听证会的规定.分析了我国行政程序法试拟稿及部分地方立法中有关于再听证规定存在的问题,并提出了具体的修改意见.     

Application of open-pit and underground mining technology for residual coal of end slopes

Given the conditions of residual coal from the boundary of a flat dipping open-pit mine,which uses strip areas mining and inner dumping with slope-covering,we propose an open-pit and underground integrated mining technology for residual coal of end slopes.In the proposal a conveyance road and ventilation conveyance near the slope are built,corresponding to the pit mining area and the surface coal mine dump,as well as an interval haulage tunnel and air-inlet tunnel.The outcome shows that such mining method may reduce the effect to slope stability from underground mining,it does not affect the dumping advance and has a high recovery rate of residual coal resources.The working face is timbered by single hydraulic props,transported by a scraper conveyor and supported by coal walls.This method of mining is one of layered top coal caving,with high resource recovery,low production cost where positive economic benefit can be realized.     

基于广东区域性高职院校创业教育的思考——记广州城建职业学院学生创业教育的探索

职业素质是劳动者对社会职业了解与适应能力的一种综合体现,主要包括职业修养和职业技能。在高职院校中开展创业教育是我国经济形势发展的需要,对于培养学生的实践能力、创新精神和解决学生的就业压力有着十分重要的意义。广州城建职业学院的创业教育可以从以下三方面着手：一是转变观念,营造氛围;二是传授本领,打好基础;三是开展活动,提高能力,逐步探索出一条适合广州城建职业学院特色高职学生创业教育的新路子。     

生活质量视阈下的大学生“精神贫困”测量指标研究

高校大学生＂精神贫困＂现象已引起人们重视,成为多方关注话题。本文在梳理前人研究成果基础上,对＂精神贫困＂测量指标进行研究,以获得科学的测量指标体系,为获得真实科学的一手资料打进行理论论证。