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131.
Taichi Sato Takato Nakamura 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1984,34(7):375-380
The complexes of bivalent manganese, cobalt and copper formed in the extraction from hydrochloric acid solutions by trioctylamine (TOA, R3N) and trioctylmethylammonium chloride (Aliquat-336, R3R'NCl) in benzene have been examined by spectrophotometry and electron spin resonance spectroscopy. It was found that the moiety MCl2-4 in all complexes studied had a tetrahedral geometry, and that the M-Cl bond in the species (R3R′N)2MCl4 was rather more ionic than that in the species (R3NH)2MCl4, in which M = Mn, Co and Cu. 相似文献
132.
Junya Nakamura Taichi Takahashi Chih‐Wei Chen Yi‐Pai Huang Yasuhiro Takaki 《Journal of the Society for Information Display》2012,20(4):228-234
Abstract— The viewing freedom of the reduced‐view super multi‐view (SMV) display was analyzed. It was found that there are separate multiple viewing ranges in the depth direction; thus, a technique that selects an appropriate viewing range to increase the longitudinal viewing freedom has been developed. Pixels of a flat‐panel display viewed by the viewer's eyes through a lenticular lens were determined from three‐dimensional (3‐D) positions of the viewer's eyes, which were obtained using an eye‐tracking system that employed a stereo camera. Parallax images corresponding to the 3‐D positions of the viewer's eyes were generated, which were displayed by the determined pixels. The experimental results show that the proposed technique successfully increased the longitudinal viewing freedom. It is also shown that a video camera was able to focus on the produced SMV images. 相似文献
133.
For the purpose of efficient utilization of waste polystyrene, the recovery method of a styrene oligomer having a molecular weight of 1000–3000 was studied. Thermal and catalytic degradations were carried out. It was impossible to obtain a styrene oligomer with a molecular weight less than 5000 by thermal degradation in the temperature range of 300–500°C. Catalytic degradation in the presence of silica–alumina catalyst in the temperature range of 190–230°C made it possible to control the decrease in molecular weight and to obtain a styrene oligomer having a molecular weight of 500–3000. Simultaneously, the molecular structures of the reaction products from thermal and catalytic degradations were determined by NMR analysis. 相似文献
134.
A CALPHAD assessment of the Cu−Pt system has been carried out. Two and four sublattice models were applied to describe the
Gibbs free energies of ordered phases where the contribution of SRO is taken explicity into account through the reciprocal
parameters. The disordered fcc A1 and liquid phases were treated as substitutional solutions. A consistent set of parameters
for the phases in the Cu−Pt system as obtained, and those parameters can satisfactorily reproduce the experimental phase equilibria
and thermodynamic properties, such as enthalpies, activity of Cu, and long-range order parameters.
This paper was presented at the International Symposium on User Aspects of Phase Diagrams. Materials Solutions Conference
and Exposition, Columbus, Ohio, 18–20 October, 2004. 相似文献
135.
Tomoaki Namioka Taichi NaruseRyosuke Yamane 《International Journal of Hydrogen Energy》2011,36(9):5581-5588
In order to determine both the criterion for diagnosing the deterioration of Ni/ScSZ cermet anodes in solid oxide fuel cells (SOFCs) by tar contaminants in wood gas and the tolerance limit of tar in wood gas for such anodes, the influence of tar concentration in wood gas on anode deterioration behavior was examined by means of scanning electron microscopy. We found that the anode degradation mechanism consisted of three phenomena: the disappearance of Ni particles, the destruction of sintered ScSZ, and carbon deposition. Furthermore, the Ni particle disappearance occurred at lower tar concentrations than did sintered ScSZ destruction and apparent carbon deposition. Therefore, we propose that the disappearance of Ni particles be set as the criterion for confirming deterioration of Ni/ScSZ cermet anodes in SOFCs by tar. On the basis of this criterion, the tolerance limit of toluene in fuel gas was determined to be 3 g/Nm3 when the operating temperature, steam to carbon molar ratio, and current density were 1073 K, 1, and 0.5 A/cm2, respectively. The tolerance limit for tar for the fuel cell constructed herein was one to two orders of magnitude higher than that for internal combustion engines. 相似文献
136.
Structural changes of capillaries around muscle fibres following their degeneration and regeneration were further examined in the extensor digitorum longus muscle of the 24-month-old normal rat. Bundles of muscle fibres were divided into three types: muscle bundles consisting of large muscle fibres exclusively more than 35 microm in diameter (type 1), various-sized muscle fibres ranging from 10 to 60 microm in diameter (type 2) and only small muscle fibres 20-40 microm in diameter (type 3). The mean number of capillaries around a muscle fibre was extremely high in the type 3 muscle bundle (4.83) and much lower in the type 2 muscle bundle (2.72) compared with that in the type 1 muscle bundle (3.48). Capillaries in the type 1 muscle bundle were round or oval in shape and were of the continuous type. In the type 2 muscle bundle, capillaries around large degenerating muscle fibres showed an irregularly compressed shape and the scaffolds of basal laminae were often found around them, being a result of the destruction of capillaries. On the other hand, small-sized capillaries less than 5 microm in diameter, being possibly regenerating capillaries, were found around small (probably regenerating) muscle fibres and often had a small number (less than 10) of fenestrae. Capillaries in the type 3 muscle bundle, similar in shape and size to those in the type 1, frequently branched or joined, but some of them were partially destroyed. These findings suggest that capillaries degenerate and regenerate to remodel capillary networks around the muscle fibres following their degeneration and regeneration, and that to effectively supply oxygen and nutrients to regenerating muscle fibres, capillaries temporarily form fenestrae and then the capillary networks become dense by sprouts from the existing capillaries, but excess capillaries may be gradually destroyed following maturation of the muscle fibres. 相似文献
137.
We examined the structural changes of capillaries in the extensor digitorum longus muscle of aged (25 months) male BUF/Mna rats, which caused severe muscle weakness of hind legs during aging. The aged muscle mostly consisted of bundles of muscle fibres 15-35 microm in diameter (type 1). In some small areas, however, muscle bundles contained small muscle fibres mainly 15-25 microm in diameter (type 2), possibly indicating that these small fibres are in the course of regeneration after necrosis. Examination of serial ultrathin sections revealed some remarkable changes of capillaries in the type 2 muscle bundle. In some capillaries, the vascular lumen became discontinuous by several close contacts of opposed endothelial cells in their course, forming plural closed vascular segments. Moreover, a solitary endothelial cell was often observed within a scaffold of basal lamina, which remained after destruction of endothelial cells. The segmentation of capillaries and the occurrence of the scaffolds of basal laminae are considered to indicate the degenerative process of capillaries. In some instances, on the other hand, endothelial cells closely apposed each other with no vascular lumen for distances of up to 100 microm, and some capillaries had a narrow vascular lumen (1-3 microm diameter) for a long distance (approximately 300 microm), probably indicating that these structures are in the course of regenerating capillaries to remodel the capillary networks around the muscle fibres. Pericytic processes circularly arranged outside the endothelium at the slit-like and narrow vascular lumen, like hoops, possibly preventing the rupture of the newly-formed vascular lumen from the increased blood flow and/or blood pressure. In addition, the occasional occurrence of capillaries with fenestrations may participate to increase the supply of nutrients and oxygen to the regenerating muscle fibres. The present findings suggest that the capillary networks in the extensor digitorum longus muscle of aged BUF/Mna rats are remodelled following the regeneration of muscle fibres after necrosis, and that on occasion, neighbouring endothelial cells may closely contact with each other both in the degenerative and regenerative processes of capillaries. 相似文献
138.
Taichi Sato Takato Nakamura 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1982,32(3):469-475
Gallium hydroxide precipitated from aqueous gallium chloride solution on addition of alkalis at varying pH have been aged in the mother liquors for different periods of time. The resulting precipitates have been examined by X-ray diffraction and i.r. spectrophotometry. It is found that the precipitate, separated immediately from the mother liquor after preparation, exists in an amorphous type and transforms to α-gallium oxyhydroxide during aging independent of pH. 相似文献
139.
Water-soluble and water-insoluble β-cyclodextrin polymers (β-CDPs) were prepared from β-CD using 1,2,3,4-butanetetracarboxylic dianhydride (BTCA) as a cross-linker. The structures of the synthesized water-soluble and water-insoluble β-CDPs were characterized in detail using FT-IR, solution- and solid-state NMR, and 1H diffusion-ordered spectroscopic techniques. The water solubility of β-CDP was dependent on the reaction temperature as well as the initial feed ratio of β-CD and BTCA. The BTCA content and the ratio of BTCA molecules cross-linked and grafted to β-CD were also found to influence the water solubility of the polymers. Insoluble β-CDPs were effective in adsorbing bisphenol A (BPA) from aqueous media, with this absorption being highest in materials of low BTCA content, which corresponds to material of high β-CD content per unit mass of β-CDP. 相似文献
140.
We produced local polarized domains of ferroelectric P(VDF/TrFE) copolymer thin films on a carbon nanotube field-effect transistor (CN-FET) channel by atomic force microscopy (AFM). The drain current versus gate voltage (I(d)-V(g)) curves measured after forming the local polarized domains showed a shift in the threshold voltages. We also found that the amount of the shifts in the threshold voltages gradually decreased during the measurement of this characteristic over 100?h after forming the polarized domains. The mechanisms of the shifts in the threshold voltages and their decreasing behaviour were explained in terms of the excessive charges that were induced upon the formation of the polarized domains. 相似文献